JPH08901A - 細管蒸留による揮発性化合物の定量濃縮方法及びシステム - Google Patents
細管蒸留による揮発性化合物の定量濃縮方法及びシステムInfo
- Publication number
- JPH08901A JPH08901A JP7178068A JP17806895A JPH08901A JP H08901 A JPH08901 A JP H08901A JP 7178068 A JP7178068 A JP 7178068A JP 17806895 A JP17806895 A JP 17806895A JP H08901 A JPH08901 A JP H08901A
- Authority
- JP
- Japan
- Prior art keywords
- capillary
- filter plate
- distillation
- capillaries
- inner diameter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 32
- 238000004821 distillation Methods 0.000 title claims abstract description 29
- 150000001875 compounds Chemical class 0.000 title description 10
- 238000000926 separation method Methods 0.000 claims abstract description 23
- 239000000126 substance Substances 0.000 claims abstract description 20
- 238000009835 boiling Methods 0.000 claims abstract description 17
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 claims description 42
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 238000001704 evaporation Methods 0.000 claims description 21
- 230000008020 evaporation Effects 0.000 claims description 21
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 17
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 14
- 239000003039 volatile agent Substances 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 12
- 239000005350 fused silica glass Substances 0.000 claims description 11
- 150000002500 ions Chemical class 0.000 claims description 11
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 10
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims description 9
- 239000004696 Poly ether ether ketone Substances 0.000 claims description 8
- 229920002530 polyetherether ketone Polymers 0.000 claims description 8
- 239000002689 soil Substances 0.000 claims description 8
- 239000010842 industrial wastewater Substances 0.000 claims description 7
- 239000011148 porous material Substances 0.000 claims description 7
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 5
- 238000012546 transfer Methods 0.000 claims description 5
- 239000004809 Teflon Substances 0.000 claims description 4
- 229920006362 Teflon® Polymers 0.000 claims description 4
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 4
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 claims description 4
- 239000000725 suspension Substances 0.000 claims description 4
- 229920002994 synthetic fiber Polymers 0.000 claims description 4
- 229910021486 amorphous silicon dioxide Inorganic materials 0.000 claims description 3
- 239000004927 clay Substances 0.000 claims description 3
- 229910052570 clay Inorganic materials 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 229910052573 porcelain Inorganic materials 0.000 claims description 3
- 239000010453 quartz Substances 0.000 claims description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims description 3
- 239000010802 sludge Substances 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 2
- 229930195733 hydrocarbon Natural products 0.000 claims description 2
- 150000002430 hydrocarbons Chemical class 0.000 claims description 2
- 229910000510 noble metal Inorganic materials 0.000 claims 2
- 230000003247 decreasing effect Effects 0.000 claims 1
- 239000000243 solution Substances 0.000 description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 13
- 239000005388 borosilicate glass Substances 0.000 description 9
- 238000009833 condensation Methods 0.000 description 9
- 230000005494 condensation Effects 0.000 description 9
- 238000004458 analytical method Methods 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- -1 polyfluoroethylene Polymers 0.000 description 5
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 4
- 230000002745 absorbent Effects 0.000 description 4
- 239000002250 absorbent Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000004575 stone Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- ZMZDMBWJUHKJPS-UHFFFAOYSA-M Thiocyanate anion Chemical compound [S-]C#N ZMZDMBWJUHKJPS-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000004817 gas chromatography Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 description 2
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical group CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 230000033558 biomineral tissue development Effects 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- IZUPBVBPLAPZRR-UHFFFAOYSA-N pentachlorophenol Chemical compound OC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl IZUPBVBPLAPZRR-UHFFFAOYSA-N 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 239000000276 potassium ferrocyanide Substances 0.000 description 2
- ZNNZYHKDIALBAK-UHFFFAOYSA-M potassium thiocyanate Chemical compound [K+].[S-]C#N ZNNZYHKDIALBAK-UHFFFAOYSA-M 0.000 description 2
- 229940116357 potassium thiocyanate Drugs 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000012086 standard solution Substances 0.000 description 2
- XOGGUFAVLNCTRS-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide Chemical compound [K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] XOGGUFAVLNCTRS-UHFFFAOYSA-N 0.000 description 2
- GWHJZXXIDMPWGX-UHFFFAOYSA-N 1,2,4-trimethylbenzene Chemical compound CC1=CC=C(C)C(C)=C1 GWHJZXXIDMPWGX-UHFFFAOYSA-N 0.000 description 1
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- VMJNTFXCTXAXTC-UHFFFAOYSA-N 2,2-difluoro-1,3-benzodioxole-5-carbonitrile Chemical group C1=C(C#N)C=C2OC(F)(F)OC2=C1 VMJNTFXCTXAXTC-UHFFFAOYSA-N 0.000 description 1
- RDHSHXFBLXCDPE-UHFFFAOYSA-N P(=O)(O)(O)P(=O)(O)O.[PH2](=O)O Chemical compound P(=O)(O)(O)P(=O)(O)O.[PH2](=O)O RDHSHXFBLXCDPE-UHFFFAOYSA-N 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000005349 anion exchange Methods 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- KFUSEUYYWQURPO-UPHRSURJSA-N cis-1,2-dichloroethene Chemical group Cl\C=C/Cl KFUSEUYYWQURPO-UPHRSURJSA-N 0.000 description 1
- 239000007979 citrate buffer Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000004255 ion exchange chromatography Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 229940078552 o-xylene Drugs 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229910052979 sodium sulfide Inorganic materials 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/12—Molecular distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/15—Special material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/28—Porous member
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/906—Wick
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4421627.0 | 1994-06-21 | ||
| DE4421627A DE4421627C1 (de) | 1994-06-21 | 1994-06-21 | Verfahren und Vorrichtung zur quantitativen Anreicherung von flüchtigen Verbindungen durch Kapillar-Destillation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH08901A true JPH08901A (ja) | 1996-01-09 |
Family
ID=6521100
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7178068A Pending JPH08901A (ja) | 1994-06-21 | 1995-06-20 | 細管蒸留による揮発性化合物の定量濃縮方法及びシステム |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5665208A (de) |
| EP (1) | EP0688587B1 (de) |
| JP (1) | JPH08901A (de) |
| AT (1) | ATE186469T1 (de) |
| DE (2) | DE4421627C1 (de) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6004433A (en) * | 1997-02-03 | 1999-12-21 | L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes George Claude | Purification of electronic specialty gases by vapor phase transfilling |
| US5910233A (en) * | 1997-08-08 | 1999-06-08 | Berg; Gary | Method of and device for producing mineralized drinking water |
| US6159345A (en) * | 1998-11-06 | 2000-12-12 | Mitsubishi Chemical America, Inc. | Method and apparatus for recovering and/or recycling solvents |
| DE10107498A1 (de) * | 2001-02-15 | 2002-09-05 | Schott Jenaer Glas Gmbh | Ein Gefäß zum Erhitzen von Flüssigkeiten ohne Siedeverzug |
| CA2552680C (en) * | 2004-01-12 | 2009-07-21 | George E. Wilson | Desalinization by evaporation from capillary material |
| RU2337743C2 (ru) * | 2006-08-14 | 2008-11-10 | Павел Алексеевич Кучер | Способ перегонки жидкостей |
| RU2362606C2 (ru) * | 2006-10-30 | 2009-07-27 | Павел Алексеевич Кучер | Способ поверхностной перегонки жидкостей |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE558462C (de) * | 1930-04-18 | 1932-09-08 | Johann Karl Wirth Dipl Ing | Verfahren zum stossfreien Erhitzen von klaren und schlammigen Fluessigkeiten |
| DE568667C (de) * | 1930-09-14 | 1933-01-21 | Johann Karl Wirth Dipl Ing | Verfahren zum Erhitzen von Fluessigkeiten |
| GB612592A (en) * | 1946-05-29 | 1948-11-15 | Shaun Maturin Cox | Improvements in and relating to boiling vessels |
| US3151061A (en) * | 1961-11-13 | 1964-09-29 | Phillips Petroleum Co | Monitor for control of liquid foaming |
| SU422427A1 (ru) * | 1971-07-19 | 1974-04-05 | Термический деаэратор | |
| US4118285A (en) * | 1975-04-29 | 1978-10-03 | Villanova University | Separation of liquid mixtures |
| SU547390A1 (ru) * | 1975-09-02 | 1977-02-25 | Предприятие П/Я А-3513 | Термический деаэратор |
| US4040975A (en) * | 1976-02-03 | 1977-08-09 | Goldwell Gmbh Chemische Fabrik H.E. Dotter | Foam generator for foaming liquids |
| SU640976A2 (ru) * | 1977-04-25 | 1979-01-05 | Ульяновский политехнический институт | Вакуумный деаэратор |
| US4265700A (en) * | 1977-09-09 | 1981-05-05 | Uddeholms Aktiebolag Ab | Method of separating a solid and a liquid phase of a mass |
| JPS5596892A (en) * | 1979-01-18 | 1980-07-23 | Hisaka Works Ltd | Heat transfer plate for plate type evaporator |
| JPS57187555A (en) * | 1981-05-13 | 1982-11-18 | Matsushita Electric Ind Co Ltd | Solar heat collector |
| JPS59161609A (ja) * | 1983-03-03 | 1984-09-12 | Mitsubishi Electric Corp | 液体燃料気化装置 |
| SU1321685A1 (ru) * | 1986-02-11 | 1987-07-07 | Куйбышевский политехнический институт им.В.В.Куйбышева | Вакуумный деаэратор |
| SU1330405A1 (ru) * | 1986-03-05 | 1987-08-15 | Уральский филиал Всесоюзного теплотехнического научно-исследовательского института им.Ф.Э.Дзержинского | Деаэрационна колонка |
| DE3616309A1 (de) * | 1986-05-15 | 1987-11-19 | Degussa | Multiextraktion von fluechtigen verbindungen aus gasphasen |
| SU1402762A1 (ru) * | 1986-11-24 | 1988-06-15 | Одесский Политехнический Институт | Деаэратор |
| JP2708454B2 (ja) * | 1988-03-25 | 1998-02-04 | 実男 稲垣 | 蒸発散式排水処理装置 |
| JP2925576B2 (ja) * | 1989-04-26 | 1999-07-28 | 日本石英硝子株式会社 | 突沸防止法および突沸防止ガラス容器 |
| RU2001590C1 (ru) * | 1992-09-01 | 1993-10-30 | Всероссийский научно-исследовательский институт консервной и овощесушильной промышленности | Аппарат дл упаривани жидких продуктов |
-
1994
- 1994-06-21 DE DE4421627A patent/DE4421627C1/de not_active Expired - Fee Related
-
1995
- 1995-06-13 AT AT95109083T patent/ATE186469T1/de not_active IP Right Cessation
- 1995-06-13 DE DE59507206T patent/DE59507206D1/de not_active Expired - Fee Related
- 1995-06-13 EP EP95109083A patent/EP0688587B1/de not_active Expired - Lifetime
- 1995-06-20 JP JP7178068A patent/JPH08901A/ja active Pending
- 1995-06-21 US US08/493,083 patent/US5665208A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0688587B1 (de) | 1999-11-10 |
| DE59507206D1 (de) | 1999-12-16 |
| EP0688587A2 (de) | 1995-12-27 |
| EP0688587A3 (de) | 1996-04-10 |
| ATE186469T1 (de) | 1999-11-15 |
| US5665208A (en) | 1997-09-09 |
| DE4421627C1 (de) | 1996-02-22 |
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