JPH09104887A - 微細沈殿物の少ない高ｔｂｎフェネートステアレートの製造方法 - Google Patents

微細沈殿物の少ない高ｔｂｎフェネートステアレートの製造方法

Info

Publication number: JPH09104887A
Authority: JP; Japan
Prior art keywords: overbased; stearate; phenate; water; ratio
Prior art date: 1995-08-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

JP26011096A

Other languages

English (en)

Japanese (ja)

Inventor

Curtis B Campbell

ビー．キャンベルカーチス

Christopher S Fridia

エス．フリディアクリストファー

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Chevron Phillips Chemical Co LP

Original Assignee

Chevron Chemical Co LLC

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1995-08-23

Filing date

1996-08-23

Publication date

1997-04-22

1996-08-23 Application filed by Chevron Chemical Co LLC filed Critical Chevron Chemical Co LLC

1997-04-22 Publication of JPH09104887A publication Critical patent/JPH09104887A/ja

Status Abandoned legal-status Critical Current

Links

239000002244 precipitate Substances 0.000 title claims abstract description 36
238000004519 manufacturing process Methods 0.000 title claims abstract description 11
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 93
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 28
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 26
238000000034 method Methods 0.000 claims abstract description 25
150000005846 sugar alcohols Polymers 0.000 claims abstract description 18
239000000203 mixture Substances 0.000 claims abstract description 14
239000001569 carbon dioxide Substances 0.000 claims abstract description 13
229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 13
125000000217 alkyl group Chemical group 0.000 claims abstract description 11
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 11
239000000920 calcium hydroxide Substances 0.000 claims abstract description 11
229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 11
239000007787 solid Substances 0.000 claims abstract description 9
239000002904 solvent Substances 0.000 claims abstract description 6
238000003756 stirring Methods 0.000 claims abstract description 6
CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims abstract description 5
239000008116 calcium stearate Substances 0.000 claims abstract description 5
235000013539 calcium stearate Nutrition 0.000 claims abstract description 5
229910052751 metal Inorganic materials 0.000 claims abstract description 4
239000002184 metal Substances 0.000 claims abstract description 4
125000004432 carbon atom Chemical group C* 0.000 claims description 4
VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical class CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims 1
238000013019 agitation Methods 0.000 abstract description 12
235000021355 Stearic acid Nutrition 0.000 abstract description 6
MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 abstract description 6
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 abstract description 6
239000008117 stearic acid Substances 0.000 abstract description 6
-1 calcium stearate Chemical compound 0.000 abstract description 4
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 abstract 1
150000003839 salts Chemical class 0.000 abstract 1
238000006243 chemical reaction Methods 0.000 description 12
239000007788 liquid Substances 0.000 description 11
230000015572 biosynthetic process Effects 0.000 description 9
239000007789 gas Substances 0.000 description 6
238000002156 mixing Methods 0.000 description 6
229910052717 sulfur Inorganic materials 0.000 description 4
239000011575 calcium Substances 0.000 description 3
239000006185 dispersion Substances 0.000 description 3
239000000047 product Substances 0.000 description 3
238000003860 storage Methods 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
238000007792 addition Methods 0.000 description 2
238000010533 azeotropic distillation Methods 0.000 description 2
150000001735 carboxylic acids Chemical class 0.000 description 2
239000003085 diluting agent Substances 0.000 description 2
238000004821 distillation Methods 0.000 description 2
238000006386 neutralization reaction Methods 0.000 description 2
239000003921 oil Substances 0.000 description 2
239000013049 sediment Substances 0.000 description 2
239000011593 sulfur Substances 0.000 description 2
238000010998 test method Methods 0.000 description 2
238000012546 transfer Methods 0.000 description 2
LYCAIKOWRPUZTN-NMQOAUCRSA-N 1,2-dideuteriooxyethane Chemical compound [2H]OCCO[2H] LYCAIKOWRPUZTN-NMQOAUCRSA-N 0.000 description 1
NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
CYEJMVLDXAUOPN-UHFFFAOYSA-N 2-dodecylphenol Chemical compound CCCCCCCCCCCCC1=CC=CC=C1O CYEJMVLDXAUOPN-UHFFFAOYSA-N 0.000 description 1
240000007124 Brassica oleracea Species 0.000 description 1
235000003899 Brassica oleracea var acephala Nutrition 0.000 description 1
235000012905 Brassica oleracea var viridis Nutrition 0.000 description 1
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
239000002253 acid Substances 0.000 description 1
150000008064 anhydrides Chemical class 0.000 description 1
LLSDKQJKOVVTOJ-UHFFFAOYSA-L calcium chloride dihydrate Chemical compound O.O.[Cl-].[Cl-].[Ca+2] LLSDKQJKOVVTOJ-UHFFFAOYSA-L 0.000 description 1
229940052299 calcium chloride dihydrate Drugs 0.000 description 1
230000007423 decrease Effects 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
238000011049 filling Methods 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
239000010687 lubricating oil Substances 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
238000010926 purge Methods 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
238000011160 research Methods 0.000 description 1
238000007655 standard test method Methods 0.000 description 1
238000006467 substitution reaction Methods 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
239000008096 xylene Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
- C10M159/12—Reaction products
- C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
- C10M159/22—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products containing phenol radicals

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
General Chemical & Material Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Lubricants (AREA)

JP26011096A 1995-08-23 1996-08-23 微細沈殿物の少ない高ｔｂｎフェネートステアレートの製造方法 Abandoned JPH09104887A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US271695P	1995-08-23	1995-08-23
US002716		1995-08-23

Publications (1)

Publication Number	Publication Date
JPH09104887A true JPH09104887A (ja)	1997-04-22

Family

ID=21702133

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP26011096A Abandoned JPH09104887A (ja)	1995-08-23	1996-08-23	微細沈殿物の少ない高ｔｂｎフェネートステアレートの製造方法

Country Status (4)

Country	Link
EP (1)	EP0761648B1 (fr)
JP (1)	JPH09104887A (fr)
CA (1)	CA2183906A1 (fr)
DE (1)	DE69603055T2 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP1710294B1 (fr)	2005-04-06	2013-03-06	Infineum International Limited	Une méthode pour améliorer la stabilité ou la compatibilité des tensioactifs

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1105217A (en) *	1965-10-05	1968-03-06	Lubrizol Corp	Process for preparing basic metal phenates
GB8628609D0 (en) *	1986-11-29	1987-01-07	Bp Chemicals Additives	Lubricating oil additives
GB8917094D0 (en) *	1989-07-26	1989-09-13	Bp Chemicals Additives	Chemical process
JPH04183792A (ja) *	1990-11-19	1992-06-30	Idemitsu Kosan Co Ltd	過塩基性硫化アルカリ土類金属フェネート及びその用途
US5292968A (en) *	1992-02-26	1994-03-08	Cosmo Research Institute	Process for producing over-based alkaline earth metal phenate
DE69327515T2 (de) *	1992-12-07	2000-06-21	Ethyl Petroleum Additives, Inc.	Verfahren zur Herstellung von überbasischen Phenolaten
TW277057B (fr) *	1993-08-25	1996-06-01	Cosmo Sogo Kenkyusho Kk

1996
- 1996-08-22 CA CA 2183906 patent/CA2183906A1/fr not_active Abandoned
- 1996-08-23 EP EP19960306180 patent/EP0761648B1/fr not_active Expired - Lifetime
- 1996-08-23 JP JP26011096A patent/JPH09104887A/ja not_active Abandoned
- 1996-08-23 DE DE1996603055 patent/DE69603055T2/de not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CA2183906A1 (fr)	1997-02-24
DE69603055D1 (de)	1999-08-05
EP0761648B1 (fr)	1999-06-30
EP0761648A3 (fr)	1997-03-26
DE69603055T2 (de)	1999-10-21
EP0761648A2 (fr)	1997-03-12

Legal Events

Date

Code

Title

Description

2003-12-22

A762

Written abandonment of application

Free format text: JAPANESE INTERMEDIATE CODE: A762

Effective date: 20031219

Publication	Publication Date	Title
US3318809A (en)	1967-05-09	Counter current carbonation process
JP4073046B2 (ja)	2008-04-09	残留燃料油のための過塩基化マグネシウム析出物抑制添加剤
JP3819431B2 (ja)	2006-09-06	原油の腐食性及び酸性度の低下方法
WO1992020694A1 (fr)	1992-11-26	Preparation de sulfonates de magnesium surbasiques
CA1259602A (fr)	1989-09-19	Additifs avec exces basique
CN1030996C (zh)	1996-02-14	含改进的酚盐产品的润滑油组合物
JP2008513551A (ja)	2008-05-01	高全酸価（ｔａｎ）原油のエマルジョンの中和
JPS62292892A (ja)	1987-12-19	塩基性塩の製法
JPH09104887A (ja)	1997-04-22	微細沈殿物の少ない高ｔｂｎフェネートステアレートの製造方法
EP0473200B1 (fr)	1996-06-12	Procédé pour la préparation de sulfonates, phénolates et/ou salicylates suralcalinisés des métaux alcalins et alcalino-terreuses par carbonatation, les produits obtenus et leur utilisation
US5728657A (en)	1998-03-17	Production of low fine sediment high TBN phenate stearate
US4749499A (en)	1988-06-07	Method for preparing very fluid overbased additives having a high basicity and composition containing the additives
US5446202A (en)	1995-08-29	Over-based sulfurized alkaline earth metal phenate and process for producing the same
US3262880A (en)	1966-07-26	Processing carbonate dispersions in oils
US1963918A (en)	1934-06-19	Pour point depressor
CA1224803A (fr)	1987-07-28	Procede a une etape pour la preparation de graisses a exces de base de sulfonates de calcium, ainsi que de compositions epaissies
US4929373A (en)	1990-05-29	Process for preparing overbased calcium sulfonates
JPS61162594A (ja)	1986-07-23	潤滑油添加剤の品質改善のためのビニル付加共重合体の利用
CA1205819A (fr)	1986-06-10	Preparation de sulfonate de calcium surbase
JPH05171170A (ja)	1993-07-09	過塩基性化スルホン酸カルシウムの製法
US3083161A (en)	1963-03-26	Method of forming metal complexcontaining concentrates
RU2046793C1 (ru)	1995-10-27	Стабильный раствор пероксида циклогексанона, не кристаллизующийся до температуры минус 20°с и способ его получения
US4557840A (en)	1985-12-10	Continuous process for overbasing petroleum sulfonate in a pipe reactor with multiple entry of countercurrent carbon dioxide
US5861523A (en)	1999-01-19	Metal carboxylates
US4028259A (en)	1977-06-07	Process for preparing a metal salt of an oxidized, phosphosulfurized hydrocarbon and lubricant compositions containing same