JPS5540921A - Method and unit for hydrogen analysis in metal - Google Patents

Method and unit for hydrogen analysis in metal

Info

Publication number
JPS5540921A
JPS5540921A JP11368878A JP11368878A JPS5540921A JP S5540921 A JPS5540921 A JP S5540921A JP 11368878 A JP11368878 A JP 11368878A JP 11368878 A JP11368878 A JP 11368878A JP S5540921 A JPS5540921 A JP S5540921A
Authority
JP
Japan
Prior art keywords
test piece
hydrogen
vessel
heating
test
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11368878A
Other languages
Japanese (ja)
Inventor
Ryoichi Suzuki
Kenichi Takimoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP11368878A priority Critical patent/JPS5540921A/en
Publication of JPS5540921A publication Critical patent/JPS5540921A/en
Pending legal-status Critical Current

Links

Landscapes

  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Investigating And Analyzing Materials By Characteristic Methods (AREA)

Abstract

PURPOSE: To increase the accuracy of quantitative analysis by decreasing the value for blank test, by introducing test piece to the extraction vessel degased with high temperature heating and heating the test piece only at a high temperature.
CONSTITUTION: The extraction vessel 4 of quartz exhausted with the ion pump 9 is heated at about 1000°C before the introduction of test piece with the electric furnace 6-1, to discharge the absorbed gas of the vessel itself. After exhausting the test piece 1 in the pre-exhaust chamber 2, it is placed on the quartz made holding stand in the vessel 4 through the gate valve 3, and the electric furnace 6-1 is selected to the spot heater 6-2 such as infrared ray heating furnace or laser light. With the heater 6-2 controlled with the thermocouple 5 and the temperature control unit 7, only the test piece 1 is heated to a high temperature without heating the external wall of the vessel 4 to discharge hydrogen, which is entered to the hydrogen analysis meter 11 through the needle valve 10. Further, the signal from the analysis meter 11 and the unit 7 enters the recorder 14 to display the amount of hydrogen and temperature. Since the test value for blank test is decreased with this two stage heating system, the accuracy of quantitative analysis for fine amount of hydrogen can especially be increased.
COPYRIGHT: (C)1980,JPO&Japio
JP11368878A 1978-09-18 1978-09-18 Method and unit for hydrogen analysis in metal Pending JPS5540921A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11368878A JPS5540921A (en) 1978-09-18 1978-09-18 Method and unit for hydrogen analysis in metal

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11368878A JPS5540921A (en) 1978-09-18 1978-09-18 Method and unit for hydrogen analysis in metal

Publications (1)

Publication Number Publication Date
JPS5540921A true JPS5540921A (en) 1980-03-22

Family

ID=14618654

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11368878A Pending JPS5540921A (en) 1978-09-18 1978-09-18 Method and unit for hydrogen analysis in metal

Country Status (1)

Country Link
JP (1) JPS5540921A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0367168A (en) * 1989-08-04 1991-03-22 Nippon Steel Corp Analysis of trace carbon, sulfur, phosphorus in metallic sample and equipment therefor
JP2009168661A (en) * 2008-01-17 2009-07-30 R-Dec Co Ltd Hydrogen amount measuring device
WO2019225573A1 (en) * 2018-05-25 2019-11-28 株式会社堀場製作所 Element analysis device and element analysis method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0367168A (en) * 1989-08-04 1991-03-22 Nippon Steel Corp Analysis of trace carbon, sulfur, phosphorus in metallic sample and equipment therefor
JP2009168661A (en) * 2008-01-17 2009-07-30 R-Dec Co Ltd Hydrogen amount measuring device
WO2019225573A1 (en) * 2018-05-25 2019-11-28 株式会社堀場製作所 Element analysis device and element analysis method
JPWO2019225573A1 (en) * 2018-05-25 2021-06-17 株式会社堀場製作所 Elemental analyzer and elemental analysis method

Similar Documents

Publication Publication Date Title
JPS5540921A (en) Method and unit for hydrogen analysis in metal
US3148032A (en) Apparatus for hydrogen analysis
DE69820162T2 (en) Leakage control of radiation pipes in industrial furnaces
da Silva et al. A simple digestion procedure for the determination of cadmium, copper, molybdenium and vanadium in plants by graphite furnace atomic absorption spectrometry and mass inductively coupled plasma spectrometry.
MacDougall et al. Determination of oxygen in refractory oxides
JPS53149392A (en) Specimen injector of gas chromatograph
GB1213900A (en) Method of treating the internal surface of glass capillaries
Littlejohn et al. Determination of the rate of hydrolysis of ytterbium sulphide films by carbon furance atomic-emission spectrometry
JPS5790142A (en) Protecting method for measuring instrument in microwave heater
Pen'kov Investigation of boron ignition and combustion by means of fast cinespectrography
JPS55112566A (en) Hydrogen quantity measuring method in metal
JPS5649960A (en) Measuring method for volatile organic solvent in water solution
JPS5262087A (en) Reference concentration gas generating device
JPS5451587A (en) Sample atom making apparatus
FR2344838A1 (en) Chromatographic appts. with directly heated column - comprises metallic tube with very thin walls enclosing electrical heater
JPS5610252A (en) Method for determining sulfur in metal
Iseler et al. A model for rapid synthesis of large volume InP melts
JPS5597416A (en) Drying of pig iron receiving container and preheating before receiving pig iron
O'hira et al. Mass spectrometric determination of lioh and Li2CO3 in Li2O
SU426333A1 (en)
JPS55103451A (en) Sample atomization device
Maxted et al. CCCCLIX.—Studies in gaseous adsorption. Part II. The heat of adsorption curve for hydrogen on platinum
JPS57139653A (en) Method for detecting dissolved, easily vaporizing organic gas
GB1507442A (en) Apparatus comprising a furnace and a device for accommodating receptacles
GB931605A (en) A method and apparatus for determining the gaseous content of metals