JPS557252A - Preparatio of iminodiacetic acid - Google Patents
Preparatio of iminodiacetic acidInfo
- Publication number
- JPS557252A JPS557252A JP8066278A JP8066278A JPS557252A JP S557252 A JPS557252 A JP S557252A JP 8066278 A JP8066278 A JP 8066278A JP 8066278 A JP8066278 A JP 8066278A JP S557252 A JPS557252 A JP S557252A
- Authority
- JP
- Japan
- Prior art keywords
- iminodiacetic acid
- hcho
- kcn
- acid
- preparatio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical compound OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 title abstract 3
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 abstract 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 2
- 229960002449 glycine Drugs 0.000 abstract 2
- 235000013905 glycine and its sodium salt Nutrition 0.000 abstract 2
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 239000013522 chelant Substances 0.000 abstract 1
- 229940079593 drug Drugs 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- NNFCIKHAZHQZJG-UHFFFAOYSA-N potassium cyanide Chemical compound [K+].N#[C-] NNFCIKHAZHQZJG-UHFFFAOYSA-N 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- MNWBNISUBARLIT-UHFFFAOYSA-N sodium cyanide Chemical compound [Na+].N#[C-] MNWBNISUBARLIT-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare iminodiacetic acid usable for various purposes, e.g. chelate group introducing bases, raw materials for medicines or pesticides, selectively on an industrial scale, by reacting easily available aminoacetic acid with NaCN or KCN and HCHO.
CONSTITUTION: One mole of aminoacetic acid is reacted with 0.9W1.1 moles each of NaCH or KCN and HCHO at a pH of 9W10 and a temperature of 0W50°C for 10 minW2 hr to give an N-cyanomethyl derivative, which is hydrolyzed with an alkali hydroxide at 90W95°C to form iminodiacetic acid in high yield.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8066278A JPS557252A (en) | 1978-07-03 | 1978-07-03 | Preparatio of iminodiacetic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8066278A JPS557252A (en) | 1978-07-03 | 1978-07-03 | Preparatio of iminodiacetic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS557252A true JPS557252A (en) | 1980-01-19 |
Family
ID=13724566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8066278A Pending JPS557252A (en) | 1978-07-03 | 1978-07-03 | Preparatio of iminodiacetic acid |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS557252A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE31463E (en) * | 1975-03-03 | 1983-12-13 | Research Corporation | Radiopharmaceutical chelates and method of external imaging |
| WO2001087827A1 (en) * | 2000-05-15 | 2001-11-22 | Monsanto Technology Llc | Preparation of iminodiacetic acid compounds from monoethanolamine substrates |
| JP2012528832A (en) * | 2009-06-05 | 2012-11-15 | アクゾ ノーベル ケミカルズ インターナショナル ベスローテン フエンノートシャップ | Method for producing chelating agent or precursor thereof using cyanide salt |
| US9628015B2 (en) | 2007-09-14 | 2017-04-18 | The Powerwise Group, Inc. | Energy saving system and method for devices with rotating or reciprocating masses |
-
1978
- 1978-07-03 JP JP8066278A patent/JPS557252A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE31463E (en) * | 1975-03-03 | 1983-12-13 | Research Corporation | Radiopharmaceutical chelates and method of external imaging |
| WO2001087827A1 (en) * | 2000-05-15 | 2001-11-22 | Monsanto Technology Llc | Preparation of iminodiacetic acid compounds from monoethanolamine substrates |
| US6555706B2 (en) | 2000-05-15 | 2003-04-29 | Monsanto Company | Process for making iminodiacetic acid compounds from monoethanolamine substrates |
| US7064235B2 (en) | 2000-05-15 | 2006-06-20 | Monsanto Technology Llc | Process for making iminodiacetic acid compounds from monoethanolamine substrates |
| CN100354256C (en) * | 2000-05-15 | 2007-12-12 | 孟山都技术有限责任公司 | Preparation of iminodiacetic acid compounds from monoethanolamine substrates |
| US9628015B2 (en) | 2007-09-14 | 2017-04-18 | The Powerwise Group, Inc. | Energy saving system and method for devices with rotating or reciprocating masses |
| JP2012528832A (en) * | 2009-06-05 | 2012-11-15 | アクゾ ノーベル ケミカルズ インターナショナル ベスローテン フエンノートシャップ | Method for producing chelating agent or precursor thereof using cyanide salt |
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