JPS5590524A - Preparation of fast hardenable phenol resin - Google Patents
Preparation of fast hardenable phenol resinInfo
- Publication number
- JPS5590524A JPS5590524A JP16105978A JP16105978A JPS5590524A JP S5590524 A JPS5590524 A JP S5590524A JP 16105978 A JP16105978 A JP 16105978A JP 16105978 A JP16105978 A JP 16105978A JP S5590524 A JPS5590524 A JP S5590524A
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- effective
- fast
- phenol resin
- zinc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000005011 phenolic resin Substances 0.000 title abstract 2
- 239000003054 catalyst Substances 0.000 abstract 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 abstract 2
- 238000007259 addition reaction Methods 0.000 abstract 2
- 238000006482 condensation reaction Methods 0.000 abstract 2
- 150000002989 phenols Chemical class 0.000 abstract 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical group [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract 2
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical group [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 abstract 1
- ITHZDDVSAWDQPZ-UHFFFAOYSA-L barium acetate Chemical compound [Ba+2].CC([O-])=O.CC([O-])=O ITHZDDVSAWDQPZ-UHFFFAOYSA-L 0.000 abstract 1
- 229940071125 manganese acetate Drugs 0.000 abstract 1
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000004246 zinc acetate Substances 0.000 abstract 1
- 239000011592 zinc chloride Chemical group 0.000 abstract 1
- 235000005074 zinc chloride Nutrition 0.000 abstract 1
- 239000011787 zinc oxide Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G8/00—Condensation polymers of aldehydes or ketones with phenols only
- C08G8/04—Condensation polymers of aldehydes or ketones with phenols only of aldehydes
- C08G8/08—Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ
- C08G8/10—Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ with phenol
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Abstract
PURPOSE: To obtain a fast hardenable phenol resin safely, easily, in high yield as well as at low cost by a method wherein phenols and formaldehyde are reacted by using a catalyst effective for addition reaction and a catalyst effective for condensation reaction together.
CONSTITUTION: Phenols and formaldehyde are reacted in a range of mole ratio 0.6W0.95 by using a catalyst A effective for addition reaction selected from divalent metal salts and a catalyst B effective for condensation reaction together. A catalyst A to be used is selected from manganese acetate, zinc acetate, barium acetate or the like and a catalyst B is selected from zinc oxide, zinc nitrate, zinc chloride or the like. The ratio of both catalysts is 0.02W4 as a mole ratio of a catalyst A/a catalyst B and the total amount of both catalysts is preferably 0.1W3wt% of phenol.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP53161059A JPS5948049B2 (en) | 1978-12-28 | 1978-12-28 | Method for producing fast-curing phenolic resin |
| DE19803022326 DE3022326A1 (en) | 1978-12-28 | 1980-06-13 | Quick-setting phenol! resin prodn. - by reacting phenolic cpd. and formaldehyde in presence of mixed catalyst for catalysing addn. and condensn. reactions |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP53161059A JPS5948049B2 (en) | 1978-12-28 | 1978-12-28 | Method for producing fast-curing phenolic resin |
| DE19803022326 DE3022326A1 (en) | 1978-12-28 | 1980-06-13 | Quick-setting phenol! resin prodn. - by reacting phenolic cpd. and formaldehyde in presence of mixed catalyst for catalysing addn. and condensn. reactions |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5590524A true JPS5590524A (en) | 1980-07-09 |
| JPS5948049B2 JPS5948049B2 (en) | 1984-11-24 |
Family
ID=25786004
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP53161059A Expired JPS5948049B2 (en) | 1978-12-28 | 1978-12-28 | Method for producing fast-curing phenolic resin |
Country Status (2)
| Country | Link |
|---|---|
| JP (1) | JPS5948049B2 (en) |
| DE (1) | DE3022326A1 (en) |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2475587A (en) * | 1945-02-27 | 1949-07-12 | Bakelite Corp | Phenolic resins |
| FR1115410A (en) * | 1953-06-16 | 1956-04-24 | Distillers Co Yeast Ltd | Preparation of phenolic resins |
| US4113700A (en) * | 1977-01-10 | 1978-09-12 | Monsanto Company | Process for preparing high ortho novolac resins |
| US4097463A (en) * | 1977-01-10 | 1978-06-27 | Monsanto Company | Process for preparing high ortho novolac resins |
| US4140845A (en) * | 1977-03-21 | 1979-02-20 | Cor Tech Research Ltd. | Control of procedures for formation of water-immiscible thermosetting phenol-formaldehyde resins |
-
1978
- 1978-12-28 JP JP53161059A patent/JPS5948049B2/en not_active Expired
-
1980
- 1980-06-13 DE DE19803022326 patent/DE3022326A1/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5948049B2 (en) | 1984-11-24 |
| DE3022326A1 (en) | 1981-12-24 |
| DE3022326C2 (en) | 1988-07-21 |
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