JPS5594325A - Preparation of vinylidene chloride - Google Patents
Preparation of vinylidene chlorideInfo
- Publication number
- JPS5594325A JPS5594325A JP100879A JP100879A JPS5594325A JP S5594325 A JPS5594325 A JP S5594325A JP 100879 A JP100879 A JP 100879A JP 100879 A JP100879 A JP 100879A JP S5594325 A JPS5594325 A JP S5594325A
- Authority
- JP
- Japan
- Prior art keywords
- vinylidene chloride
- catalyst
- trichloroethane
- steam
- specific
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare vinylidene chloride in high yield, by dehydrochlorinating 1,1,2-trichloroethane in vapor phase at a specific temperature in the presence of a specific amount of steam and a specific catalyst.
CONSTITUTION: Vinylidene chloride is prepared in high yield and in remarkably high selectivity with exceedingly suppressed lowering of the catalyst activity, by the vapor-phase dehydrochlorination of 1,1,2-trichloroethane at 250W500°C, preferably at 300W450°C in the presence of 0.1W10mol, preferably of 0.5W5mol on the basis of 1mol of the raw material of steam, and a catalyst provided by impregnating a silica carrier with a halide of anelement selected from cesium, rubidium and potassium.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP100879A JPS5594325A (en) | 1979-01-11 | 1979-01-11 | Preparation of vinylidene chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP100879A JPS5594325A (en) | 1979-01-11 | 1979-01-11 | Preparation of vinylidene chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5594325A true JPS5594325A (en) | 1980-07-17 |
Family
ID=11489545
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP100879A Pending JPS5594325A (en) | 1979-01-11 | 1979-01-11 | Preparation of vinylidene chloride |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5594325A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02256630A (en) * | 1988-12-12 | 1990-10-17 | Tosoh Corp | Dehydrohalogenation process |
| CN106669757A (en) * | 2016-12-22 | 2017-05-17 | 江苏三美化工有限公司 | Method for preparing catalyst of vinylidene chloride by gas phase catalytic cracking |
-
1979
- 1979-01-11 JP JP100879A patent/JPS5594325A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02256630A (en) * | 1988-12-12 | 1990-10-17 | Tosoh Corp | Dehydrohalogenation process |
| CN106669757A (en) * | 2016-12-22 | 2017-05-17 | 江苏三美化工有限公司 | Method for preparing catalyst of vinylidene chloride by gas phase catalytic cracking |
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