JPS5835172B2 - アントラキノンルイノゴウセイホウ - Google Patents

アントラキノンルイノゴウセイホウ

Info

Publication number: JPS5835172B2
Authority: JP; Japan
Prior art keywords: activated clay; acetone; anthraquinone; yield; orthobenzoylbenzoic
Prior art date: 1974-01-10
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP624074A

Other languages

English (en)

Japanese (ja)

Other versions

JPS50100048A (mo

Inventor

修真鍋

誠司池上

恒亮平島

健一郎野田

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Yamamoto Chemicals Inc

Original Assignee

Yamamoto Chemicals Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1974-01-10

Filing date

1974-01-10

Publication date

1983-08-01

1974-01-10 Application filed by Yamamoto Chemicals Inc filed Critical Yamamoto Chemicals Inc

1974-01-10 Priority to JP624074A priority Critical patent/JPS5835172B2/ja

1975-08-08 Publication of JPS50100048A publication Critical patent/JPS50100048A/ja

1983-08-01 Publication of JPS5835172B2 publication Critical patent/JPS5835172B2/ja

Status Expired legal-status Critical Current

Links

150000004056 anthraquinones Chemical class 0.000 title claims description 11
PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 title description 4
239000004927 clay Substances 0.000 claims description 18
238000000034 method Methods 0.000 claims description 16
239000002253 acid Substances 0.000 claims description 5
150000007513 acids Chemical class 0.000 claims description 5
125000000217 alkyl group Chemical group 0.000 claims description 3
125000004432 carbon atom Chemical group C* 0.000 claims description 3
230000002194 synthesizing effect Effects 0.000 claims description 3
125000003277 amino group Chemical group 0.000 claims description 2
125000005843 halogen group Chemical group 0.000 claims description 2
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 30
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 20
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 16
239000005711 Benzoic acid Substances 0.000 description 10
235000010233 benzoic acid Nutrition 0.000 description 10
150000001875 compounds Chemical class 0.000 description 6
239000002994 raw material Substances 0.000 description 6
FGTYTUFKXYPTML-UHFFFAOYSA-N 2-benzoylbenzoic acid Chemical class OC(=O)C1=CC=CC=C1C(=O)C1=CC=CC=C1 FGTYTUFKXYPTML-UHFFFAOYSA-N 0.000 description 5
238000006243 chemical reaction Methods 0.000 description 5
238000007796 conventional method Methods 0.000 description 5
238000010438 heat treatment Methods 0.000 description 5
239000000203 mixture Substances 0.000 description 5
NJWGQARXZDRHCD-UHFFFAOYSA-N 2-methylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(C)=CC=C3C(=O)C2=C1 NJWGQARXZDRHCD-UHFFFAOYSA-N 0.000 description 4
238000004587 chromatography analysis Methods 0.000 description 4
239000007789 gas Substances 0.000 description 4
238000004519 manufacturing process Methods 0.000 description 4
238000002360 preparation method Methods 0.000 description 4
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
KHUFHLFHOQVFGB-UHFFFAOYSA-N 1-aminoanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2N KHUFHLFHOQVFGB-UHFFFAOYSA-N 0.000 description 2
WUKWGUZTPMOXOW-UHFFFAOYSA-N 2-(2-methylbutan-2-yl)anthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)(C)CC)=CC=C3C(=O)C2=C1 WUKWGUZTPMOXOW-UHFFFAOYSA-N 0.000 description 2
FPKCTSIVDAWGFA-UHFFFAOYSA-N 2-chloroanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(Cl)=CC=C3C(=O)C2=C1 FPKCTSIVDAWGFA-UHFFFAOYSA-N 0.000 description 2
SJEBAWHUJDUKQK-UHFFFAOYSA-N 2-ethylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(CC)=CC=C3C(=O)C2=C1 SJEBAWHUJDUKQK-UHFFFAOYSA-N 0.000 description 2
YTPSFXZMJKMUJE-UHFFFAOYSA-N 2-tert-butylanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)(C)C)=CC=C3C(=O)C2=C1 YTPSFXZMJKMUJE-UHFFFAOYSA-N 0.000 description 2
MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
238000009833 condensation Methods 0.000 description 2
230000005494 condensation Effects 0.000 description 2
230000018044 dehydration Effects 0.000 description 2
238000006297 dehydration reaction Methods 0.000 description 2
238000004817 gas chromatography Methods 0.000 description 2
-1 inglovil Chemical group 0.000 description 2
239000007788 liquid Substances 0.000 description 2
238000007363 ring formation reaction Methods 0.000 description 2
239000004576 sand Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
239000002699 waste material Substances 0.000 description 2
YWECCEXWKFHHQJ-UHFFFAOYSA-N 2-(4-chlorobenzoyl)benzoic acid Chemical compound OC(=O)C1=CC=CC=C1C(=O)C1=CC=C(Cl)C=C1 YWECCEXWKFHHQJ-UHFFFAOYSA-N 0.000 description 1
XOGPDSATLSAZEK-UHFFFAOYSA-N 2-Aminoanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(N)=CC=C3C(=O)C2=C1 XOGPDSATLSAZEK-UHFFFAOYSA-N 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000009835 boiling Methods 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000003247 decreasing effect Effects 0.000 description 1
YWEUIGNSBFLMFL-UHFFFAOYSA-N diphosphonate Chemical compound O=P(=O)OP(=O)=O YWEUIGNSBFLMFL-UHFFFAOYSA-N 0.000 description 1
238000004821 distillation Methods 0.000 description 1
230000007613 environmental effect Effects 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
238000000605 extraction Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000000479 mixture part Substances 0.000 description 1
125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
DLYUQMMRRRQYAE-UHFFFAOYSA-N phosphorus pentoxide Inorganic materials O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 1
229920000137 polyphosphoric acid Polymers 0.000 description 1
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
238000004445 quantitative analysis Methods 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
238000000859 sublimation Methods 0.000 description 1
230000008022 sublimation Effects 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP624074A 1974-01-10 1974-01-10 アントラキノンルイノゴウセイホウ Expired JPS5835172B2 (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP624074A JPS5835172B2 (ja)	1974-01-10	1974-01-10	アントラキノンルイノゴウセイホウ

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP624074A JPS5835172B2 (ja)	1974-01-10	1974-01-10	アントラキノンルイノゴウセイホウ

Publications (2)

Publication Number	Publication Date
JPS50100048A JPS50100048A (mo)	1975-08-08
JPS5835172B2 true JPS5835172B2 (ja)	1983-08-01

Family

ID=11632970

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP624074A Expired JPS5835172B2 (ja)	1974-01-10	1974-01-10	アントラキノンルイノゴウセイホウ

Country Status (1)

Country	Link
JP (1)	JPS5835172B2 (mo)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2545483B1 (fr) *	1983-05-03	1986-01-10	Ugine Kuhlmann	Procede de cyclisation de l'acide orthobenzoylbenzoique
FR2548662B2 (fr) *	1983-05-03	1986-02-28	Ugine Kuhlmann	Procede de separation de l'acide phtalique et de l'anhydride phtalique dans un procede de cyclisation d'acide orthobenzoylbenzoique

1974
- 1974-01-10 JP JP624074A patent/JPS5835172B2/ja not_active Expired

Also Published As

Publication number	Publication date
JPS50100048A (mo)	1975-08-08

Publication	Publication Date	Title
Holcombe et al.	1986	A new and specific method for the protection of phenols as the corresponding tert-butyl ethers
JP4209626B2 (ja)	2009-01-14	トリエチルアミンの回収方法
US2179809A (en)	1939-11-14	Condensation products
US2262262A (en)	1941-11-11	Process of making maleanils
JPS5835172B2 (ja)	1983-08-01	アントラキノンルイノゴウセイホウ
Bublitz et al.	1962	Comparison of Reactivities of Metallocenylphenylcarbinyl Azides in Acid-catalyzed Decomposition Reactions
US2214117A (en)	1940-09-10	Preparation of aromatic 1, 3-diketones
JP2001233870A (ja)	2001-08-28	３−（１−ヒドロキシ−ペンチリデン）−５−ニトロ−３ｈ−ベンゾフラン−２−オン、その製造方法及びその用途
Dime et al.	1981	Synthesis of isoquinolines from indenes
JPS5949207B2 (ja)	1984-12-01	ジエンの製造方法
Natelson et al.	1939	Study of the Reformatsky reaction; efficient procedure for the preparation of bromoacetic ester in large quantities
US4237322A (en)	1980-12-02	Process for preparation of 1,5-dimethylbicyclo[3,2,1]octan-8-ol
Collins	1948	The Synthesis of Phenanthrene-9-C14 (1, 2)
Hafez et al.	1961	Carbonyl and thiocarbonyl compounds. v. 1 synthesis of newer unsaturated nitriles, carboxylic acids, and esters derived from xanthene and thiaxanthene
US2421090A (en)	1947-05-27	Long chain aliphatic halides and method of preparing same
US3122588A (en)	1964-02-25	Process for the production of aldehydes
JPH01186844A (ja)	1989-07-26	３−（４’−ブロモビフェニル）−３−ヒドロキシ−４−フェニル酪酸エチルエステルの製造方法
US3968163A (en)	1976-07-06	Preparation of 4 and 5-methylindanes
US1887396A (en)	1932-11-08	Aromatic halogen-methyl compound and alpha process of preparing it
JP2890856B2 (ja)	1999-05-17	クアドラート酸の製造方法
US3504036A (en)	1970-03-31	Process for the production of cycloalkane-1,3-diones
KR870001042B1 (ko)	1987-05-26	분지상 알카노인산의 제조방법
KR960002601B1 (ko)	1996-02-23	류코트리엔 길항제 중간체의 제조방법
US2750402A (en)	1956-06-12	6, 7-diacetyl-1, 2, 3, 4, 4a, 9, 10, 10a-octahydro-1, 4a-dimethyl-9-oxophenanthrene-1-carbonitrile
US2619504A (en)	1952-11-25	Process of making 4(5)-p-menthen-3-one

JPS5835172B2 - アントラキノンルイノ ゴウセイホウ - Google Patents