JPS59207804A - 安定な亜臭素酸ナトリウム結晶の製造法 - Google Patents

安定な亜臭素酸ナトリウム結晶の製造法

Info

Publication number: JPS59207804A
Authority: JP; Japan
Prior art keywords: crystals; nabro2; concentration; sodium bromite; aqueous solution
Prior art date: 1983-05-12
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP8340083A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0422842B2 (it

Inventor

Toshio Shiozawa

塩沢　寿夫

Kihachiro Matsuda

松田　喜八郎

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

NIPPON SHIRIKA KOGYO KK

Original Assignee

NIPPON SHIRIKA KOGYO KK

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-05-12

Filing date

1983-05-12

Publication date

1984-11-26

1983-05-12 Application filed by NIPPON SHIRIKA KOGYO KK filed Critical NIPPON SHIRIKA KOGYO KK

1983-05-12 Priority to JP8340083A priority Critical patent/JPS59207804A/ja

1984-11-26 Publication of JPS59207804A publication Critical patent/JPS59207804A/ja

1985-11-12 Priority to US06/796,524 priority patent/US4650658A/en

1992-04-20 Publication of JPH0422842B2 publication Critical patent/JPH0422842B2/ja

Status Granted legal-status Critical Current

Links

239000013078 crystal Substances 0.000 title claims abstract description 106
NYCVSSWORUBFET-UHFFFAOYSA-M sodium;bromite Chemical compound [Na+].[O-]Br=O NYCVSSWORUBFET-UHFFFAOYSA-M 0.000 title claims abstract description 43
238000004519 manufacturing process Methods 0.000 title claims description 14
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 89
239000007864 aqueous solution Substances 0.000 claims abstract description 57
JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 claims abstract description 51
239000007788 liquid Substances 0.000 claims abstract description 40
150000003839 salts Chemical class 0.000 claims abstract description 25
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 12
238000003756 stirring Methods 0.000 claims abstract description 9
238000005119 centrifugation Methods 0.000 claims abstract description 8
238000001556 precipitation Methods 0.000 claims abstract description 7
XUXNAKZDHHEHPC-UHFFFAOYSA-M sodium bromate Chemical compound [Na+].[O-]Br(=O)=O XUXNAKZDHHEHPC-UHFFFAOYSA-M 0.000 claims abstract description 6
239000011780 sodium chloride Substances 0.000 claims abstract description 6
230000001376 precipitating effect Effects 0.000 claims abstract description 3
239000000243 solution Substances 0.000 claims description 32
238000000034 method Methods 0.000 claims description 31
238000001816 cooling Methods 0.000 claims description 18
238000000926 separation method Methods 0.000 claims description 16
239000002994 raw material Substances 0.000 claims description 14
239000011734 sodium Substances 0.000 claims description 14
239000007791 liquid phase Substances 0.000 claims description 8
238000009833 condensation Methods 0.000 claims description 5
230000005494 condensation Effects 0.000 claims description 5
238000005406 washing Methods 0.000 claims description 5
108091006629 SLC13A2 Proteins 0.000 claims description 4
238000012805 post-processing Methods 0.000 claims 1
239000012141 concentrate Substances 0.000 abstract description 15
238000003860 storage Methods 0.000 abstract description 12
238000010438 heat treatment Methods 0.000 abstract description 10
239000002244 precipitate Substances 0.000 abstract description 4
238000013019 agitation Methods 0.000 abstract 1
239000012670 alkaline solution Substances 0.000 abstract 1
238000002360 preparation method Methods 0.000 abstract 1
239000012452 mother liquor Substances 0.000 description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
238000006243 chemical reaction Methods 0.000 description 11
238000000354 decomposition reaction Methods 0.000 description 10
WTXXSZUATXIAJO-OWBHPGMISA-N (Z)-14-methylpentadec-2-enoic acid Chemical group CC(CCCCCCCCCC\C=C/C(=O)O)C WTXXSZUATXIAJO-OWBHPGMISA-N 0.000 description 6
DKSMCEUSSQTGBK-UHFFFAOYSA-M bromite Chemical compound [O-]Br=O DKSMCEUSSQTGBK-UHFFFAOYSA-M 0.000 description 6
238000002425 crystallisation Methods 0.000 description 6
230000008025 crystallization Effects 0.000 description 6
239000002002 slurry Substances 0.000 description 5
CHZVHNZRFPALHO-UHFFFAOYSA-N [Br].[Na] Chemical compound [Br].[Na] CHZVHNZRFPALHO-UHFFFAOYSA-N 0.000 description 4
239000007800 oxidant agent Substances 0.000 description 4
238000013112 stability test Methods 0.000 description 4
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical compound BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
239000000498 cooling water Substances 0.000 description 3
230000007423 decrease Effects 0.000 description 3
239000012535 impurity Substances 0.000 description 3
229920006395 saturated elastomer Polymers 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
CRWJEUDFKNYSBX-UHFFFAOYSA-N sodium;hypobromite Chemical compound [Na+].Br[O-] CRWJEUDFKNYSBX-UHFFFAOYSA-N 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
230000001133 acceleration Effects 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
239000012153 distilled water Substances 0.000 description 2
230000000694 effects Effects 0.000 description 2
239000012530 fluid Substances 0.000 description 2
229910001385 heavy metal Inorganic materials 0.000 description 2
239000008235 industrial water Substances 0.000 description 2
230000001590 oxidative effect Effects 0.000 description 2
239000002245 particle Substances 0.000 description 2
238000004321 preservation Methods 0.000 description 2
238000011084 recovery Methods 0.000 description 2
239000007787 solid Substances 0.000 description 2
230000006641 stabilisation Effects 0.000 description 2
238000011105 stabilization Methods 0.000 description 2
-1 that is Substances 0.000 description 2
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
241000251730 Chondrichthyes Species 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
241000219094 Vitaceae Species 0.000 description 1
208000000260 Warts Diseases 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000004480 active ingredient Substances 0.000 description 1
239000003513 alkali Substances 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
229910052794 bromium Inorganic materials 0.000 description 1
DKSMCEUSSQTGBK-UHFFFAOYSA-N bromous acid Chemical compound OBr=O DKSMCEUSSQTGBK-UHFFFAOYSA-N 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
239000003638 chemical reducing agent Substances 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
239000011651 chromium Substances 0.000 description 1
238000011437 continuous method Methods 0.000 description 1
230000008602 contraction Effects 0.000 description 1
230000006837 decompression Effects 0.000 description 1
238000007323 disproportionation reaction Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
239000000835 fiber Substances 0.000 description 1
235000021021 grapes Nutrition 0.000 description 1
239000008236 heating water Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000000203 mixture Substances 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
239000012071 phase Substances 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
235000019396 potassium bromate Nutrition 0.000 description 1
125000001453 quaternary ammonium group Chemical group 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
201000010153 skin papilloma Diseases 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
239000004753 textile Substances 0.000 description 1
230000002485 urinary effect Effects 0.000 description 1

Landscapes

Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

JP8340083A 1983-05-12 1983-05-12 安定な亜臭素酸ナトリウム結晶の製造法 Granted JPS59207804A (ja)

Priority Applications (2)

Application Number	Priority Date	Filing Date	Title
JP8340083A JPS59207804A (ja)	1983-05-12	1983-05-12	安定な亜臭素酸ナトリウム結晶の製造法
US06/796,524 US4650658A (en)	1983-05-12	1985-11-12	Stable crystals of sodium bromite trihydrate

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP8340083A JPS59207804A (ja)	1983-05-12	1983-05-12	安定な亜臭素酸ナトリウム結晶の製造法

Publications (2)

Publication Number	Publication Date
JPS59207804A true JPS59207804A (ja)	1984-11-26
JPH0422842B2 JPH0422842B2 (it)	1992-04-20

Family

ID=13801373

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP8340083A Granted JPS59207804A (ja)	1983-05-12	1983-05-12	安定な亜臭素酸ナトリウム結晶の製造法

Country Status (1)

Country	Link
JP (1)	JPS59207804A (it)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN102701155A (zh) *	2012-07-09	2012-10-03	山东天信化工有限公司	一种亚溴酸钠水溶液的制备方法

1983
- 1983-05-12 JP JP8340083A patent/JPS59207804A/ja active Granted

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN102701155A (zh) *	2012-07-09	2012-10-03	山东天信化工有限公司	一种亚溴酸钠水溶液的制备方法

Also Published As

Publication number	Publication date
JPH0422842B2 (it)	1992-04-20

Publication	Publication Date	Title
US4981664A (en)	1991-01-01	Method of production of high purity silica and ammonium fluoride
CN108862335A (zh)	2018-11-23	一种用磷酸锂制备碳酸锂的方法
RU2235065C2 (ru)	2004-08-27	Способ получения сульфата калия из поташа и сульфата натрия
CN105960444A (zh)	2016-09-21	从混合碱金属甲酸盐共混物收取甲酸铯的方法
JPH08508231A (ja)	1996-09-03	無水塩化マグネシウムの製造方法
EP0001537A1 (fr)	1979-04-18	Procédé de traitement de solutions contenant des carbonate, sulfate, éventuellement hydroxyde de sodium ou potassium, ainsi que l'un au moins des métaux vanadium, uranium, molybdène
US6692716B1 (en)	2004-02-17	Method of formulating alkali earth salts
US4650658A (en)	1987-03-17	Stable crystals of sodium bromite trihydrate
EP1121327A1 (en)	2001-08-08	Method of formulating alkali metal salts
JPH03204844A (ja)	1991-09-06	結晶廃液からグリシン及び芒硝の回収
JPH0422842B2 (it)	1992-04-20
JPH0696455B2 (ja)	1994-11-30	高純度硫酸コバルトの製造方法
JP7050353B2 (ja)	2022-04-08	２－アミノエチルスルホン酸の製造方法
JPH01313333A (ja)	1989-12-18	高純度水酸化ニオブまたは水酸化タンタルの製造方法
JPS6230123B2 (it)	1987-06-30
JPS60231647A (ja)	1985-11-18	パラフインのスルホ酸化で生じた反応混合物から残留硫酸を除く方法
US1354642A (en)	1920-10-05	Process for obtaining potassium chlorid
US2540648A (en)	1951-02-06	Process for recovering sodium bicarbonate and sodium borate from a complex brine
US3005685A (en)	1961-10-24	Process for desilicifying fluorspar and the like minerals
US1284380A (en)	1918-11-12	Art of preparing ammonium perchlorate.
US1300947A (en)	1919-04-15	Separation and recovery of potassium salts from commercial nitrate of soda containing such salts.
US970909A (en)	1910-09-20	Process of making ammonium chlorid.
US1883261A (en)	1932-10-18	Process of recovering glaserite
JPS586681B2 (ja)	1983-02-05	次亜塩素酸ナトリウム・５水和物の製造方法
US2309569A (en)	1943-01-26	Method of separating sodium salts

JPS59207804A - 安定な亜臭素酸ナトリウム結晶の製造法 - Google Patents

Info

Links

Landscapes

Priority Applications (2)

Applications Claiming Priority (1)

Publications (2)

Family

ID=13801373

Family Applications (1)

Country Status (1)

Cited By (1)

Cited By (1)

Also Published As

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