JPS59500714A - セラミツク材料の製造方法 - Google Patents

セラミツク材料の製造方法

Info

Publication number: JPS59500714A
Authority: JP; Japan
Prior art keywords: slurry; powder; sintering; titanium; alkoxide
Prior art date: 1983-04-04
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP58501619A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0333671B2 (2

Inventor

ヤン・マン・フエイ

Original Assignee

ウエスタ−ン　エレクトリツク　カムパニ−，インコ−ポレ−テツド

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-04-04

Filing date

1983-04-04

Publication date

1984-04-26

1983-04-04 Application filed by ウエスタ−ン　エレクトリツク　カムパニ−，インコ−ポレ−テツド filed Critical ウエスタ−ン　エレクトリツク　カムパニ−，インコ−ポレ−テツド

1983-04-04 Priority claimed from PCT/US1983/000457 external-priority patent/WO1983003823A1/en

1984-04-26 Publication of JPS59500714A publication Critical patent/JPS59500714A/ja

1991-05-17 Publication of JPH0333671B2 publication Critical patent/JPH0333671B2/ja

Status Granted legal-status Critical Current

Links

229910010293 ceramic material Inorganic materials 0.000 title claims description 16
238000004519 manufacturing process Methods 0.000 title claims description 10
239000000843 powder Substances 0.000 claims description 35
238000000034 method Methods 0.000 claims description 30
238000005245 sintering Methods 0.000 claims description 28
239000002002 slurry Substances 0.000 claims description 26
150000004703 alkoxides Chemical class 0.000 claims description 15
239000007788 liquid Substances 0.000 claims description 11
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 10
229910044991 metal oxide Inorganic materials 0.000 claims description 9
150000004706 metal oxides Chemical class 0.000 claims description 9
239000010936 titanium Chemical group 0.000 claims description 9
229910052719 titanium Chemical group 0.000 claims description 7
239000006185 dispersion Substances 0.000 claims description 6
238000000498 ball milling Methods 0.000 claims description 5
JMXKSZRRTHPKDL-UHFFFAOYSA-N titanium ethoxide Chemical group [Ti+4].CC[O-].CC[O-].CC[O-].CC[O-] JMXKSZRRTHPKDL-UHFFFAOYSA-N 0.000 claims description 5
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 4
YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims description 4
238000001354 calcination Methods 0.000 claims description 4
238000001035 drying Methods 0.000 claims description 3
239000006228 supernatant Substances 0.000 claims description 3
229910052758 niobium Inorganic materials 0.000 claims description 2
229910052715 tantalum Inorganic materials 0.000 claims description 2
238000007599 discharging Methods 0.000 claims 1
239000002245 particle Substances 0.000 description 29
VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 12
239000000243 solution Substances 0.000 description 10
239000000919 ceramic Substances 0.000 description 9
235000019441 ethanol Nutrition 0.000 description 9
238000006460 hydrolysis reaction Methods 0.000 description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
239000002019 doping agent Substances 0.000 description 7
230000007062 hydrolysis Effects 0.000 description 7
239000011148 porous material Substances 0.000 description 7
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
239000000463 material Substances 0.000 description 6
229910052751 metal Inorganic materials 0.000 description 6
239000002184 metal Substances 0.000 description 6
-1 phosphorous alkoxides Chemical class 0.000 description 6
238000004062 sedimentation Methods 0.000 description 5
238000005324 grain boundary diffusion Methods 0.000 description 4
239000007787 solid Substances 0.000 description 4
238000005054 agglomeration Methods 0.000 description 3
230000002776 aggregation Effects 0.000 description 3
238000005119 centrifugation Methods 0.000 description 3
239000003985 ceramic capacitor Substances 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
238000009826 distribution Methods 0.000 description 3
238000003801 milling Methods 0.000 description 3
239000000203 mixture Substances 0.000 description 3
239000000126 substance Substances 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
125000002091 cationic group Chemical group 0.000 description 2
239000007795 chemical reaction product Substances 0.000 description 2
238000000280 densification Methods 0.000 description 2
238000009792 diffusion process Methods 0.000 description 2
239000007772 electrode material Substances 0.000 description 2
238000001914 filtration Methods 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000008018 melting Effects 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
239000010955 niobium Substances 0.000 description 2
239000001301 oxygen Substances 0.000 description 2
229910052760 oxygen Inorganic materials 0.000 description 2
239000002244 precipitate Substances 0.000 description 2
OGHBATFHNDZKSO-UHFFFAOYSA-N propan-2-olate Chemical compound CC(C)[O-] OGHBATFHNDZKSO-UHFFFAOYSA-N 0.000 description 2
NGCRLFIYVFOUMZ-UHFFFAOYSA-N 2,3-dichloroquinoxaline-6-carbonyl chloride Chemical compound N1=C(Cl)C(Cl)=NC2=CC(C(=O)Cl)=CC=C21 NGCRLFIYVFOUMZ-UHFFFAOYSA-N 0.000 description 1
239000004743 Polypropylene Substances 0.000 description 1
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
241000981595 Zoysia japonica Species 0.000 description 1
239000002253 acid Substances 0.000 description 1
230000004913 activation Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
229910045601 alloy Inorganic materials 0.000 description 1
239000000956 alloy Substances 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
229910002113 barium titanate Inorganic materials 0.000 description 1
JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 1
239000008280 blood Substances 0.000 description 1
210000004369 blood Anatomy 0.000 description 1
HKCLKCUQYRJCED-UHFFFAOYSA-N butane titanium Chemical compound [Ti].CCCC HKCLKCUQYRJCED-UHFFFAOYSA-N 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000003990 capacitor Substances 0.000 description 1
238000010276 construction Methods 0.000 description 1
238000011109 contamination Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
230000003111 delayed effect Effects 0.000 description 1
230000002939 deleterious effect Effects 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
238000005538 encapsulation Methods 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
238000005189 flocculation Methods 0.000 description 1
230000016615 flocculation Effects 0.000 description 1
238000005469 granulation Methods 0.000 description 1
230000003179 granulation Effects 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
238000000462 isostatic pressing Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
ZTILUDNICMILKJ-UHFFFAOYSA-N niobium(v) ethoxide Chemical compound CCO[Nb](OCC)(OCC)(OCC)OCC ZTILUDNICMILKJ-UHFFFAOYSA-N 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
229910000510 noble metal Inorganic materials 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
229920001155 polypropylene Polymers 0.000 description 1
239000007774 positive electrode material Substances 0.000 description 1
239000010970 precious metal Substances 0.000 description 1
239000002243 precursor Substances 0.000 description 1
238000003672 processing method Methods 0.000 description 1
IKNCGYCHMGNBCP-UHFFFAOYSA-N propan-1-olate Chemical compound CCC[O-] IKNCGYCHMGNBCP-UHFFFAOYSA-N 0.000 description 1
239000012798 spherical particle Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
230000007723 transport mechanism Effects 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002023 wood Substances 0.000 description 1

Landscapes

Compositions Of Oxide Ceramics (AREA)
Compression Or Coding Systems Of Tv Signals (AREA)
Compression Of Band Width Or Redundancy In Fax (AREA)
Compression, Expansion, Code Conversion, And Decoders (AREA)
Image Processing (AREA)

JP58501619A 1983-04-04 1983-04-04 セラミツク材料の製造方法 Granted JPS59500714A (ja)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PCT/US1983/000457 WO1983003823A1 (en)	1982-05-03	1983-04-04	Method for fabricating ceramic materials

Publications (2)

Publication Number	Publication Date
JPS59500714A true JPS59500714A (ja)	1984-04-26
JPH0333671B2 JPH0333671B2 (2)	1991-05-17

Family

ID=22174946

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP58501619A Granted JPS59500714A (ja)	1983-04-04	1983-04-04	セラミツク材料の製造方法

Country Status (1)

Country	Link
JP (1)	JPS59500714A (2)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS63141657A (ja) *	1986-12-03	1988-06-14	日本セメント株式会社	セラミツクス用原料微粉末の製造方法
JPH02111658A (ja) *	1988-10-18	1990-04-24	Shinko Electric Ind Co Ltd	セラミック絶縁材料およびその製造方法

1983
- 1983-04-04 JP JP58501619A patent/JPS59500714A/ja active Granted

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS63141657A (ja) *	1986-12-03	1988-06-14	日本セメント株式会社	セラミツクス用原料微粉末の製造方法
JPH02111658A (ja) *	1988-10-18	1990-04-24	Shinko Electric Ind Co Ltd	セラミック絶縁材料およびその製造方法

Also Published As

Publication number	Publication date
JPH0333671B2 (2)	1991-05-17

Publication	Publication Date	Title
Pithan et al.	2005	Progress in the synthesis of nanocrystalline BaTiO3 powders for MLCC
Viswanath et al.	1997	Preparation and ferroelectric phase transition studies of nanocrystalline BaTiO3
NL194755C (nl)	2003-02-04	Werkwijze voor het bereiden van een perovskiet-verbindingen bevattende samenstelling.
US4800051A (en)	1989-01-24	Method for fabricating ceramic materials
Shimooka et al.	1995	Preparation of Dense BaTiO3 Ceramics from Sol‐Gel‐Derived Monolithic Gels
JPS63103827A (ja)	1988-05-09	チタン酸バリウムの製造方法
CN111465580A (zh)	2020-07-28	钙钛矿型钛酸钡粉末的制造方法
CN101098828A (zh)	2008-01-02	微粒锆钛酸铅、锆钛水合物和钛酸锆及其制备方法
Wang et al.	2017	Sintering of Nano-Ceramics
JPS63156054A (ja)	1988-06-29	多成分系セラミツクスの製造方法
JP2018190956A (ja)	2018-11-29	非強誘電性高誘電体及びその製造方法
JP5119008B2 (ja)	2013-01-16	ペロブスカイト型チタン酸バリウム粉末の製造方法
EP0107700B1 (en)	1991-08-14	Method for fabricating ceramic materials
JPS59500714A (ja)	1984-04-26	セラミツク材料の製造方法
Ali et al.	1993	Synthesis and Processing Characteristics of Ba0. 65Sr0. 35TiO3 Powders from Catecholate Precursors
JPH02226611A (ja)	1990-09-10	マイクロ波デバイスの製造方法
US6592805B1 (en)	2003-07-15	Method for producing sintered electroceramic materials from hydroxide and oxalate precursors
JPS63236713A (ja)	1988-10-03	ペロブスカイト型化合物の無機微粉体の製造方法
JPS5939725A (ja)	1984-03-05	厚膜用誘電体粉末の製造法
JPS5939724A (ja)	1984-03-05	厚膜用誘電体粉末の製造法
JPS63218514A (ja)	1988-09-12	ジルコニウムを含むペロブスカイトセラミツクス粉末の製造方法
JP3030359B1 (ja)	2000-04-10	ペロブスカイト型構造を有する鉛含有チタン酸複合酸化物高密度多結晶焼結体とその製造方法
JP2608558B2 (ja)	1997-05-07	光学セラミックスの製造方法
Nam et al.	1992	Fabrication and piezoelectric properties of PZT ceramics prepared by partial oxalate method
CN101027735A (zh)	2007-08-29	陶瓷电容器及其制造方法

JPS59500714A - セラミツク材料の製造方法 - Google Patents

Info

Links

Landscapes

Applications Claiming Priority (1)

Publications (2)

Family

ID=22174946

Family Applications (1)

Country Status (1)

Cited By (2)

Cited By (2)

Also Published As

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