JPS6072811A - 生活歯髄覆罩兼根管充填剤の製造方法 - Google Patents

生活歯髄覆罩兼根管充填剤の製造方法

Info

Publication number: JPS6072811A
Authority: JP; Japan
Prior art keywords: catalyst; polymer; added; vegetable oil; mixture
Prior art date: 1983-09-29
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP58181555A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6260362B2 (da

Inventor

Chuichi Takahashi

高橋　忠一

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Individual

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-09-29

Filing date

1983-09-29

Publication date

1985-04-24

1983-09-29 Application filed by Individual filed Critical Individual

1983-09-29 Priority to JP58181555A priority Critical patent/JPS6072811A/ja

1985-04-24 Publication of JPS6072811A publication Critical patent/JPS6072811A/ja

1987-12-16 Publication of JPS6260362B2 publication Critical patent/JPS6260362B2/ja

Status Granted legal-status Critical Current

Links

239000000945 filler Substances 0.000 title claims abstract description 13
210000004262 dental pulp cavity Anatomy 0.000 title claims description 12
238000004519 manufacturing process Methods 0.000 title claims description 8
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims abstract description 27
239000000203 mixture Substances 0.000 claims abstract description 20
235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 16
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 14
239000003054 catalyst Substances 0.000 claims abstract description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 11
239000000920 calcium hydroxide Substances 0.000 claims abstract description 11
229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 11
229920000642 polymer Polymers 0.000 claims abstract description 11
RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims abstract description 10
238000010438 heat treatment Methods 0.000 claims abstract description 9
BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 7
239000000292 calcium oxide Substances 0.000 claims abstract description 7
ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 7
239000000843 powder Substances 0.000 claims abstract description 7
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 6
239000008103 glucose Substances 0.000 claims abstract description 6
239000011261 inert gas Substances 0.000 claims abstract description 6
NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims abstract description 5
239000005770 Eugenol Substances 0.000 claims abstract description 5
UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims abstract description 5
239000002872 contrast media Substances 0.000 claims abstract description 5
229960002217 eugenol Drugs 0.000 claims abstract description 5
NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims abstract description 5
238000005406 washing Methods 0.000 claims abstract description 4
229960001763 zinc sulfate Drugs 0.000 claims abstract description 4
229910000368 zinc sulfate Inorganic materials 0.000 claims abstract description 4
238000002156 mixing Methods 0.000 claims abstract description 3
239000008158 vegetable oil Substances 0.000 claims description 15
229920002472 Starch Polymers 0.000 claims description 14
239000008107 starch Substances 0.000 claims description 14
235000019698 starch Nutrition 0.000 claims description 14
238000006243 chemical reaction Methods 0.000 claims description 11
150000002989 phenols Chemical class 0.000 claims description 8
210000003074 dental pulp Anatomy 0.000 claims description 7
150000007524 organic acids Chemical class 0.000 claims description 7
150000005846 sugar alcohols Polymers 0.000 claims description 7
238000004898 kneading Methods 0.000 claims description 6
238000000034 method Methods 0.000 claims description 5
239000006188 syrup Substances 0.000 claims description 5
235000020357 syrup Nutrition 0.000 claims description 5
239000003827 pulp capping and pulpectomy agent Substances 0.000 claims description 3
150000003839 salts Chemical class 0.000 claims description 3
150000007522 mineralic acids Chemical class 0.000 claims description 2
235000005985 organic acids Nutrition 0.000 claims description 2
238000004581 coalescence Methods 0.000 claims 1
239000011248 coating agent Substances 0.000 claims 1
238000000576 coating method Methods 0.000 claims 1
238000002845 discoloration Methods 0.000 abstract description 11
LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 abstract description 10
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 8
229960001867 guaiacol Drugs 0.000 abstract description 5
230000007794 irritation Effects 0.000 abstract description 5
WHRZCXAVMTUTDD-UHFFFAOYSA-N 1h-furo[2,3-d]pyrimidin-2-one Chemical compound N1C(=O)N=C2OC=CC2=C1 WHRZCXAVMTUTDD-UHFFFAOYSA-N 0.000 abstract description 3
244000073231 Larrea tridentata Species 0.000 abstract description 3
235000006173 Larrea tridentata Nutrition 0.000 abstract description 3
239000004359 castor oil Substances 0.000 abstract description 3
235000019438 castor oil Nutrition 0.000 abstract description 3
229960002126 creosote Drugs 0.000 abstract description 3
ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 abstract description 3
239000000463 material Substances 0.000 abstract description 3
239000003921 oil Substances 0.000 abstract description 3
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 2
229910052791 calcium Inorganic materials 0.000 abstract description 2
239000011575 calcium Substances 0.000 abstract description 2
239000007795 chemical reaction product Substances 0.000 abstract description 2
235000019197 fats Nutrition 0.000 abstract description 2
235000019198 oils Nutrition 0.000 abstract description 2
235000019871 vegetable fat Nutrition 0.000 abstract description 2
GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 abstract 1
150000002148 esters Chemical class 0.000 abstract 1
235000020429 malt syrup Nutrition 0.000 abstract 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
230000000694 effects Effects 0.000 description 5
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
230000000622 irritating effect Effects 0.000 description 3
238000006116 polymerization reaction Methods 0.000 description 3
239000000047 product Substances 0.000 description 3
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
208000035415 Reinfection Diseases 0.000 description 2
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
150000001299 aldehydes Chemical class 0.000 description 2
TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
238000006482 condensation reaction Methods 0.000 description 2
210000004268 dentin Anatomy 0.000 description 2
239000003925 fat Substances 0.000 description 2
WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
238000004659 sterilization and disinfection Methods 0.000 description 2
238000003756 stirring Methods 0.000 description 2
238000005809 transesterification reaction Methods 0.000 description 2
QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 1
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
241000894006 Bacteria Species 0.000 description 1
BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
235000019483 Peanut oil Nutrition 0.000 description 1
239000002202 Polyethylene glycol Substances 0.000 description 1
208000014151 Stomatognathic disease Diseases 0.000 description 1
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
150000001669 calcium Chemical class 0.000 description 1
229910001424 calcium ion Inorganic materials 0.000 description 1
235000015165 citric acid Nutrition 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
229930003836 cresol Natural products 0.000 description 1
229940013361 cresol Drugs 0.000 description 1
229910001873 dinitrogen Inorganic materials 0.000 description 1
201000010099 disease Diseases 0.000 description 1
208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
235000011187 glycerol Nutrition 0.000 description 1
230000005764 inhibitory process Effects 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
239000004006 olive oil Substances 0.000 description 1
235000008390 olive oil Nutrition 0.000 description 1
235000006408 oxalic acid Nutrition 0.000 description 1
239000000312 peanut oil Substances 0.000 description 1
229920001223 polyethylene glycol Polymers 0.000 description 1
239000008213 purified water Substances 0.000 description 1
230000005855 radiation Effects 0.000 description 1
239000002994 raw material Substances 0.000 description 1
229960001755 resorcinol Drugs 0.000 description 1
239000003549 soybean oil Substances 0.000 description 1
235000012424 soybean oil Nutrition 0.000 description 1
230000000638 stimulation Effects 0.000 description 1
235000002906 tartaric acid Nutrition 0.000 description 1
239000011975 tartaric acid Substances 0.000 description 1
210000005239 tubule Anatomy 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011787 zinc oxide Substances 0.000 description 1

Landscapes

Dental Preparations (AREA)

JP58181555A 1983-09-29 1983-09-29 生活歯髄覆罩兼根管充填剤の製造方法 Granted JPS6072811A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP58181555A JPS6072811A (ja)	1983-09-29	1983-09-29	生活歯髄覆罩兼根管充填剤の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP58181555A JPS6072811A (ja)	1983-09-29	1983-09-29	生活歯髄覆罩兼根管充填剤の製造方法

Publications (2)

Publication Number	Publication Date
JPS6072811A true JPS6072811A (ja)	1985-04-24
JPS6260362B2 JPS6260362B2 (da)	1987-12-16

Family

ID=16102828

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP58181555A Granted JPS6072811A (ja)	1983-09-29	1983-09-29	生活歯髄覆罩兼根管充填剤の製造方法

Country Status (1)

Country	Link
JP (1)	JPS6072811A (da)

1983
- 1983-09-29 JP JP58181555A patent/JPS6072811A/ja active Granted

Also Published As

Publication number	Publication date
JPS6260362B2 (da)	1987-12-16

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