JPS6086119A - 難燃性シリコ−ン変性エポキシ樹脂の製造方法 - Google Patents

難燃性シリコ−ン変性エポキシ樹脂の製造方法

Info

Publication number: JPS6086119A
Authority: JP; Japan
Prior art keywords: epoxy resin; resin; tetrabromobisphenol; epoxy; silicone
Prior art date: 1983-10-17
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP19368983A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6231729B2 (fr

Inventor

Katsuji Shibata

勝司柴田

Masami Yusa

正己湯佐

Kohei Yasuzawa

安沢　興平

Yukio Yoshimura

幸雄吉村

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Resonac Corp

Original Assignee

Hitachi Chemical Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-10-17

Filing date

1983-10-17

Publication date

1985-05-15

1983-10-17 Application filed by Hitachi Chemical Co Ltd filed Critical Hitachi Chemical Co Ltd

1983-10-17 Priority to JP19368983A priority Critical patent/JPS6086119A/ja

1985-05-15 Publication of JPS6086119A publication Critical patent/JPS6086119A/ja

1987-07-10 Publication of JPS6231729B2 publication Critical patent/JPS6231729B2/ja

Status Granted legal-status Critical Current

Links

239000003822 epoxy resin Substances 0.000 title claims abstract description 17
229920000647 polyepoxide Polymers 0.000 title claims abstract description 17
229920001296 polysiloxane Polymers 0.000 title claims abstract description 16
RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims description 5
239000003063 flame retardant Substances 0.000 title claims description 5
125000002887 hydroxy group Chemical group [H]O* 0.000 claims abstract description 9
239000000203 mixture Substances 0.000 claims abstract description 4
239000004593 Epoxy Substances 0.000 claims description 19
239000000543 intermediate Substances 0.000 claims description 10
CMQUQOHNANGDOR-UHFFFAOYSA-N 2,3-dibromo-4-(2,4-dibromo-5-hydroxyphenyl)phenol Chemical compound BrC1=C(Br)C(O)=CC=C1C1=CC(O)=C(Br)C=C1Br CMQUQOHNANGDOR-UHFFFAOYSA-N 0.000 claims description 5
125000003545 alkoxy group Chemical group 0.000 abstract description 8
229920005989 resin Polymers 0.000 abstract description 8
239000011347 resin Substances 0.000 abstract description 8
238000006243 chemical reaction Methods 0.000 abstract description 7
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 abstract description 5
238000000034 method Methods 0.000 abstract description 5
VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 abstract description 4
239000003054 catalyst Substances 0.000 abstract description 3
150000003242 quaternary ammonium salts Chemical class 0.000 abstract description 3
230000000694 effects Effects 0.000 abstract description 2
238000002156 mixing Methods 0.000 abstract description 2
238000010438 heat treatment Methods 0.000 abstract 1
238000004904 shortening Methods 0.000 abstract 1
239000003925 fat Substances 0.000 description 8
238000005553 drilling Methods 0.000 description 6
238000009826 distribution Methods 0.000 description 4
239000011799 hole material Substances 0.000 description 4
OKIZCWYLBDKLSU-UHFFFAOYSA-M N,N,N-Trimethylmethanaminium chloride Chemical compound [Cl-].C[N+](C)(C)C OKIZCWYLBDKLSU-UHFFFAOYSA-M 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 3
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 3
239000000047 product Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
150000001412 amines Chemical class 0.000 description 2
239000002585 base Substances 0.000 description 2
235000009508 confectionery Nutrition 0.000 description 2
238000004821 distillation Methods 0.000 description 2
125000003700 epoxy group Chemical group 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
-1 methoxy, ethoxy Chemical group 0.000 description 2
229920003986 novolac Polymers 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
239000007787 solid Substances 0.000 description 2
DDFYFBUWEBINLX-UHFFFAOYSA-M tetramethylammonium bromide Chemical compound [Br-].C[N+](C)(C)C DDFYFBUWEBINLX-UHFFFAOYSA-M 0.000 description 2
239000002966 varnish Substances 0.000 description 2
LXBGSDVWAMZHDD-UHFFFAOYSA-N 2-methyl-1h-imidazole Chemical compound CC1=NC=CN1 LXBGSDVWAMZHDD-UHFFFAOYSA-N 0.000 description 1
QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 1
ZCUJYXPAKHMBAZ-UHFFFAOYSA-N 2-phenyl-1h-imidazole Chemical compound C1=CNC(C=2C=CC=CC=2)=N1 ZCUJYXPAKHMBAZ-UHFFFAOYSA-N 0.000 description 1
ULKLGIFJWFIQFF-UHFFFAOYSA-N 5K8XI641G3 Chemical compound CCC1=NC=C(C)N1 ULKLGIFJWFIQFF-UHFFFAOYSA-N 0.000 description 1
235000017166 Bambusa arundinacea Nutrition 0.000 description 1
235000017491 Bambusa tulda Nutrition 0.000 description 1
229930185605 Bisphenol Natural products 0.000 description 1
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
240000007594 Oryza sativa Species 0.000 description 1
235000007164 Oryza sativa Nutrition 0.000 description 1
240000002834 Paulownia tomentosa Species 0.000 description 1
244000082204 Phyllostachys viridis Species 0.000 description 1
235000015334 Phyllostachys viridis Nutrition 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
235000012544 Viola sororia Nutrition 0.000 description 1
241001106476 Violaceae Species 0.000 description 1
125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
239000002253 acid Substances 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
239000011425 bamboo Substances 0.000 description 1
238000005452 bending Methods 0.000 description 1
XLRCXWHGTFHOKU-UHFFFAOYSA-M benzyl(dimethyl)sulfanium;chloride Chemical compound [Cl-].C[S+](C)CC1=CC=CC=C1 XLRCXWHGTFHOKU-UHFFFAOYSA-M 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000008280 blood Substances 0.000 description 1
210000004369 blood Anatomy 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
YMKDRGPMQRFJGP-UHFFFAOYSA-M cetylpyridinium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YMKDRGPMQRFJGP-UHFFFAOYSA-M 0.000 description 1
RLGQACBPNDBWTB-UHFFFAOYSA-N cetyltrimethylammonium ion Chemical compound CCCCCCCCCCCCCCCC[N+](C)(C)C RLGQACBPNDBWTB-UHFFFAOYSA-N 0.000 description 1
USJRLGNYCQWLPF-UHFFFAOYSA-N chlorophosphane Chemical compound ClP USJRLGNYCQWLPF-UHFFFAOYSA-N 0.000 description 1
238000004581 coalescence Methods 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
229930003836 cresol Natural products 0.000 description 1
238000005520 cutting process Methods 0.000 description 1
230000006378 damage Effects 0.000 description 1
150000002085 enols Chemical class 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
238000004880 explosion Methods 0.000 description 1
238000005755 formation reaction Methods 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
WJRBRSLFGCUECM-UHFFFAOYSA-N hydantoin Chemical compound O=C1CNC(=O)N1 WJRBRSLFGCUECM-UHFFFAOYSA-N 0.000 description 1
229940091173 hydantoin Drugs 0.000 description 1
229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000010804 inert waste Substances 0.000 description 1
238000002347 injection Methods 0.000 description 1
239000007924 injection Substances 0.000 description 1
125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 1
JNMIXMFEVJHFNY-UHFFFAOYSA-M methyl(triphenyl)phosphanium;iodide Chemical compound [I-].C=1C=CC=CC=1[P+](C=1C=CC=CC=1)(C)C1=CC=CC=C1 JNMIXMFEVJHFNY-UHFFFAOYSA-M 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
PMOIAJVKYNVHQE-UHFFFAOYSA-N phosphanium;bromide Chemical compound [PH4+].[Br-] PMOIAJVKYNVHQE-UHFFFAOYSA-N 0.000 description 1
150000004714 phosphonium salts Chemical class 0.000 description 1
229910000073 phosphorus hydride Inorganic materials 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
229910052573 porcelain Inorganic materials 0.000 description 1
239000000843 powder Substances 0.000 description 1
DGMKFQYCZXERLX-UHFFFAOYSA-N proglumide Chemical compound CCCN(CCC)C(=O)C(CCC(O)=O)NC(=O)C1=CC=CC=C1 DGMKFQYCZXERLX-UHFFFAOYSA-N 0.000 description 1
229960003857 proglumide Drugs 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
235000009566 rice Nutrition 0.000 description 1
239000000243 solution Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
RWSOTUBLDIXVET-UHFFFAOYSA-O sulfonium Chemical compound [SH3+] RWSOTUBLDIXVET-UHFFFAOYSA-O 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1
IBWGNZVCJVLSHB-UHFFFAOYSA-M tetrabutylphosphanium;chloride Chemical compound [Cl-].CCCC[P+](CCCC)(CCCC)CCCC IBWGNZVCJVLSHB-UHFFFAOYSA-M 0.000 description 1
238000003856 thermoforming Methods 0.000 description 1
TUQOTMZNTHZOKS-UHFFFAOYSA-N tributylphosphine Chemical compound CCCCP(CCCC)CCCC TUQOTMZNTHZOKS-UHFFFAOYSA-N 0.000 description 1
ZFEAYIKULRXTAR-UHFFFAOYSA-M triphenylsulfanium;chloride Chemical compound [Cl-].C1=CC=CC=C1[S+](C=1C=CC=CC=1)C1=CC=CC=C1 ZFEAYIKULRXTAR-UHFFFAOYSA-M 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Compositions Of Macromolecular Compounds (AREA)
Epoxy Resins (AREA)

JP19368983A 1983-10-17 1983-10-17 難燃性シリコ−ン変性エポキシ樹脂の製造方法 Granted JPS6086119A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP19368983A JPS6086119A (ja)	1983-10-17	1983-10-17	難燃性シリコ−ン変性エポキシ樹脂の製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP19368983A JPS6086119A (ja)	1983-10-17	1983-10-17	難燃性シリコ−ン変性エポキシ樹脂の製造方法

Publications (2)

Publication Number	Publication Date
JPS6086119A true JPS6086119A (ja)	1985-05-15
JPS6231729B2 JPS6231729B2 (fr)	1987-07-10

Family

ID=16312139

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP19368983A Granted JPS6086119A (ja)	1983-10-17	1983-10-17	難燃性シリコ−ン変性エポキシ樹脂の製造方法

Country Status (1)

Country	Link
JP (1)	JPS6086119A (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2007007234A (ja) *	2005-07-01	2007-01-18	World Ring:Kk	外側リング体と内側リング体からなる空洞部を設けた身飾品の製造方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51118728A (en) *	1975-04-11	1976-10-18	Dow Corning	Process for manufacturing silicone resin
JPS5431021A (en) *	1977-08-12	1979-03-07	Japan Steel Works Ltd	Method of producing dendrite microostructure of chromiummmolybdenum steel by adding titanium and zirconium
JPS55152716A (en) *	1979-05-18	1980-11-28	Matsushita Electric Works Ltd	Preparation of epoxy resin composition

1983
- 1983-10-17 JP JP19368983A patent/JPS6086119A/ja active Granted

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51118728A (en) *	1975-04-11	1976-10-18	Dow Corning	Process for manufacturing silicone resin
JPS5431021A (en) *	1977-08-12	1979-03-07	Japan Steel Works Ltd	Method of producing dendrite microostructure of chromiummmolybdenum steel by adding titanium and zirconium
JPS55152716A (en) *	1979-05-18	1980-11-28	Matsushita Electric Works Ltd	Preparation of epoxy resin composition

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2007007234A (ja) *	2005-07-01	2007-01-18	World Ring:Kk	外側リング体と内側リング体からなる空洞部を設けた身飾品の製造方法

Also Published As

Publication number	Publication date
JPS6231729B2 (fr)	1987-07-10

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JPS6086119A - 難燃性シリコ−ン変性エポキシ樹脂の製造方法 - Google Patents

Info

Links

Landscapes

Priority Applications (1)

Applications Claiming Priority (1)

Publications (2)

Family

ID=16312139

Family Applications (1)

Country Status (1)

Cited By (1)

Citations (3)

Patent Citations (3)

Cited By (1)

Also Published As

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