JPS6176443A - ２価フエノールのエステル誘導体を製造する改良方法 - Google Patents

２価フエノールのエステル誘導体を製造する改良方法

Info

Publication number: JPS6176443A
Authority: JP; Japan
Prior art keywords: adsorbent; activated carbon; acid; dihydric phenol; carbon atoms
Prior art date: 1984-09-18
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Pending

Application number

JP20360985A

Other languages

English (en)

Japanese (ja)

Inventor

ベニト、シー

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Union Carbide Corp

Original Assignee

Union Carbide Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-09-18

Filing date

1985-09-17

Publication date

1986-04-18

1985-09-17 Application filed by Union Carbide Corp filed Critical Union Carbide Corp

1986-04-18 Publication of JPS6176443A publication Critical patent/JPS6176443A/ja

Status Pending legal-status Critical Current

Links

ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title claims description 11
150000002148 esters Chemical class 0.000 title claims description 10
238000004519 manufacturing process Methods 0.000 title description 3
238000000034 method Methods 0.000 claims description 36
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 31
239000003463 adsorbent Substances 0.000 claims description 21
WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical group CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 15
150000002989 phenols Chemical class 0.000 claims description 12
150000008065 acid anhydrides Chemical class 0.000 claims description 11
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 11
AREMQPPGVQNRIE-UHFFFAOYSA-N acetic acid;4-[2-(4-hydroxyphenyl)propan-2-yl]phenol Chemical compound CC(O)=O.CC(O)=O.C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 AREMQPPGVQNRIE-UHFFFAOYSA-N 0.000 claims description 8
125000004432 carbon atom Chemical group C* 0.000 claims description 8
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
239000002253 acid Substances 0.000 claims description 5
239000002808 molecular sieve Substances 0.000 claims description 5
239000000741 silica gel Substances 0.000 claims description 5
229910002027 silica gel Inorganic materials 0.000 claims description 5
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 5
239000000126 substance Substances 0.000 claims description 4
125000002993 cycloalkylene group Chemical group 0.000 claims description 3
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims description 2
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
125000000217 alkyl group Chemical group 0.000 claims description 2
229940106691 bisphenol a Drugs 0.000 claims description 2
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims description 2
229910052794 bromium Inorganic materials 0.000 claims description 2
229910052801 chlorine Inorganic materials 0.000 claims description 2
239000000460 chlorine Substances 0.000 claims description 2
238000010438 heat treatment Methods 0.000 claims 1
125000001183 hydrocarbyl group Chemical group 0.000 claims 1
229930195734 saturated hydrocarbon Natural products 0.000 claims 1
239000002904 solvent Substances 0.000 description 10
241001550224 Apha Species 0.000 description 8
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 8
150000005690 diesters Chemical class 0.000 description 8
229920001230 polyarylate Polymers 0.000 description 8
239000000047 product Substances 0.000 description 7
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
239000000376 reactant Substances 0.000 description 5
239000011541 reaction mixture Substances 0.000 description 5
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
239000000178 monomer Substances 0.000 description 4
239000001294 propane Substances 0.000 description 4
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
150000007513 acids Chemical class 0.000 description 3
-1 aromatic dicarboxylic acids Chemical class 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
229920000642 polymer Polymers 0.000 description 3
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
239000003377 acid catalyst Substances 0.000 description 2
239000003610 charcoal Substances 0.000 description 2
MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
238000004090 dissolution Methods 0.000 description 2
QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
239000000203 mixture Substances 0.000 description 2
238000000746 purification Methods 0.000 description 2
238000001953 recrystallisation Methods 0.000 description 2
238000002834 transmittance Methods 0.000 description 2
OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
RKSBPFMNOJWYSB-UHFFFAOYSA-N 3,3-Bis(4-hydroxyphenyl)pentane Chemical compound C=1C=C(O)C=CC=1C(CC)(CC)C1=CC=C(O)C=C1 RKSBPFMNOJWYSB-UHFFFAOYSA-N 0.000 description 1
DXADWKPCWTXPOY-UHFFFAOYSA-N 3-[(3-hydroxyphenyl)methyl]phenol Chemical compound OC1=CC=CC(CC=2C=C(O)C=CC=2)=C1 DXADWKPCWTXPOY-UHFFFAOYSA-N 0.000 description 1
XDGXPHFWSPGAIB-UHFFFAOYSA-N 4-[1-(4-hydroxy-3-methylphenyl)ethyl]-2-methylphenol Chemical compound C=1C=C(O)C(C)=CC=1C(C)C1=CC=C(O)C(C)=C1 XDGXPHFWSPGAIB-UHFFFAOYSA-N 0.000 description 1
ZZXOXJAAKGCFNH-UHFFFAOYSA-N 4-[2-(4-hydroxyphenyl)-1,2-diphenylpropyl]phenol Chemical compound C=1C=CC=CC=1C(C=1C=CC(O)=CC=1)(C)C(C=1C=CC(O)=CC=1)C1=CC=CC=C1 ZZXOXJAAKGCFNH-UHFFFAOYSA-N 0.000 description 1
WCUDAIJOADOKAW-UHFFFAOYSA-N 4-[2-(4-hydroxyphenyl)pentan-2-yl]phenol Chemical compound C=1C=C(O)C=CC=1C(C)(CCC)C1=CC=C(O)C=C1 WCUDAIJOADOKAW-UHFFFAOYSA-N 0.000 description 1
229930185605 Bisphenol Natural products 0.000 description 1
235000013162 Cocos nucifera Nutrition 0.000 description 1
244000060011 Cocos nucifera Species 0.000 description 1
OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
241000545760 Unio Species 0.000 description 1
125000001931 aliphatic group Chemical group 0.000 description 1
125000002947 alkylene group Chemical group 0.000 description 1
125000001118 alkylidene group Chemical group 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
229910000323 aluminium silicate Inorganic materials 0.000 description 1
229910052786 argon Inorganic materials 0.000 description 1
150000001491 aromatic compounds Chemical class 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
239000012298 atmosphere Substances 0.000 description 1
238000009835 boiling Methods 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
230000007423 decrease Effects 0.000 description 1
229940117389 dichlorobenzene Drugs 0.000 description 1
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
229920006258 high performance thermoplastic Polymers 0.000 description 1
125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
235000006408 oxalic acid Nutrition 0.000 description 1
239000007800 oxidant agent Substances 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
230000009257 reactivity Effects 0.000 description 1
238000010992 reflux Methods 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
150000003457 sulfones Chemical class 0.000 description 1
150000003462 sulfoxides Chemical class 0.000 description 1
ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
239000002023 wood Substances 0.000 description 1
239000008096 xylene Substances 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Polyesters Or Polycarbonates (AREA)

JP20360985A 1984-09-18 1985-09-17 ２価フエノールのエステル誘導体を製造する改良方法 Pending JPS6176443A (ja)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US65180784A	1984-09-18	1984-09-18
US651807		2007-01-10

Publications (1)

Publication Number	Publication Date
JPS6176443A true JPS6176443A (ja)	1986-04-18

Family

ID=24614302

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP20360985A Pending JPS6176443A (ja)	1984-09-18	1985-09-17	２価フエノールのエステル誘導体を製造する改良方法

Country Status (2)

Country	Link
JP (1)	JPS6176443A (fr)
CA (1)	CA1263403A (fr)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51118715A (en) *	1975-04-11	1976-10-18	Konsutanchiinobitsuchi Borisu	Method of producing ester of glycerine * polyglycerine and monobasic aliphatic acid having five to nine carbon atoms
JPS5912923A (ja) *	1982-06-30	1984-01-23	アモコ、コ−ポレ−ション	ポリアリ−レ−トの改良製法

1985
- 1985-09-10 CA CA000490385A patent/CA1263403A/fr not_active Expired
- 1985-09-17 JP JP20360985A patent/JPS6176443A/ja active Pending

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51118715A (en) *	1975-04-11	1976-10-18	Konsutanchiinobitsuchi Borisu	Method of producing ester of glycerine * polyglycerine and monobasic aliphatic acid having five to nine carbon atoms
JPS5912923A (ja) *	1982-06-30	1984-01-23	アモコ、コ−ポレ−ション	ポリアリ−レ−トの改良製法

Also Published As

Publication number	Publication date
CA1263403A (fr)	1989-11-28

Publication	Publication Date	Title
US4439586A (en)	1984-03-27	Process for preparing polyarylates
JP3004722B2 (ja)	2000-01-31	テレフタル酸、２，６−ナフタレンジカルボン酸、ハイドロキノン及び４，４’−ビフェノールからのポリエステル
JP3121012B2 (ja)	2000-12-25	テレフタル酸、２，６−ナフタレンジカルボン酸及びハイドロキノンからのポリエステル
US5136018A (en)	1992-08-04	Macrocyclic polyarylate compositions of decreased crystallinity
US3787475A (en)	1974-01-22	Process for making aryloxy derivatives of aromatic diesters and dinitriles
JPH02147631A (ja)	1990-06-06	熱可塑性の液晶性全芳香族ポリイミドエステル及びその製造法
US4612360A (en)	1986-09-16	Melt polymerization process for preparing polyarylates
JPS6176443A (ja)	1986-04-18	２価フエノールのエステル誘導体を製造する改良方法
US5079335A (en)	1992-01-07	Process for preparing a color-improved thermoplastic polyarylate polymer
US4978739A (en)	1990-12-18	Process for preparing polyarylate from an ester derivative of a dihydric phenol
FR2481287A1 (fr)	1981-10-30	Procede pour la preparation et la purification d'anhydrides d'acides dicarboxyliques et polycarboxyliques
EP0117556B1 (fr)	1991-04-24	Polyestersulfones aromatiques résistant aux températures élevées et procédé pour leur préparation
US4362858A (en)	1982-12-07	Process for producing an aromatic polyester copolymer
US3511809A (en)	1970-05-12	Polyesters from p-arylene-bis (dimethyl acetic acid)
US4958000A (en)	1990-09-18	Process for preparing polyarylates
JPH05287061A (ja)	1993-11-02	液晶ポリマー組成物
US4536564A (en)	1985-08-20	Polyamide from bis-carboxy containing 3,5,3',5'-tetraoxo-1,2-dipiperazine compound and diamine
JPH06239999A (ja)	1994-08-30	ポリエーテルスルホンを含むエステルの製造方法
JP2003292598A (ja)	2003-10-15	ポリエステル
JPS63260922A (ja)	1988-10-27	フエノキシ‐オキシテレフタル酸を基礎とする芳香族系ポリエステル、その製造方法およびその用途
US4127561A (en)	1978-11-28	Polycarbonates and a process for their preparation
JPS63501423A (ja)	1988-06-02	芳香族カルボキシレ−トおよびヨウ化アルキルの同時製造法
JPS5936644A (ja)	1984-02-28	芳香族カルボン酸アリ−ルエステルの精製法
US4520168A (en)	1985-05-28	Color improved polyarylate
US3770804A (en)	1973-11-06	Simultaneous recovery of terephthalic acid and dimethyl terephthalatefrom crude terephthalic acid