JPS62121640A - 貴金属オルガノゾルの製造方法 - Google Patents

貴金属オルガノゾルの製造方法

Info

Publication number: JPS62121640A
Authority: JP; Japan
Prior art keywords: gold; silver; salt; organosol; aqueous solution
Prior art date: 1985-11-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

JP60261889A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0251667B2 (2

Inventor

Yukimichi Nakao

幸道中尾

Kyoji Kaeriyama

帰山　享二

Masao Suda

須田　昌男

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

National Institute of Advanced Industrial Science and Technology AIST

Original Assignee

Agency of Industrial Science and Technology

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-11-21

Filing date

1985-11-21

Publication date

1987-06-02

1985-11-21 Application filed by Agency of Industrial Science and Technology filed Critical Agency of Industrial Science and Technology

1985-11-21 Priority to JP60261889A priority Critical patent/JPS62121640A/ja

1987-06-02 Publication of JPS62121640A publication Critical patent/JPS62121640A/ja

1990-11-08 Publication of JPH0251667B2 publication Critical patent/JPH0251667B2/ja

Status Granted legal-status Critical Current

Links

229910000510 noble metal Inorganic materials 0.000 title description 6
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims abstract description 24
229910052737 gold Inorganic materials 0.000 claims abstract description 24
239000010931 gold Substances 0.000 claims abstract description 24
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract description 18
150000003839 salts Chemical class 0.000 claims abstract description 17
229910052709 silver Inorganic materials 0.000 claims abstract description 17
239000004332 silver Substances 0.000 claims abstract description 17
239000007864 aqueous solution Substances 0.000 claims abstract description 14
239000004094 surface-active agent Substances 0.000 claims abstract description 9
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims abstract description 8
229910052783 alkali metal Inorganic materials 0.000 claims abstract description 6
150000001340 alkali metals Chemical class 0.000 claims abstract description 6
229910052751 metal Inorganic materials 0.000 claims abstract description 5
239000002184 metal Substances 0.000 claims abstract description 5
239000007787 solid Substances 0.000 claims abstract description 3
239000003960 organic solvent Substances 0.000 claims description 8
238000001704 evaporation Methods 0.000 claims description 3
238000004519 manufacturing process Methods 0.000 claims description 3
239000000203 mixture Substances 0.000 abstract description 4
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 abstract description 4
229910001961 silver nitrate Inorganic materials 0.000 abstract description 2
229910003803 Gold(III) chloride Inorganic materials 0.000 abstract 1
RJHLTVSLYWWTEF-UHFFFAOYSA-K gold trichloride Chemical compound Cl[Au](Cl)Cl RJHLTVSLYWWTEF-UHFFFAOYSA-K 0.000 abstract 1
239000000017 hydrogel Substances 0.000 abstract 1
239000012266 salt solution Substances 0.000 abstract 1
239000002904 solvent Substances 0.000 abstract 1
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 8
238000000034 method Methods 0.000 description 7
239000007788 liquid Substances 0.000 description 5
239000010970 precious metal Substances 0.000 description 5
239000000084 colloidal system Substances 0.000 description 4
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
239000002253 acid Substances 0.000 description 3
239000002612 dispersion medium Substances 0.000 description 3
239000002245 particle Substances 0.000 description 3
239000002244 precipitate Substances 0.000 description 3
238000001556 precipitation Methods 0.000 description 3
SDKPSXWGRWWLKR-UHFFFAOYSA-M sodium;9,10-dioxoanthracene-1-sulfonate Chemical compound [Na+].O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2S(=O)(=O)[O-] SDKPSXWGRWWLKR-UHFFFAOYSA-M 0.000 description 3
239000000243 solution Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
238000010908 decantation Methods 0.000 description 2
238000005516 engineering process Methods 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
229930195733 hydrocarbon Natural products 0.000 description 2
150000002823 nitrates Chemical class 0.000 description 2
229910001112 rose gold Inorganic materials 0.000 description 2
JHJLBTNAGRQEKS-UHFFFAOYSA-M sodium bromide Chemical compound [Na+].[Br-] JHJLBTNAGRQEKS-UHFFFAOYSA-M 0.000 description 2
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
-1 alicyclic hydrocarbons Chemical class 0.000 description 1
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
239000003513 alkali Substances 0.000 description 1
229910052784 alkaline earth metal Inorganic materials 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical compound B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 description 1
229910010277 boron hydride Inorganic materials 0.000 description 1
YMKDRGPMQRFJGP-UHFFFAOYSA-M cetylpyridinium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+]1=CC=CC=C1 YMKDRGPMQRFJGP-UHFFFAOYSA-M 0.000 description 1
239000003638 chemical reducing agent Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000004040 coloring Methods 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
239000006185 dispersion Substances 0.000 description 1
238000009826 distribution Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000010891 electric arc Methods 0.000 description 1
GCFHZZWXZLABBL-UHFFFAOYSA-N ethanol;hexane Chemical compound CCO.CCCCCC GCFHZZWXZLABBL-UHFFFAOYSA-N 0.000 description 1
239000000835 fiber Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
FDWREHZXQUYJFJ-UHFFFAOYSA-M gold monochloride Chemical compound [Cl-].[Au+] FDWREHZXQUYJFJ-UHFFFAOYSA-M 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
229910010272 inorganic material Inorganic materials 0.000 description 1
239000011147 inorganic material Substances 0.000 description 1
239000002923 metal particle Substances 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical class OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
239000002861 polymer material Substances 0.000 description 1
239000003223 protective agent Substances 0.000 description 1
239000002994 raw material Substances 0.000 description 1
239000012279 sodium borohydride Substances 0.000 description 1
229910000033 sodium borohydride Inorganic materials 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000006228 supernatant Substances 0.000 description 1

Landscapes

Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Colloid Chemistry (AREA)
Manufacture And Refinement Of Metals (AREA)

JP60261889A 1985-11-21 1985-11-21 貴金属オルガノゾルの製造方法 Granted JPS62121640A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP60261889A JPS62121640A (ja)	1985-11-21	1985-11-21	貴金属オルガノゾルの製造方法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP60261889A JPS62121640A (ja)	1985-11-21	1985-11-21	貴金属オルガノゾルの製造方法

Publications (2)

Publication Number	Publication Date
JPS62121640A true JPS62121640A (ja)	1987-06-02
JPH0251667B2 JPH0251667B2 (2)	1990-11-08

Family

ID=17368172

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP60261889A Granted JPS62121640A (ja)	1985-11-21	1985-11-21	貴金属オルガノゾルの製造方法

Country Status (1)

Country	Link
JP (1)	JPS62121640A (2)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH02277706A (ja) *	1989-04-19	1990-11-14	Tanaka Kikinzoku Kogyo Kk	貴金属微粒子の調製方法
WO2005023468A1 (ja) *	2003-08-28	2005-03-17	Tama-Tlo, Ltd.	貴金属コロイド、貴金属微粒子、組成物および貴金属微粒子の製造方法
JP2011052326A (ja) *	1999-06-15	2011-03-17	Akio Komatsu	金属複合超微粒子及びその製造方法

1985
- 1985-11-21 JP JP60261889A patent/JPS62121640A/ja active Granted

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPH02277706A (ja) *	1989-04-19	1990-11-14	Tanaka Kikinzoku Kogyo Kk	貴金属微粒子の調製方法
JP2011052326A (ja) *	1999-06-15	2011-03-17	Akio Komatsu	金属複合超微粒子及びその製造方法
JP4732645B2 (ja) *	1999-06-15	2011-07-27	丸山稔	金属複合超微粒子の製造方法
WO2005023468A1 (ja) *	2003-08-28	2005-03-17	Tama-Tlo, Ltd.	貴金属コロイド、貴金属微粒子、組成物および貴金属微粒子の製造方法
US7928149B2 (en)	2003-08-28	2011-04-19	Tama-Tlo, Ltd.	Precious metal colloid, precious metal fine-particle, composition, and method for producing precious metal fine-particle

Also Published As

Publication number	Publication date
JPH0251667B2 (2)	1990-11-08

Legal Events

Date	Code	Title	Description
2005-11-21	EXPY	Cancellation because of completion of term

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