JPS6236650B2 - - Google Patents
Info
- Publication number
- JPS6236650B2 JPS6236650B2 JP55058491A JP5849180A JPS6236650B2 JP S6236650 B2 JPS6236650 B2 JP S6236650B2 JP 55058491 A JP55058491 A JP 55058491A JP 5849180 A JP5849180 A JP 5849180A JP S6236650 B2 JPS6236650 B2 JP S6236650B2
- Authority
- JP
- Japan
- Prior art keywords
- extraction
- extract
- rich
- stock
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000605 extraction Methods 0.000 claims description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- 239000000284 extract Substances 0.000 claims description 21
- 235000014347 soups Nutrition 0.000 claims description 17
- 125000003118 aryl group Chemical group 0.000 claims description 15
- 239000000796 flavoring agent Substances 0.000 claims description 11
- 235000019634 flavors Nutrition 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 239000012141 concentrate Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 description 11
- 238000009835 boiling Methods 0.000 description 10
- 241000269821 Scombridae Species 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 235000020640 mackerel Nutrition 0.000 description 6
- 241001377695 Polygonum arenastrum Species 0.000 description 5
- 235000006386 Polygonum aviculare Nutrition 0.000 description 5
- 241000269851 Sarda sarda Species 0.000 description 5
- 239000002253 acid Substances 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 235000021067 refined food Nutrition 0.000 description 1
- 238000013077 scoring method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Landscapes
- Seeds, Soups, And Other Foods (AREA)
- Seasonings (AREA)
Description
本発明は風味の優れた濃厚だしの製造方法に関
する。
風味の良い抽出液、いわゆる“だし”を作るに
は大量の熱湯を用いて抽出する方法が最も良く、
一般的には節に対して20〜50倍の熱湯が用いられ
る。しかしながら、この20〜50倍の熱湯による抽
出液であるいわゆるだし液そのものは、量販性に
欠け、また、加工食品、調味料などにおいてもだ
し液そのものよりも、これを濃厚した、節類濃厚
抽出液、即ち濃厚だしが要求される。
従来、節類より濃厚な抽出液を得る方法として
は、節類を熱湯抽出後単に濃厚する方法、節類を
酵素分解又は鉱酸分解する方法、節類を有機溶剤
で節芳香成分を抽出した後残渣を熱湯にて抽出す
るか又は鉱酸分解して呈味成分を得、両者を合せ
る方法などが知られている。
この内、鉱酸や酵素で加水分解する方法、ある
いは有機溶剤で抽出する方法では最も大切である
芳香成分等の変質が避けられず、風味の良いもの
は得られない。また、節類を熱湯抽出後、単に濃
縮する方法では、濃縮の際多量のエネルギーを消
費し、その上大部分の芳香成分が飛散してしまう
ため、風味の良い濃厚だしは得られていない。
熱湯で抽出する際、熱湯の量を少くすれば濃縮
が少くてすむが、熱湯が少ないと抽出が充分行わ
れないので風味の良いだしが得られない。
本発明者等は上記現状に鑑み、風味の優れた濃
厚だしを効率良く製造する方法を開発することを
目的として種々研究を重ねた結果、節類の呈味成
分と芳香成分を熱湯及び含水アルコールで夫々効
率良く抽出する工程を組合せることにより風味の
優れた濃厚だしが効率良く製造できることを発見
し本発明を完成するに至つた。
本発明の節類としてはかつお節、宗田節、サバ
節などの節類、あるいはけずり節が使用される。
第1工程は節類から主として呈味成分を抽出する
工程で節類を小さく粉砕し、節類に対し1〜10
倍、望ましくは2〜5倍の熱湯を用いて抽出す
る。抽出は70〜98℃の温度で抽出することが望ま
しく、又効率的に抽出する目的から連続又は半連
続的に向流多段抽出することが望ましい。一般に
節類からだしを抽出するには20〜50倍の水を用い
るが、本発明では1〜10倍と少ない水を用いてい
る。本発明者等は水の量と得られるだしの品質に
ついて調べたところ、だしの品質は抽出時の節類
に対する水の量により大きく左右され、水が少な
くなるに従い、呈味性核酸等の呈味成分の抽出率
は変らないが、節の芳香成分の抽出率が低下する
ため、節特有の芳香の乏しいだししか得られない
ことがわかつた。
又、この現象は他の抽出条件、例えば節類の形
状、粒度、抽出温度、時間、抽出残渣との分離の
条件等によつて変化しないことが判明した。
抽出残渣を分離して得られる抽出液“だし”は
呈味の強さは充分であるが、芳香は弱く、節の芳
香成分の大部分は抽出残渣に残つている。この芳
香成分は含水アルコールで抽出すれば簡単に抽出
することができる。
抽出方法は少ない水で効率良く抽出するには向
流多段抽出法が望ましい。向流多段抽出機はどの
ようなタイプでも良いが、抽出時の芳香成分の飛
散を防ぐため密閉型とし、蒸発部は回収すること
が望ましい。
本発明の方法の第2工程では、抽出残渣中に残
存している芳香成分をアルコール又は含水アルコ
ールを加えて20〜80℃で抽出を行い、抽出残渣を
除去し、次いでアルコール分を除去して芳香成分
に富んだ抽出液を得る。
抽出の際使用するアルコールはエタノール、プ
ロパノール、あるいはイソプロパノール等の低級
アルコールが用いられ、水抽出した抽出残渣の乾
物1部に対し1〜10倍のアルコール又は含水アル
コールが使用される。抽出液からアルコールを除
去する方法は単に加熱するだけでも良いし、又減
圧濃縮によつても良い。芳香成分はアルコールへ
は移行しないので、濃厚な芳香成分抽出液が得ら
れる。蒸発させたアルコールは回収して再度使用
する。回収アルコールには節の芳香成分は移行し
ない。このようにして得られた抽出液の芳香は、
芳香成分の一部は既に第1工程の熱水抽出で抽出
されてしまつているため、節類の芳香成分の全て
が濃縮されているわけではないので、これ自体で
は節類特有の芳香を有しているわけではない。第
3工程に於て第1工程の呈味成分抽出液と第2工
程の芳香成分抽出液を合せることによつてはじめ
て節類特有の芳香を有する濃厚だしが得られる。
本発明の方法ではアルコール抽出法を含んでいる
が従来法のようにアルコールによる風味の変質は
全く見られず、本発明の方法で得られる濃厚だし
は従来法では得られない節特有の芳香を有し、水
で希釈することにより、通常のだしを完全に再現
することができる。
以下、実施例にて詳細に説明する。
実施例 1
かつお枯節20kgを阻砕し、密閉型のパドル型連
続向流抽出機を用い、抽出温度90℃で45分間熱湯
60kgと節粒子を向流接触させた。次いで遠心分離
して抽出残渣を分離し、抽出液45kgと抽出残渣35
kgを得た。
この抽出残渣35kg(乾物18kg)に95%エタノー
ルを54kgを加え60℃で30分間抽出し、遠心分離
し、抽出残渣を少量の95%エタノールで洗浄して
付着分を回収し抽出液を合わせた。この抽出液を
減圧濃縮してエタノールを除去し、1.2kgの濃縮
液を得た。このエタノールは回収した。回収エタ
ノールには節の芳香は殆んど無く、芳香成分は濃
縮液に濃縮された。この濃縮液を最初に得られた
抽出液に加えて46.2kgの濃縮だしを得た。この濃
厚だし100gは使用したかつお節30gの有効成分
を含む濃厚だしに相当するものであることが確認
された。
一方、上記で得られた濃厚だしの品質を確認す
るため、かつお枯節を単に30%濃度で熱湯1回抽
出した濃厚だしを調製した。
このようにして作つた2種の濃厚だしを水で10
倍に希釈し、かつお枯節の3%抽出液をコントロ
ールとしてパネル数20による官能検査を行つた。
結果を第1表に示す。
The present invention relates to a method for producing rich soup stock with excellent flavor. The best way to make a flavorful extract, known as dashi, is to use a large amount of boiling water.
Generally, 20 to 50 times more hot water is used than knots. However, the so-called stock itself, which is an extraction liquid made with 20 to 50 times as much boiling water, lacks the ability to be sold in large quantities, and it is also used for processed foods and seasonings. A liquid, or thick stock, is required. Conventionally, methods for obtaining a thicker extract from knotweed include simply enriching it after extracting knotweed with boiling water, decomposing the knotlet with an enzyme or mineral acid, and extracting the aromatic components of knotweed with an organic solvent. There are known methods such as extracting the residue with hot water or decomposing it with mineral acid to obtain flavor components and combining the two. Among these methods, the methods of hydrolysis using mineral acids or enzymes, or the methods of extraction using organic solvents, cannot avoid deterioration of the most important aromatic components, making it impossible to obtain products with good flavor. In addition, simply concentrating the joints after extracting them with hot water consumes a large amount of energy during concentration, and most of the aromatic components are scattered, making it impossible to obtain a rich and flavorful soup stock. When extracting with boiling water, reducing the amount of boiling water will reduce the concentration, but if the amount of boiling water is too small, the extraction will not be carried out sufficiently, making it impossible to obtain a stock with good flavor. In view of the above-mentioned current situation, the present inventors have conducted various studies with the aim of developing a method for efficiently producing rich soup stock with excellent flavor. The inventors have discovered that a rich and flavorful soup stock can be efficiently produced by combining the efficient extraction steps of each method, leading to the completion of the present invention. The knots used in the present invention include bonito flakes, Sota flakes, mackerel flakes, etc., or kezuri flakes.
The first step is to mainly extract flavor components from the knots, and the knots are crushed into small pieces.
Extract using twice as much hot water, preferably 2 to 5 times as much hot water. Extraction is preferably carried out at a temperature of 70 to 98°C, and for the purpose of efficient extraction, continuous or semi-continuous countercurrent multi-stage extraction is desirable. Generally, 20 to 50 times as much water is used to extract dashi from knotweed, but in the present invention, 1 to 10 times less water is used. The present inventors investigated the amount of water and the quality of the resulting stock, and found that the quality of the stock was largely influenced by the amount of water relative to the joints at the time of extraction, and as the amount of water decreased, the quality of taste-producing nucleic acids, etc. It was found that although the extraction rate of flavor components remained the same, the extraction rate of the aromatic components of knots decreased, resulting in a stock that lacked the aroma characteristic of knots. It was also found that this phenomenon does not change depending on other extraction conditions, such as the shape of the knots, particle size, extraction temperature, time, and conditions for separation from the extraction residue. The extract "dashi" obtained by separating the extraction residue has a strong enough taste, but the aroma is weak, and most of the aromatic components of the knots remain in the extraction residue. This aromatic component can be easily extracted using hydroalcohol. As for the extraction method, a countercurrent multistage extraction method is preferable for efficient extraction with a small amount of water. Any type of countercurrent multistage extractor may be used, but it is preferable to use a closed type to prevent aroma components from scattering during extraction, and to recover the evaporation section. In the second step of the method of the present invention, the aromatic components remaining in the extraction residue are extracted at 20 to 80°C by adding alcohol or hydrous alcohol to remove the extraction residue, and then the alcohol content is removed. Obtain an extract rich in aromatic components. The alcohol used in the extraction is a lower alcohol such as ethanol, propanol, or isopropanol, and 1 to 10 times the amount of alcohol or hydrous alcohol is used per 1 part of the dry matter of the water-extracted extraction residue. Alcohol can be removed from the extract by simply heating it or by concentrating it under reduced pressure. Since aroma components do not transfer to alcohol, a rich aroma component extract can be obtained. The evaporated alcohol is collected and used again. The aromatic components of knots do not transfer to the recovered alcohol. The aroma of the extract obtained in this way is
Some of the aromatic components have already been extracted in the first step of hot water extraction, so not all of the aromatic components of the joints are concentrated, so this product itself does not have the characteristic aroma of joints. Not that I'm doing it. In the third step, by combining the taste component extract from the first step and the aromatic component extract from the second step, a rich soup stock having the aroma characteristic of knotweed can be obtained.
Although the method of the present invention includes an alcohol extraction method, unlike the conventional method, there is no change in flavor due to alcohol, and the rich soup stock obtained by the method of the present invention has a unique aroma unique to knots that cannot be obtained with the conventional method. By diluting it with water, it is possible to perfectly reproduce normal soup stock. Hereinafter, this will be explained in detail in Examples. Example 1 20 kg of dried bonito flakes were crushed and extracted using boiling water at an extraction temperature of 90°C for 45 minutes using a closed paddle-type continuous countercurrent extractor.
60 kg and the nodal particles were brought into countercurrent contact. Next, the extraction residue was separated by centrifugation, and 45 kg of extract liquid and 35 kg of extraction residue were separated.
gained kg. 54 kg of 95% ethanol was added to 35 kg of this extraction residue (18 kg dry matter), extracted at 60°C for 30 minutes, centrifuged, the extracted residue was washed with a small amount of 95% ethanol, the adhering matter was collected, and the extracts were combined. . This extract was concentrated under reduced pressure to remove ethanol, and 1.2 kg of concentrated solution was obtained. This ethanol was recovered. The recovered ethanol had almost no knot aroma, and the aroma components were concentrated into a concentrated liquid. This concentrated liquid was added to the first obtained extract to obtain 46.2 kg of concentrated stock. It was confirmed that 100 g of this thick soup stock was equivalent to the thick soup stock containing the active ingredients of the 30 g of dried bonito flakes used. On the other hand, in order to confirm the quality of the rich soup stock obtained above, a rich stock was prepared by simply extracting dried bonito flakes once with boiling water at a concentration of 30%. Add the two types of rich soup stock made in this way to 10% with water.
A sensory test was conducted using 20 panels using a 3% extract of dried bonito flakes as a control.
The results are shown in Table 1.
【表】
尚、評点は、コントロールのだしと比較して、
コントロールより良いとき5点、同等であるとき
4点、やや劣るとき3点、劣るとき2点、非常に
劣るとき1点として評点した。
実施例 2
さば節20kgを粗砕し、密閉型のパドル型連続向
流抽出機を用い抽出温度90℃で45分間熱湯60kgと
節粒子を向流接触させ、次いで遠心分離して抽出
残渣を分離し、抽出液42kgと抽出残渣38kgを得
た。
この抽出残渣38kgから、実施例1と同様の方法
で芳香成分濃縮液約1.6kgを得、これを最初に得
られた抽出液42kgに加えて、さば節を原料とした
濃厚だし43.6kgを得た。この濃厚だし100gはさ
ば節30gの有効成分を含む濃厚だしに相当するも
のであることが確認された。
実施例1と同様にさば節を30%濃度で熱湯1回
抽出したものを比較のため調製した。別に、コン
トロールとして、さば節の3%抽出液を調製し、
前記2種の濃厚だしについても水で10倍に希釈
し、実施例1と同様の評点法でパネル数20による
官能検査を実施した。結果を第2表に示す。[Table] The scores are compared to the control stock.
The score was 5 points when it was better than the control, 4 points when it was equivalent, 3 points when it was slightly inferior, 2 points when it was inferior, and 1 point when it was very inferior. Example 2 20 kg of mackerel flakes were roughly crushed, and 60 kg of hot water was brought into countercurrent contact with 60 kg of boiling water for 45 minutes at an extraction temperature of 90°C using a closed paddle-type continuous countercurrent extractor, followed by centrifugation to separate the extraction residue. 42 kg of extract liquid and 38 kg of extraction residue were obtained. From 38 kg of this extraction residue, approximately 1.6 kg of aroma component concentrate was obtained in the same manner as in Example 1, and this was added to 42 kg of the initially obtained extract to obtain 43.6 kg of concentrated stock made from mackerel flakes. Ta. It was confirmed that 100g of this thick stock was equivalent to a thick stock containing 30g of active ingredients from mackerel flakes. Similar to Example 1, mackerel flakes were extracted once with boiling water at a concentration of 30% and prepared for comparison. Separately, as a control, a 3% extract of mackerel was prepared,
The above two types of concentrated soup stock were also diluted 10 times with water, and a sensory test was conducted using 20 panels using the same scoring method as in Example 1. The results are shown in Table 2.
【表】
第1表及び第2表に示すように、本発明の方法
で得られる濃厚だしは、通常のだしと比較した場
合においても、むしろ風味全体が好まれる傾向に
あり、充分満足できる品質であつた。[Table] As shown in Tables 1 and 2, the rich soup stock obtained by the method of the present invention tends to have a more favorable overall flavor, even when compared with regular soup stock, and has a sufficiently satisfactory quality. It was hot.
Claims (1)
造方法。 節類1部に水1〜10部を接触させて呈味成分を
抽出し、抽出残渣を分離し、所望により抽出液を
濃縮する第1工程、該抽出残渣を含水アルコール
と接触させて芳香成分を抽出し、抽出残渣を分離
した後、アルコールを除去して芳香成分を得る第
2工程、 第2工程で得られる芳香成分を第1工程の抽出
液に加えて風味の良い濃厚だしを製造する第3工
程。 2 節類からの呈味成分の抽出が向流多段抽出に
よるものであることを特徴とする特許請求の範囲
第1項記載の濃厚だしの製造方法。 3 前記第1工程において、節類1部に対し、接
触させる水の量が2〜5部であることを特徴とす
る特許請求の範囲第1項記載の濃厚だしの製造方
法。 4 前記第2工程において、抽出残渣乾燥物1部
に対し、含水アルコールを2〜5部接触させ、抽
出温度20〜80℃にて1回抽出を行うことを特徴と
する特許請求の範囲第1項記載の濃厚だしの製造
方法。[Claims] 1. A method for producing rich and flavorful soup stock comprising the following three steps: The first step is to contact 1 part of the joints with 1 to 10 parts of water to extract the flavor components, separate the extraction residue, and optionally concentrate the extract.The extraction residue is brought into contact with hydroalcohol to extract the aromatic components. After extracting and separating the extraction residue, the second step is to remove alcohol to obtain aromatic components.The aromatic components obtained in the second step are added to the extract from the first step to produce a rich and flavorful soup stock. Third step. 2. The method for producing a rich stock according to claim 1, wherein the extraction of flavor components from the joints is carried out by countercurrent multi-stage extraction. 3. The method for producing a rich stock according to claim 1, wherein in the first step, the amount of water brought into contact with 1 part of joints is 2 to 5 parts. 4. Claim 1, characterized in that in the second step, 1 part of the dried extraction residue is brought into contact with 2 to 5 parts of hydrous alcohol, and extraction is performed once at an extraction temperature of 20 to 80°C. Method for producing thick soup stock as described in section.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5849180A JPS56154975A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5849180A JPS56154975A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS56154975A JPS56154975A (en) | 1981-11-30 |
| JPS6236650B2 true JPS6236650B2 (en) | 1987-08-07 |
Family
ID=13085888
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5849180A Granted JPS56154975A (en) | 1980-05-01 | 1980-05-01 | Preparation of concentrated soup stock |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS56154975A (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015159789A (en) * | 2014-02-28 | 2015-09-07 | キッコーマン株式会社 | Bonito soup stock and method of producing the same |
| JP6905735B2 (en) * | 2017-04-04 | 2021-07-21 | ヤマキ株式会社 | How to make flavor oil |
-
1980
- 1980-05-01 JP JP5849180A patent/JPS56154975A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS56154975A (en) | 1981-11-30 |
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