JPS6310939B2 - - Google Patents

Info

Publication number: JPS6310939B2
Authority: JP; Japan
Prior art keywords: tin; oxalate; tin oxalate; dissolved; solution
Prior art date: 1980-02-22
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP2137080A

Other languages

English (en)

Japanese (ja)

Other versions

JPS56118037A (en

Inventor

Masataka Murata

Masaaki Takimoto

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Fujifilm Holdings Corp

Original Assignee

Fuji Photo Film Co Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-02-22

Filing date

1980-02-22

Publication date

1988-03-10

1980-02-22 Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd

1980-02-22 Priority to JP2137080A priority Critical patent/JPS56118037A/ja

1981-09-16 Publication of JPS56118037A publication Critical patent/JPS56118037A/ja

1988-03-10 Publication of JPS6310939B2 publication Critical patent/JPS6310939B2/ja

Status Granted legal-status Critical Current

Links

NGCDGPPKVSZGRR-UHFFFAOYSA-J 1,4,6,9-tetraoxa-5-stannaspiro[4.4]nonane-2,3,7,8-tetrone Chemical compound [Sn+4].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O NGCDGPPKVSZGRR-UHFFFAOYSA-J 0.000 claims description 30
-1 sulfuric acid compound Chemical class 0.000 claims description 18
150000003606 tin compounds Chemical class 0.000 claims description 9
238000004519 manufacturing process Methods 0.000 claims description 6
239000002736 nonionic surfactant Substances 0.000 claims description 5
QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 5
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 16
238000000034 method Methods 0.000 description 13
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
TXUICONDJPYNPY-UHFFFAOYSA-N (1,10,13-trimethyl-3-oxo-4,5,6,7,8,9,11,12,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-17-yl) heptanoate Chemical compound C1CC2CC(=O)C=C(C)C2(C)C2C1C1CCC(OC(=O)CCCCCC)C1(C)CC2 TXUICONDJPYNPY-UHFFFAOYSA-N 0.000 description 7
229910021626 Tin(II) chloride Inorganic materials 0.000 description 7
235000014113 dietary fatty acids Nutrition 0.000 description 7
239000000194 fatty acid Substances 0.000 description 7
229930195729 fatty acid Natural products 0.000 description 7
150000004665 fatty acids Chemical class 0.000 description 7
239000001119 stannous chloride Substances 0.000 description 7
235000011150 stannous chloride Nutrition 0.000 description 7
229920003171 Poly (ethylene oxide) Polymers 0.000 description 6
230000015572 biosynthetic process Effects 0.000 description 6
235000006408 oxalic acid Nutrition 0.000 description 6
239000002904 solvent Substances 0.000 description 6
239000004094 surface-active agent Substances 0.000 description 6
238000003786 synthesis reaction Methods 0.000 description 6
239000013078 crystal Substances 0.000 description 5
238000003756 stirring Methods 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 4
239000002994 raw material Substances 0.000 description 4
ZSUXOVNWDZTCFN-UHFFFAOYSA-L tin(ii) bromide Chemical compound Br[Sn]Br ZSUXOVNWDZTCFN-UHFFFAOYSA-L 0.000 description 4
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
239000000203 mixture Substances 0.000 description 3
XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 3
229910001887 tin oxide Inorganic materials 0.000 description 3
JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
239000004372 Polyvinyl alcohol Substances 0.000 description 2
239000002253 acid Substances 0.000 description 2
VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 2
239000003054 catalyst Substances 0.000 description 2
239000000084 colloidal system Substances 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
239000006258 conductive agent Substances 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000008018 melting Effects 0.000 description 2
238000002156 mixing Methods 0.000 description 2
229920002451 polyvinyl alcohol Polymers 0.000 description 2
230000001681 protective effect Effects 0.000 description 2
238000001953 recrystallisation Methods 0.000 description 2
RCIVOBGSMSSVTR-UHFFFAOYSA-L stannous sulfate Chemical compound [SnH2+2].[O-]S([O-])(=O)=O RCIVOBGSMSSVTR-UHFFFAOYSA-L 0.000 description 2
229910000375 tin(II) sulfate Inorganic materials 0.000 description 2
JTDNNCYXCFHBGG-UHFFFAOYSA-L tin(ii) iodide Chemical compound I[Sn]I JTDNNCYXCFHBGG-UHFFFAOYSA-L 0.000 description 2
CQMNNMLVXSWLCH-UHFFFAOYSA-B 2-hydroxypropane-1,2,3-tricarboxylate;tin(4+) Chemical compound [Sn+4].[Sn+4].[Sn+4].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O CQMNNMLVXSWLCH-UHFFFAOYSA-B 0.000 description 1
IOVSQAQVXZOFTD-UHFFFAOYSA-N 2-hydroxypropane-1,2,3-tricarboxylic acid;tin Chemical compound [Sn].OC(=O)CC(O)(C(O)=O)CC(O)=O IOVSQAQVXZOFTD-UHFFFAOYSA-N 0.000 description 1
RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
235000008733 Citrus aurantifolia Nutrition 0.000 description 1
108010010803 Gelatin Proteins 0.000 description 1
235000011941 Tilia x europaea Nutrition 0.000 description 1
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
238000002441 X-ray diffraction Methods 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
150000003973 alkyl amines Chemical class 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
238000002048 anodisation reaction Methods 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
ZCLVNIZJEKLGFA-UHFFFAOYSA-H bis(4,5-dioxo-1,3,2-dioxalumolan-2-yl) oxalate Chemical compound [Al+3].[Al+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O ZCLVNIZJEKLGFA-UHFFFAOYSA-H 0.000 description 1
QXDMQSPYEZFLGF-UHFFFAOYSA-L calcium oxalate Chemical compound [Ca+2].[O-]C(=O)C([O-])=O QXDMQSPYEZFLGF-UHFFFAOYSA-L 0.000 description 1
239000001768 carboxy methyl cellulose Substances 0.000 description 1
235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
239000008112 carboxymethyl-cellulose Substances 0.000 description 1
239000001913 cellulose Substances 0.000 description 1
229920002678 cellulose Polymers 0.000 description 1
239000011248 coating agent Substances 0.000 description 1
238000000576 coating method Methods 0.000 description 1
YNQRWVCLAIUHHI-UHFFFAOYSA-L dilithium;oxalate Chemical compound [Li+].[Li+].[O-]C(=O)C([O-])=O YNQRWVCLAIUHHI-UHFFFAOYSA-L 0.000 description 1
IRXRGVFLQOSHOH-UHFFFAOYSA-L dipotassium;oxalate Chemical compound [K+].[K+].[O-]C(=O)C([O-])=O IRXRGVFLQOSHOH-UHFFFAOYSA-L 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
238000001035 drying Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000003792 electrolyte Substances 0.000 description 1
238000000921 elemental analysis Methods 0.000 description 1
238000005886 esterification reaction Methods 0.000 description 1
150000002148 esters Chemical class 0.000 description 1
LRMHFDNWKCSEQU-UHFFFAOYSA-N ethoxyethane;phenol Chemical compound CCOCC.OC1=CC=CC=C1 LRMHFDNWKCSEQU-UHFFFAOYSA-N 0.000 description 1
239000000835 fiber Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
238000009472 formulation Methods 0.000 description 1
229920000159 gelatin Polymers 0.000 description 1
239000008273 gelatin Substances 0.000 description 1
235000019322 gelatine Nutrition 0.000 description 1
235000011852 gelatine desserts Nutrition 0.000 description 1
150000002314 glycerols Chemical class 0.000 description 1
150000002334 glycols Chemical class 0.000 description 1
238000005984 hydrogenation reaction Methods 0.000 description 1
150000002433 hydrophilic molecules Chemical class 0.000 description 1
125000001165 hydrophobic group Chemical group 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
239000004571 lime Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical class OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920001451 polypropylene glycol Polymers 0.000 description 1
235000019422 polyvinyl alcohol Nutrition 0.000 description 1
229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
239000001267 polyvinylpyrrolidone Substances 0.000 description 1
235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 description 1
229940039790 sodium oxalate Drugs 0.000 description 1
229940108184 stannous iodide Drugs 0.000 description 1
239000000126 substance Substances 0.000 description 1
150000003445 sucroses Chemical class 0.000 description 1
238000001308 synthesis method Methods 0.000 description 1
238000005979 thermal decomposition reaction Methods 0.000 description 1
QPBYLOWPSRZOFX-UHFFFAOYSA-J tin(iv) iodide Chemical compound I[Sn](I)(I)I QPBYLOWPSRZOFX-UHFFFAOYSA-J 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

JP2137080A 1980-02-22 1980-02-22 Needle-like tin oxalate and its preparation Granted JPS56118037A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP2137080A JPS56118037A (en)	1980-02-22	1980-02-22	Needle-like tin oxalate and its preparation

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP2137080A JPS56118037A (en)	1980-02-22	1980-02-22	Needle-like tin oxalate and its preparation

Publications (2)

Publication Number	Publication Date
JPS56118037A JPS56118037A (en)	1981-09-16
JPS6310939B2 true JPS6310939B2 (fr)	1988-03-10

Family

ID=12053203

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2137080A Granted JPS56118037A (en)	1980-02-22	1980-02-22	Needle-like tin oxalate and its preparation

Country Status (1)

Country	Link
JP (1)	JPS56118037A (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AUPM402094A0 (en) *	1994-02-18	1994-03-17	University Of Sydney, The	Chemical compounds

1980
- 1980-02-22 JP JP2137080A patent/JPS56118037A/ja active Granted

Also Published As

Publication number	Publication date
JPS56118037A (en)	1981-09-16

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JPS6310939B2 (fr)	1988-03-10
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