JPS6324663B2 - - Google Patents

Info

Publication number
JPS6324663B2
JPS6324663B2 JP57155975A JP15597582A JPS6324663B2 JP S6324663 B2 JPS6324663 B2 JP S6324663B2 JP 57155975 A JP57155975 A JP 57155975A JP 15597582 A JP15597582 A JP 15597582A JP S6324663 B2 JPS6324663 B2 JP S6324663B2
Authority
JP
Japan
Prior art keywords
soy sauce
moromi
temperature
spore
heating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP57155975A
Other languages
Japanese (ja)
Other versions
JPS5945853A (en
Inventor
Tadao Arai
Hiroshi Motai
Shigeo Okada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kikkoman Corp
Original Assignee
Kikkoman Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kikkoman Corp filed Critical Kikkoman Corp
Priority to JP57155975A priority Critical patent/JPS5945853A/en
Publication of JPS5945853A publication Critical patent/JPS5945853A/en
Publication of JPS6324663B2 publication Critical patent/JPS6324663B2/ja
Granted legal-status Critical Current

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  • Soy Sauces And Products Related Thereto (AREA)

Description

【発明の詳細な説明】[Detailed description of the invention]

本発明は醤油の製造法に関し、その目的とする
ところは芽胞子細菌のほとんどもしくは全く存在
しない清澄な醤油を簡易な操作で効率良く得るこ
とにある。 通常市販醤油には、通常102〜105/mlのバチル
ス・ズブチリス等の芽胞子細菌が含まれており、
これらの芽胞子細菌は佃煮、漬物、酢の物等の加
工食品を製造する際、例えば食塩等が希釈される
と醤油原液中に残存する芽胞子細菌は発芽生育し
著しく醤油品質の劣下をきたす。 従つて、上記した加工食品に使用する醤油に対
しては、芽胞子細菌の除去が特に要求されてい
る。 そこで本発明者等は、上記現況に鑑み芽胞子細
菌の実質的に存在しない醤油の製造法に関し鉛意
検討した結果、醤油諸味を可及的急速に95℃以上
に昇温し、この温度で達温ないし20分間保時する
ことにより、諸味中に生存する芽胞子細菌等の微
生物をほとんどもしくは完全に死滅させることが
出来ること、更に上記加熱諸味を可及的急速に50
℃以下に冷却し、これを常法により圧搾すること
により、醤油粕と共に芽胞子細菌の微生物及び火
入〓の母体物質も効率良く圧搾除去される為、著
しく清澄度の良い製品醤油が得られること等の知
見を得、本発明を完成した。 即ち、本発明は、醤油諸味を可及的急速に95℃
以上に昇温し、この温度で達温ないし20分間保持
した後、これを可及的急速に50℃以下に冷却し、
常法により圧搾することを特徴とする醤油の製造
法である。 先ず本発明に用いられる醤油諸味としては、醤
油醸造諸味を少なくとも1部含む醤油諸味であれ
ばその種別を問わず使用出来る。 本発明を実施するに際しては、醤油諸味を出来
るだけ急速に95℃以上、特に好ましくは100〜125
℃の温度域に昇温する。 次いでこの温度範囲内で一定温度であるいは順
次高めるか、もしくは順次下げた温度で達温ない
し20分間、特に好ましくは達温ないし5分間保持
した後、可及的急速に50℃以下、好ましくは40℃
以下に冷却する。 醤油諸味を上記した温度及び時間保時すること
により、該諸味中の芽胞子細菌をほとんどもしく
は完全に死滅させ、かつ諸味中に存在する種々の
酵素群をほゞ確実に失活させ火入〓母体物質を破
壌する。 この際、可及的急速に95℃以上に諸味を昇温さ
せる手段としては、例えばかき取り式熱交換器、
二重管式熱交換器あるいはタンクの外壁に加熱蒸
気もしくは熱水を流す等の人為的操作により強制
的に加熱することを意味し、又可及的急速に50℃
以下に冷却する手段としては、例えばプレート式
熱交換器、二重管式熱交換器あるいはタンクの外
壁に強制的に冷却水を流す等の人為的操作により
強制的に冷却することを夫々意味し、これらの所
要時間は諸味温度、諸味容量等により多少異なる
がほぼ0.5時間以内に行なうのが望ましい。 上記可及的急速に加熱及び冷却する操作は、2
次〓の生成防止並びに過度な着色を抑え、製品の
品質劣下を防止する上で、本発明に於いては不可
欠な要件である。 前記加熱温度に対応して時間は、醸造諸味に含
まれるプロテアーゼの種類と量、火入〓母体蚤白
質量、醤油諸味中の窒素、食塩量、諸味PH等によ
り影響されるが、例えば95〜100℃で10〜20分間、
100〜105℃で10秒〜10分間、110℃で5秒〜5分
間、120℃で達温〜1分間、130℃で達温〜20秒間
等が好適な例として挙げられる。 上記した範囲外で、醤油諸味を加熱及び冷却処
理した場合には、芽胞子細菌のほとんどもしくは
全く存在しない清澄な醤油は得られず、又諸味圧
搾効率の改善も達成されない。 そして前記諸味を可及的急速に加熱及び冷却す
る操作は、開放状態で行なつてもよいが、該操作
を密閉状態で行なえば、エチルアルコール等の揮
発性芳香成分の飛散が防止され、又酸化増色も抑
えられる為有利となる。 次に前記冷却後の醤油諸味を常法により圧搾
し、醤油粕と同時に芽胞子細菌及び火入〓の母体
物質等を分離、除去する。 次いで得られた生揚醤油を、火入加熱及び〓引
を全く省略し、常法により清澄濾過、規格調整を
行なつて製品とするか、又は該生揚醤油を60〜
130℃で達温〜60分程度火入加熱し、次いで常法
により清澄濾過、規格調整して製品を得ても良
い。 上記した如く、本発明によれば芽胞子細菌のほ
とんどもしくは全く存在しない清澄な製品醤油を
短期間に効率良く得ることが出来、本発明は産業
上極めて有意義である。 以下実施例を挙げ、本発明を具体的に示す。 実施例 1試験区当り、濃口醸造諸味〔TN;1.73%、
NaCl;16.9%、Alc;2.8%、PH4.8、芽胞子細菌
数;2.0×104/ml(諸味液汁)〕5.0KLを、かき取
り式熱交換器(岩井機械工業株式会社製)を用い
て急速に密閉条件下で、第1表に示す如く83〜
130℃に昇温し、この温度で達温〜20分間保持し
た後、該加熱諸味を二重管式熱交換器で急速に30
℃に冷却し、次いで常法により諸味圧搾し生揚醤
油を得、これに濾過助剤として珪藻土を加えて清
澄濾過し製品醤油を夫々得た。 なお第1表中濁度の測定は、得られた製品を
UT−11型濁度計(コロナ電気株式会社製)で測
定した値である。
The present invention relates to a method for producing soy sauce, and its purpose is to efficiently obtain clear soy sauce containing little or no spore-forming bacteria through simple operations. Commercially available soy sauce usually contains 10 2 to 10 5 /ml of spore-forming bacteria such as Bacillus subtilis.
When these spore-spore bacteria are used to produce processed foods such as tsukudani, pickles, and vinegared foods, for example, when salt is diluted, the spore-spore bacteria remaining in the soy sauce stock solution germinate and grow, significantly deteriorating the quality of the soy sauce. Therefore, the soy sauce used in the above-mentioned processed foods is particularly required to remove spore bacteria. Therefore, in view of the above-mentioned current situation, the present inventors conducted a preliminary study on a method for producing soy sauce that does not substantially contain spore-forming bacteria, and as a result, the present inventors raised the temperature of soy sauce moromi to 95°C or higher as quickly as possible, and at this temperature. It is possible to almost or completely kill microorganisms such as spore bacteria that exist in the moromi by keeping it at temperature for 20 minutes, and furthermore, the above-mentioned heated moromi can be heated to 50% temperature as quickly as possible.
By cooling the soy sauce to below ℃ and squeezing it using a conventional method, the microorganisms of spore bacteria and the parent material of pasteurization are efficiently squeezed out along with the soy sauce lees, resulting in a product soy sauce with extremely high clarity. Based on these findings, the present invention was completed. That is, the present invention allows soy sauce moromi to be heated to 95°C as quickly as possible.
After raising the temperature to a temperature above or keeping it at this temperature for 20 minutes, cool it as quickly as possible to below 50℃,
This is a method for producing soy sauce, which is characterized by pressing it using a conventional method. First, as the soy sauce moromi used in the present invention, any type of soy sauce moromi can be used as long as it contains at least one part of soy sauce brewed moromi. When carrying out the present invention, the soy sauce moromi should be heated as rapidly as possible to above 95°C, particularly preferably at 100 to 125°C.
Raise the temperature to a temperature range of ℃. Next, within this temperature range, the temperature is maintained at a constant temperature or gradually increased or decreased for 20 minutes, particularly preferably for 5 minutes after reaching temperature, and then heated as quickly as possible to 50°C or less, preferably 40°C. ℃
Cool below. By keeping the soy sauce moromi at the above-mentioned temperature and time, the spore bacteria in the moromi are almost or completely killed, and the various enzyme groups present in the moromi are almost certainly inactivated. Destroys the parent material. At this time, as a means to raise the temperature of the moromi to 95°C or higher as rapidly as possible, for example, a scraping type heat exchanger,
It means forced heating by artificial operation such as flowing heated steam or hot water through a double pipe heat exchanger or the outer wall of a tank, and it also means heating to 50℃ as rapidly as possible.
The means of cooling below refers to forcible cooling by, for example, a plate heat exchanger, a double pipe heat exchanger, or artificial operation such as forcing cooling water to flow through the outer wall of a tank. The time required for these steps varies depending on the moromi temperature, moromi volume, etc., but it is desirable to carry out the process within approximately 0.5 hours. The above-mentioned operation of heating and cooling as rapidly as possible is performed in 2
This is an essential requirement in the present invention in order to prevent the formation of the following, excessive coloring, and deterioration of product quality. The time corresponding to the heating temperature is influenced by the type and amount of protease contained in the brewed moromi, the amount of fleas in the cooked mother, the nitrogen in the soy sauce moromi, the amount of salt, the pH of the moromi, etc. 10-20 minutes at 100℃
Preferred examples include 10 seconds to 10 minutes at 100 to 105°C, 5 seconds to 5 minutes at 110°C, 1 minute to reach temperature at 120°C, and 20 seconds to reach temperature at 130°C. If soy sauce moromi is heated and cooled outside the above-mentioned range, clear soy sauce containing little or no spore bacteria will not be obtained, nor will improvement in moromi compression efficiency be achieved. The operation of heating and cooling the moromi as rapidly as possible may be performed in an open state, but if the operation is performed in a closed state, scattering of volatile aromatic components such as ethyl alcohol is prevented, and This is advantageous because oxidative color addition can also be suppressed. Next, the cooled soy sauce moromi is pressed in a conventional manner to separate and remove the soy sauce lees as well as the spore-forming bacteria and the parent substance of the pasteurization. Next, the obtained raw fried soy sauce is made into a product by completely omitting heating, heating, and reduction, and is subjected to clarification and filtration and specification adjustment according to the usual method, or the raw fried soy sauce is made into a product by 60 to 60%
The product may be obtained by heating at 130°C for about 60 minutes until reaching the temperature, followed by clarification filtration and adjustment of specifications by a conventional method. As described above, according to the present invention, it is possible to efficiently obtain a clear product soy sauce containing little or no spore bacteria in a short period of time, and the present invention is extremely significant industrially. The present invention will be specifically illustrated with reference to Examples below. Example: Koikuchi Jozo Moromi [TN; 1.73%,
NaCl: 16.9%, Alc: 2.8%, PH4.8, number of spore bacteria: 2.0×10 4 /ml (moromi liquid)] 5.0 KL using a scraped heat exchanger (manufactured by Iwai Kikai Kogyo Co., Ltd.) under closed conditions, as shown in Table 1.
After raising the temperature to 130℃ and keeping it at this temperature for 20 minutes, the heated moromi was rapidly heated to 30℃ in a double tube heat exchanger.
The mixture was cooled to 0.degree. C. and then pressed with moromi in a conventional manner to obtain raw fried soy sauce. Diatomaceous earth was added as a filter aid to this and clarified and filtered to obtain product soy sauces. In addition, the turbidity measurement in Table 1 is based on the obtained product.
This is a value measured with a UT-11 turbidity meter (manufactured by Corona Electric Co., Ltd.).

【表】 第1表の結果より明らかな如く、本発明の諸味
加熱条件範囲で処理して得られる製品は、対照に
比し著しく芽胞子細菌数が少なく、しかも清澄度
も著しく優れたものである。
[Table] As is clear from the results in Table 1, the products obtained by processing the Moromi heating conditions of the present invention had a significantly lower number of spore bacteria than the control, and also had significantly superior clarity. be.

Claims (1)

【特許請求の範囲】 1 醤油諸味を可及的急速に95℃以上に昇温し、
この温度で達温ないし20分間保持した後、これを
可及的急速に50℃以下に冷却し、常法により圧搾
することを特徴とする醤油の製造法。 2 醤油諸味を、密閉条件下で昇温、加熱及び冷
却することを特徴とする特許請求の範囲第1項記
載の醤油の製造法。
[Claims] 1. Raising the temperature of soy sauce moromi to 95°C or higher as rapidly as possible,
A method for producing soy sauce, which comprises maintaining the soy sauce at this temperature for 20 minutes, cooling it as quickly as possible to 50°C or less, and squeezing it by a conventional method. 2. The method for producing soy sauce according to claim 1, which comprises heating, heating, and cooling soy sauce moromi under closed conditions.
JP57155975A 1982-09-09 1982-09-09 Preparation of soy sauce Granted JPS5945853A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP57155975A JPS5945853A (en) 1982-09-09 1982-09-09 Preparation of soy sauce

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP57155975A JPS5945853A (en) 1982-09-09 1982-09-09 Preparation of soy sauce

Publications (2)

Publication Number Publication Date
JPS5945853A JPS5945853A (en) 1984-03-14
JPS6324663B2 true JPS6324663B2 (en) 1988-05-21

Family

ID=15617620

Family Applications (1)

Application Number Title Priority Date Filing Date
JP57155975A Granted JPS5945853A (en) 1982-09-09 1982-09-09 Preparation of soy sauce

Country Status (1)

Country Link
JP (1) JPS5945853A (en)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5010957B2 (en) * 1972-02-23 1975-04-25

Also Published As

Publication number Publication date
JPS5945853A (en) 1984-03-14

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