LU84790A1 - Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore,leur procede de preparation et leur utilisation - Google Patents

Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore,leur procede de preparation et leur utilisation Download PDF

Info

Publication number: LU84790A1
Authority: LU; Luxembourg
Prior art keywords: chosen; crystalline; molar ratio; synthetic materials; cation
Prior art date: 1982-05-07

Application number

LU84790A

Other languages

English (en)

French (fr)

Inventor

Vittorio Fattore

Marco Taramasso

Giovanni Perego

Original Assignee

Snam Progetti

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-05-07

Filing date

1983-05-06

Publication date

1984-03-07

1983-05-06 Application filed by Snam Progetti filed Critical Snam Progetti

1984-03-07 Publication of LU84790A1 publication Critical patent/LU84790A1/fr

Links

229910052710 silicon Inorganic materials 0.000 title claims description 8
239000010703 silicon Substances 0.000 title claims description 8
238000002360 preparation method Methods 0.000 title description 7
239000000463 material Substances 0.000 title description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 23
229920002994 synthetic fiber Polymers 0.000 claims description 11
239000002585 base Substances 0.000 claims description 10
238000001228 spectrum Methods 0.000 claims description 10
150000001768 cations Chemical class 0.000 claims description 8
238000002441 X-ray diffraction Methods 0.000 claims description 7
239000000203 mixture Substances 0.000 claims description 6
150000001638 boron Chemical class 0.000 claims description 5
QEMXHQIAXOOASZ-UHFFFAOYSA-N tetramethylammonium Chemical compound C[N+](C)(C)C QEMXHQIAXOOASZ-UHFFFAOYSA-N 0.000 claims description 5
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 4
ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 4
229910052796 boron Inorganic materials 0.000 claims description 4
239000000908 ammonium hydroxide Substances 0.000 claims description 3
229910021538 borax Inorganic materials 0.000 claims description 3
KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 3
239000004327 boric acid Substances 0.000 claims description 3
239000003153 chemical reaction reagent Substances 0.000 claims description 3
239000004033 plastic Substances 0.000 claims description 3
229920003023 plastic Polymers 0.000 claims description 3
239000000376 reactant Substances 0.000 claims description 3
239000000377 silicon dioxide Substances 0.000 claims description 3
235000010339 sodium tetraborate Nutrition 0.000 claims description 3
DZLFLBLQUQXARW-UHFFFAOYSA-N tetrabutylammonium Chemical compound CCCC[N+](CCCC)(CCCC)CCCC DZLFLBLQUQXARW-UHFFFAOYSA-N 0.000 claims description 3
WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical class [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 claims description 3
229910002012 Aerosil® Inorganic materials 0.000 claims description 2
239000004115 Sodium Silicate Substances 0.000 claims description 2
229910052783 alkali metal Inorganic materials 0.000 claims description 2
150000001340 alkali metals Chemical class 0.000 claims description 2
IJRVQAXSAHHCNH-UHFFFAOYSA-M butyl(trimethyl)azanium;hydroxide Chemical group [OH-].CCCC[N+](C)(C)C IJRVQAXSAHHCNH-UHFFFAOYSA-M 0.000 claims description 2
229910002027 silica gel Inorganic materials 0.000 claims description 2
239000000741 silica gel Substances 0.000 claims description 2
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 2
229910052911 sodium silicate Inorganic materials 0.000 claims description 2
BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 claims description 2
QCOGKXLOEWLIDC-UHFFFAOYSA-O butyl(methyl)azanium Chemical compound CCCC[NH2+]C QCOGKXLOEWLIDC-UHFFFAOYSA-O 0.000 claims 3
JLMKXBLSZPRYPU-UHFFFAOYSA-N [OH-].C(CCC)[NH2+]C Chemical compound [OH-].C(CCC)[NH2+]C JLMKXBLSZPRYPU-UHFFFAOYSA-N 0.000 claims 1
150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
235000010338 boric acid Nutrition 0.000 claims 1
KFJNCGCKGILQMF-UHFFFAOYSA-M dibutyl(dimethyl)azanium;hydroxide Chemical group [OH-].CCCC[N+](C)(C)CCCC KFJNCGCKGILQMF-UHFFFAOYSA-M 0.000 claims 1
239000004328 sodium tetraborate Substances 0.000 claims 1
-1 tetraa lkylammonium cation Chemical class 0.000 claims 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 5
238000000034 method Methods 0.000 description 5
BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 2
239000005695 Ammonium acetate Substances 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
235000019257 ammonium acetate Nutrition 0.000 description 2
229940043376 ammonium acetate Drugs 0.000 description 2
235000011114 ammonium hydroxide Nutrition 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
239000008119 colloidal silica Substances 0.000 description 2
238000005342 ion exchange Methods 0.000 description 2
125000001453 quaternary ammonium group Chemical group 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
125000005207 tetraalkylammonium group Chemical group 0.000 description 2
CBXCPBUEXACCNR-UHFFFAOYSA-N tetraethylammonium Chemical compound CC[N+](CC)(CC)CC CBXCPBUEXACCNR-UHFFFAOYSA-N 0.000 description 2
RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
241000984642 Cura Species 0.000 description 1
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
229910001413 alkali metal ion Inorganic materials 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
229910052810 boron oxide Inorganic materials 0.000 description 1
150000001642 boronic acid derivatives Chemical class 0.000 description 1
238000001354 calcination Methods 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000004927 clay Substances 0.000 description 1
229910052570 clay Inorganic materials 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000001816 cooling Methods 0.000 description 1
239000013256 coordination polymer Substances 0.000 description 1
JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000000499 gel Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
239000012535 impurity Substances 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000005297 pyrex Substances 0.000 description 1
230000005855 radiation Effects 0.000 description 1
229910052814 silicon oxide Inorganic materials 0.000 description 1
239000011734 sodium Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000000758 substrate Substances 0.000 description 1
VDZOOKBUILJEDG-UHFFFAOYSA-M tetrabutylammonium hydroxide Chemical class [OH-].CCCC[N+](CCCC)(CCCC)CCCC VDZOOKBUILJEDG-UHFFFAOYSA-M 0.000 description 1
LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
OSBSFAARYOCBHB-UHFFFAOYSA-N tetrapropylammonium Chemical compound CCC[N+](CCC)(CCC)CCC OSBSFAARYOCBHB-UHFFFAOYSA-N 0.000 description 1
FYFNFZLMMGXBMT-UHFFFAOYSA-M tributyl(ethyl)azanium;hydroxide Chemical compound [OH-].CCCC[N+](CC)(CCCC)CCCC FYFNFZLMMGXBMT-UHFFFAOYSA-M 0.000 description 1
QVOFCQBZXGLNAA-UHFFFAOYSA-M tributyl(methyl)azanium;hydroxide Chemical compound [OH-].CCCC[N+](C)(CCCC)CCCC QVOFCQBZXGLNAA-UHFFFAOYSA-M 0.000 description 1
230000003313 weakening effect Effects 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
- C01B35/10—Compounds containing boron and oxygen
- C01B35/1009—Compounds containing boron and oxygen having molecular-sieve properties
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/10—Compounds containing silicon, fluorine, and other elements

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)
Catalysts (AREA)
Silicon Compounds (AREA)
Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)

LU84790A 1982-05-07 1983-05-06 Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore,leur procede de preparation et leur utilisation LU84790A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
IT21132/82A IT1157932B (it)	1982-05-07	1982-05-07	Materiali sintetici, cristallini, porosi costituiti da ossidi di silicio e boro, loro metodo di preparazione e loro usi
IT2113282		1982-05-07

Publications (1)

Publication Number	Publication Date
LU84790A1 true LU84790A1 (fr)	1984-03-07

Family

ID=11177209

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU84790A LU84790A1 (fr)	1982-05-07	1983-05-06	Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore,leur procede de preparation et leur utilisation

Country Status (23)

Country	Link
JP (1)	JPS58208129A (de)
KR (1)	KR840004534A (de)
AU (1)	AU1383983A (de)
BE (1)	BE896686A (de)
BR (1)	BR8302358A (de)
DD (1)	DD209795A5 (de)
DE (1)	DE3316488A1 (de)
DK (1)	DK195883A (de)
ES (1)	ES522608A0 (de)
FR (1)	FR2526414A1 (de)
GB (1)	GB2120226B (de)
GR (1)	GR78258B (de)
IL (1)	IL68543A0 (de)
IT (1)	IT1157932B (de)
LU (1)	LU84790A1 (de)
NL (1)	NL8301590A (de)
NO (1)	NO831584L (de)
PL (1)	PL241838A1 (de)
PT (1)	PT76656B (de)
SE (1)	SE8302576L (de)
YU (1)	YU95483A (de)
ZA (1)	ZA832934B (de)
ZW (1)	ZW9183A1 (de)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2582639B1 (fr) *	1985-05-28	1987-08-28	Centre Nat Rech Scient	Nouveau procede de synthese de zeolites du type borosilicate, produits ainsi obtenus et leur utilisation
IT1213504B (it)	1986-10-22	1989-12-20	Eniricerche Spa	Zeoliti legate e procedimenye per la loro prosuzione.
AU634962B2 (en) *	1988-06-10	1993-03-11	Kohmix Co., Ltd.	Water-Soluble, film-forming inorganic compounds

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
IN146957B (de) *	1976-10-18	1979-10-20	Standard Oil Co
GR66589B (de) *	1978-06-22	1981-03-30	Snam Progetti
US4331641A (en) *	1979-11-07	1982-05-25	National Distillers & Chemical Corp.	Synthetic crystalline metal silicate compositions and preparation thereof

1982
- 1982-05-07 IT IT21132/82A patent/IT1157932B/it active
1983
- 1983-04-11 GR GR71163A patent/GR78258B/el unknown
- 1983-04-21 AU AU13839/83A patent/AU1383983A/en not_active Abandoned
- 1983-04-22 ZW ZW91/83A patent/ZW9183A1/xx unknown
- 1983-04-26 ZA ZA832934A patent/ZA832934B/xx unknown
- 1983-04-26 GB GB08311310A patent/GB2120226B/en not_active Expired
- 1983-04-27 YU YU00954/83A patent/YU95483A/xx unknown
- 1983-05-01 IL IL68543A patent/IL68543A0/xx unknown
- 1983-05-03 BR BR8302358A patent/BR8302358A/pt unknown
- 1983-05-03 DK DK195883A patent/DK195883A/da not_active Application Discontinuation
- 1983-05-04 NL NL8301590A patent/NL8301590A/nl not_active Application Discontinuation
- 1983-05-05 NO NO831584A patent/NO831584L/no unknown
- 1983-05-05 FR FR8307488A patent/FR2526414A1/fr active Granted
- 1983-05-05 DE DE19833316488 patent/DE3316488A1/de not_active Ceased
- 1983-05-05 SE SE8302576A patent/SE8302576L/ not_active Application Discontinuation
- 1983-05-06 JP JP58078389A patent/JPS58208129A/ja active Pending
- 1983-05-06 PT PT76656A patent/PT76656B/pt unknown
- 1983-05-06 ES ES522608A patent/ES522608A0/es active Granted
- 1983-05-06 DD DD83250710A patent/DD209795A5/de unknown
- 1983-05-06 LU LU84790A patent/LU84790A1/fr unknown
- 1983-05-06 PL PL24183883A patent/PL241838A1/xx unknown
- 1983-05-06 BE BE0/210720A patent/BE896686A/fr not_active IP Right Cessation
- 1983-05-07 KR KR1019830001960A patent/KR840004534A/ko not_active Ceased

Also Published As

Publication number	Publication date
PT76656B (en)	1986-04-16
YU95483A (en)	1985-10-31
PL241838A1 (en)	1984-06-18
FR2526414B1 (de)	1985-04-19
SE8302576D0 (sv)	1983-05-05
SE8302576L (sv)	1983-11-08
ZW9183A1 (en)	1983-07-20
IL68543A0 (en)	1983-09-30
DK195883A (da)	1983-11-08
KR840004534A (ko)	1984-10-22
ES8406380A1 (es)	1984-08-01
DD209795A5 (de)	1984-05-23
JPS58208129A (ja)	1983-12-03
AU1383983A (en)	1983-11-10
FR2526414A1 (fr)	1983-11-10
GR78258B (de)	1984-09-26
PT76656A (en)	1983-06-01
GB2120226A (en)	1983-11-30
DE3316488A1 (de)	1983-11-10
BR8302358A (pt)	1984-01-10
IT8221132A0 (it)	1982-05-07
IT1157932B (it)	1987-02-18
DK195883D0 (da)	1983-05-03
ES522608A0 (es)	1984-08-01
NO831584L (no)	1983-11-08
GB8311310D0 (en)	1983-06-02
NL8301590A (nl)	1983-12-01
GB2120226B (en)	1985-10-23
ZA832934B (en)	1984-04-25
BE896686A (fr)	1983-11-07

Publication	Publication Date	Title
Chao et al.	1981	Kinetic studies on the formation of zeolite ZSM-5
EP0419334B1 (de)	1994-01-05	Zeolith vom beta-Typ sowie Verfahren zu seiner Herstellung
FR2882744A1 (fr)	2006-09-08	Solide cristallise cok-7, procede de preparation et utilisation pour la transformation d'hydrocarbures
EP0172068A1 (de)	1986-02-19	Verfahren zur Synthese von Zeolithen vom Alumosilikat-Typ, durch dieses Verfahren erzeugte Produkte sowie deren Verwendung
LU83204A1 (fr)	1981-10-30	Procede pour la preparation de silicates d'aluminium ayant une structure du genre zeolite
EP3801893A1 (de)	2021-04-14	Verfahren zur synthese eines zeolithen mit afx-struktur mit sehr hoher reinheit in gegenwart eines organischen stickstoffhaltigen strukturierungsmittels
EP0517891A1 (de)	1992-12-16	Zeolith vom mfi-typ sowie verfahren zu seiner herstellung.
FR2924110A1 (fr)	2009-05-29	Solide cristallise izm-3 et son procede de preparation
EP0516801A1 (de)	1992-12-09	Zeolith vom mtw-typ sowie verfahren zu seiner herstellung.
US4495371A (en)	1985-01-22	Process for isomerizing styrene oxide or homologues to β-phenylaldehydes
WO2019224087A1 (fr)	2019-11-28	Procede de preparation d'une zeolithe de type structural afx par synthese en presence d'un structurant organique azote
EP0264744A2 (de)	1988-04-27	Verfahren zur Herstellung von 4,4' Diaminodiphenylmethan und Derivaten davon
Qisheng et al.	1988	First syntheses of pentasil-type silica zeolites from non-aqueous systems
EP3798189B1 (de)	2022-04-20	Syntheseverfahren von izm-2-zeolith in gegenwart eines stickstoffhaltigen organischen strukturbildners in der hydroxidform und eines alkalimetallchlorids, in einem fluorierten oder nicht fluorierten medium
EP1510501B1 (de)	2011-09-14	IM-11 kristalliner Festkörper des Strukturtyps LTA und Verfahren zu seiner Herstellung
EP0345106B1 (de)	1993-09-29	Zeolithe mit dem Strukturtyp von Ton, ihre Herstellung und ihre Verwendung
EP0347273B1 (de)	1993-09-29	Verfahren zur Synthese von Zeolithen vom MTT-Strukturtyp
FR2472538A1 (fr)	1981-07-03	Procede de production de zeolithes cristallines
US5241119A (en)	1993-08-31	Process for the preparation of 4,4'-diaminodiphenyl-methane and its derivatives
FR2526414A1 (fr)	1983-11-10	Matieres synthetiques cristallines et poreuses constituees par des oxydes de silicium et de bore, leur procede de preparation et leur utilisation
EP3801892A1 (de)	2021-04-14	Verfahren zur herstellung eines hochreinen afx-strukturzeoliths mit einem stickstoffhaltigen organischen strukturierungsmittel
EP0427579B1 (de)	1995-05-24	Zeolith vom Mordenit-Typ und Verfahren zu seiner Herstellung
EP0224531B1 (de)	1988-12-28	Fluorhaltige zeolithe vom borosilikattyp
WO2023066715A1 (fr)	2023-04-27	Procédé de préparation de zéolithe fau en présence d'un structurant hydroxyde de tétraéthylammonium teaoh
EP0437989B1 (de)	1994-03-09	Zeolith vom Levyn-Typ sowie Verfahren zu dessen Herstellung