LU86148A1 - Peintures primaires - Google Patents

Peintures primaires Download PDF

Info

Publication number: LU86148A1
Authority: LU; Luxembourg
Prior art keywords: resin; composition according; phenolic resin; polyisocyanate; chosen
Prior art date: 1985-10-31

Application number

LU86148A

Other languages

English (en)

French (fr)

Inventor

Paul Vranken

Jozef Brabken

Original Assignee

Labofina Sa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-10-31

Filing date

1985-10-31

Publication date

1987-06-02

1985-10-31 Application filed by Labofina Sa filed Critical Labofina Sa

1985-10-31 Priority to LU86148A priority Critical patent/LU86148A1/fr

1986-10-28 Priority to DE8686870158T priority patent/DE3684664D1/de

1986-10-28 Priority to ES198686870158T priority patent/ES2030670T3/es

1986-10-28 Priority to EP86870158A priority patent/EP0221877B1/de

1986-10-28 Priority to AT86870158T priority patent/ATE74373T1/de

1987-06-02 Publication of LU86148A1 publication Critical patent/LU86148A1/fr

Links

239000003973 paint Substances 0.000 title claims abstract description 60
229920005989 resin Polymers 0.000 claims abstract description 40
239000011347 resin Substances 0.000 claims abstract description 40
239000000203 mixture Substances 0.000 claims abstract description 35
229920001568 phenolic resin Polymers 0.000 claims abstract description 23
239000005011 phenolic resin Substances 0.000 claims abstract description 22
KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 21
125000004432 carbon atom Chemical group C* 0.000 claims abstract description 11
239000000113 methacrylic resin Substances 0.000 claims abstract description 10
239000005056 polyisocyanate Substances 0.000 claims description 30
229920001228 polyisocyanate Polymers 0.000 claims description 30
239000011230 binding agent Substances 0.000 claims description 13
-1 alkyl methacrylate Chemical compound 0.000 claims description 9
239000003054 catalyst Substances 0.000 claims description 9
SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 claims description 6
239000005058 Isophorone diisocyanate Substances 0.000 claims description 6
VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 5
229920001577 copolymer Polymers 0.000 claims description 5
JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims description 4
NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 4
PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 claims description 4
230000015572 biosynthetic process Effects 0.000 claims description 3
239000004814 polyurethane Substances 0.000 claims description 3
VZXPHDGHQXLXJC-UHFFFAOYSA-N 1,6-diisocyanato-5,6-dimethylheptane Chemical compound O=C=NC(C)(C)C(C)CCCCN=C=O VZXPHDGHQXLXJC-UHFFFAOYSA-N 0.000 claims description 2
RUMACXVDVNRZJZ-UHFFFAOYSA-N 2-methylpropyl 2-methylprop-2-enoate Chemical compound CC(C)COC(=O)C(C)=C RUMACXVDVNRZJZ-UHFFFAOYSA-N 0.000 claims description 2
JJLKTTCRRLHVGL-UHFFFAOYSA-L [acetyloxy(dibutyl)stannyl] acetate Chemical compound CC([O-])=O.CC([O-])=O.CCCC[Sn+2]CCCC JJLKTTCRRLHVGL-UHFFFAOYSA-L 0.000 claims description 2
XKILITIYNKWIPW-UHFFFAOYSA-L [dibutyl(8-methylnonanoyloxy)stannyl] 8-methylnonanoate Chemical compound CC(C)CCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCC(C)C XKILITIYNKWIPW-UHFFFAOYSA-L 0.000 claims description 2
UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 2
AWFFJJAOMMAGFE-BGSQTJHASA-L [dibutyl-[(z)-octadec-9-enoyl]oxystannyl] (z)-octadec-9-enoate Chemical compound CCCC[Sn+2]CCCC.CCCCCCCC\C=C/CCCCCCCC([O-])=O.CCCCCCCC\C=C/CCCCCCCC([O-])=O AWFFJJAOMMAGFE-BGSQTJHASA-L 0.000 claims description 2
239000000539 dimer Substances 0.000 claims description 2
RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims description 2
239000000178 monomer Substances 0.000 claims description 2
229920002635 polyurethane Polymers 0.000 claims description 2
DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 2
239000013638 trimer Substances 0.000 claims description 2
239000005057 Hexamethylene diisocyanate Substances 0.000 claims 1
WCRDXYSYPCEIAK-UHFFFAOYSA-N dibutylstannane Chemical compound CCCC[SnH2]CCCC WCRDXYSYPCEIAK-UHFFFAOYSA-N 0.000 claims 1
KIQKWYUGPPFMBV-UHFFFAOYSA-N diisocyanatomethane Chemical compound O=C=NCN=C=O KIQKWYUGPPFMBV-UHFFFAOYSA-N 0.000 claims 1
229920000642 polymer Polymers 0.000 claims 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 abstract description 24
229920002554 vinyl polymer Polymers 0.000 abstract description 24
239000006185 dispersion Substances 0.000 abstract description 21
229910052751 metal Inorganic materials 0.000 abstract description 12
239000002184 metal Substances 0.000 abstract description 12
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 abstract description 3
239000004999 plastisol Substances 0.000 description 29
229920001944 Plastisol Polymers 0.000 description 28
239000002904 solvent Substances 0.000 description 10
239000000049 pigment Substances 0.000 description 7
239000004014 plasticizer Substances 0.000 description 7
238000000034 method Methods 0.000 description 6
229910001335 Galvanized steel Inorganic materials 0.000 description 5
239000008397 galvanized steel Substances 0.000 description 5
238000000576 coating method Methods 0.000 description 4
SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 description 4
239000000463 material Substances 0.000 description 4
239000002245 particle Substances 0.000 description 4
229920003229 poly(methyl methacrylate) Polymers 0.000 description 4
239000004926 polymethyl methacrylate Substances 0.000 description 4
239000004800 polyvinyl chloride Substances 0.000 description 4
229920000915 polyvinyl chloride Polymers 0.000 description 4
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
239000004925 Acrylic resin Substances 0.000 description 3
229920000178 Acrylic resin Polymers 0.000 description 3
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
239000004927 clay Substances 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000005007 epoxy-phenolic resin Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
125000005395 methacrylic acid group Chemical group 0.000 description 3
229920001169 thermoplastic Polymers 0.000 description 3
239000004416 thermosoftening plastic Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
239000000654 additive Substances 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
239000003822 epoxy resin Substances 0.000 description 2
JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 description 2
239000006224 matting agent Substances 0.000 description 2
239000007769 metal material Substances 0.000 description 2
238000010422 painting Methods 0.000 description 2
235000011837 pasties Nutrition 0.000 description 2
229920000647 polyepoxide Polymers 0.000 description 2
229920005862 polyol Polymers 0.000 description 2
150000003077 polyols Chemical class 0.000 description 2
150000003254 radicals Chemical class 0.000 description 2
NVKTUNLPFJHLCG-UHFFFAOYSA-N strontium chromate Chemical compound [Sr+2].[O-][Cr]([O-])(=O)=O NVKTUNLPFJHLCG-UHFFFAOYSA-N 0.000 description 2
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
PTTPXKJBFFKCEK-UHFFFAOYSA-N 2-Methyl-4-heptanone Chemical compound CC(C)CC(=O)CC(C)C PTTPXKJBFFKCEK-UHFFFAOYSA-N 0.000 description 1
ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 1
ATVJXMYDOSMEPO-UHFFFAOYSA-N 3-prop-2-enoxyprop-1-ene Chemical compound C=CCOCC=C ATVJXMYDOSMEPO-UHFFFAOYSA-N 0.000 description 1
UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 description 1
DWZBSOVYCROKJR-UHFFFAOYSA-N 4-(2-methylphenyl)butan-1-ol Chemical compound CC1=CC=CC=C1CCCCO DWZBSOVYCROKJR-UHFFFAOYSA-N 0.000 description 1
NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 1
UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
YVHDRFKHKGNLNW-UHFFFAOYSA-L [dibutyl(octadecanoyloxy)stannyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCCCCCCCC YVHDRFKHKGNLNW-UHFFFAOYSA-L 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
239000002981 blocking agent Substances 0.000 description 1
210000000988 bone and bone Anatomy 0.000 description 1
ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
229910017052 cobalt Inorganic materials 0.000 description 1
239000010941 cobalt Substances 0.000 description 1
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000000470 constituent Substances 0.000 description 1
238000010411 cooking Methods 0.000 description 1
230000007797 corrosion Effects 0.000 description 1
238000005260 corrosion Methods 0.000 description 1
230000001627 detrimental effect Effects 0.000 description 1
JGFBRKRYDCGYKD-UHFFFAOYSA-N dibutyl(oxo)tin Chemical compound CCCC[Sn](=O)CCCC JGFBRKRYDCGYKD-UHFFFAOYSA-N 0.000 description 1
239000003085 diluting agent Substances 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
238000010304 firing Methods 0.000 description 1
230000004927 fusion Effects 0.000 description 1
LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
CBOIHMRHGLHBPB-UHFFFAOYSA-N hydroxymethyl Chemical compound O[CH2] CBOIHMRHGLHBPB-UHFFFAOYSA-N 0.000 description 1
IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 description 1
ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
239000011133 lead Substances 0.000 description 1
238000002844 melting Methods 0.000 description 1
230000008018 melting Effects 0.000 description 1
229910044991 metal oxide Inorganic materials 0.000 description 1
150000004706 metal oxides Chemical class 0.000 description 1
238000002156 mixing Methods 0.000 description 1
125000005609 naphthenate group Chemical group 0.000 description 1
125000005474 octanoate group Chemical group 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
239000005022 packaging material Substances 0.000 description 1
229920000768 polyamine Polymers 0.000 description 1
239000004848 polyfunctional curative Substances 0.000 description 1
102200073741 rs121909602 Human genes 0.000 description 1
CQRYARSYNCAZFO-UHFFFAOYSA-N salicyl alcohol Chemical compound OCC1=CC=CC=C1O CQRYARSYNCAZFO-UHFFFAOYSA-N 0.000 description 1
238000000926 separation method Methods 0.000 description 1
230000007928 solubilization Effects 0.000 description 1
238000005063 solubilization Methods 0.000 description 1
239000011877 solvent mixture Substances 0.000 description 1
238000010998 test method Methods 0.000 description 1
229920001187 thermosetting polymer Polymers 0.000 description 1
238000005829 trimerization reaction Methods 0.000 description 1
239000008096 xylene Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011701 zinc Substances 0.000 description 1
239000011787 zinc oxide Substances 0.000 description 1
LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
229910000165 zinc phosphate Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
- C09D161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09D161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L61/00—Compositions of condensation polymers of aldehydes or ketones; Compositions of derivatives of such polymers
- C08L61/04—Condensation polymers of aldehydes or ketones with phenols only
- C08L61/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Paints Or Removers (AREA)
Laminated Bodies (AREA)
Adhesives Or Adhesive Processes (AREA)
Formation Of Insulating Films (AREA)
Application Of Or Painting With Fluid Materials (AREA)
Materials For Medical Uses (AREA)

LU86148A 1985-10-31 1985-10-31 Peintures primaires LU86148A1 (fr)

Priority Applications (5)

Application Number	Priority Date	Filing Date	Title
LU86148A LU86148A1 (fr)	1985-10-31	1985-10-31	Peintures primaires
DE8686870158T DE3684664D1 (de)	1985-10-31	1986-10-28	Grundschichtueberzuege.
ES198686870158T ES2030670T3 (es)	1985-10-31	1986-10-28	Pinturas primarias.
EP86870158A EP0221877B1 (de)	1985-10-31	1986-10-28	Grundschichtüberzüge
AT86870158T ATE74373T1 (de)	1985-10-31	1986-10-28	Grundschichtueberzuege.

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
LU86148A LU86148A1 (fr)	1985-10-31	1985-10-31	Peintures primaires
LU86148		1985-10-31

Publications (1)

Publication Number	Publication Date
LU86148A1 true LU86148A1 (fr)	1987-06-02

Family

ID=19730577

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU86148A LU86148A1 (fr)	1985-10-31	1985-10-31	Peintures primaires

Country Status (5)

Country	Link
EP (1)	EP0221877B1 (de)
AT (1)	ATE74373T1 (de)
DE (1)	DE3684664D1 (de)
ES (1)	ES2030670T3 (de)
LU (1)	LU86148A1 (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP1081199A1 (de) *	1999-09-06	2001-03-07	Dsm N.V.	Zusammensetzung

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3216848A (en) *	1962-01-12	1965-11-09	Pittsburgh Plate Glass Co	Primer for vinyl dispersion coatings

1985
- 1985-10-31 LU LU86148A patent/LU86148A1/fr unknown
1986
- 1986-10-28 AT AT86870158T patent/ATE74373T1/de not_active IP Right Cessation
- 1986-10-28 EP EP86870158A patent/EP0221877B1/de not_active Expired - Lifetime
- 1986-10-28 DE DE8686870158T patent/DE3684664D1/de not_active Expired - Lifetime
- 1986-10-28 ES ES198686870158T patent/ES2030670T3/es not_active Expired - Lifetime

Also Published As

Publication number	Publication date
ATE74373T1 (de)	1992-04-15
ES2030670T3 (es)	1992-11-16
EP0221877A3 (en)	1988-11-30
EP0221877B1 (de)	1992-04-01
DE3684664D1 (de)	1992-05-07
EP0221877A2 (de)	1987-05-13

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