LU87685A1 - Procede et appareil pour mesurer la surface specifique non poreuse du noir de carbone - Google Patents

Procede et appareil pour mesurer la surface specifique non poreuse du noir de carbone Download PDF

Info

Publication number: LU87685A1
Authority: LU; Luxembourg
Prior art keywords: carbon black; filtrate; cetyltrimethylammonium bromide; dispersion; filter
Prior art date: 1989-05-19

Application number

LU87685A

Other languages

English (en)

French (fr)

Inventor

Daniel R Sanders

Original Assignee

Cabot Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-05-19

Filing date

1990-02-23

Publication date

1990-07-24

1990-02-23 Application filed by Cabot Corp filed Critical Cabot Corp

1990-07-24 Publication of LU87685A1 publication Critical patent/LU87685A1/fr

Links

239000006229 carbon black Substances 0.000 title claims description 56
238000000034 method Methods 0.000 title claims description 37
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title 1
LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 75
239000000706 filtrate Substances 0.000 claims description 32
239000000243 solution Substances 0.000 claims description 30
239000006185 dispersion Substances 0.000 claims description 28
238000005259 measurement Methods 0.000 claims description 17
238000004128 high performance liquid chromatography Methods 0.000 claims description 12
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 7
239000012088 reference solution Substances 0.000 claims description 5
229910052799 carbon Inorganic materials 0.000 claims description 4
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 claims 1
238000004811 liquid chromatography Methods 0.000 claims 1
238000001507 sample dispersion Methods 0.000 claims 1
235000019241 carbon black Nutrition 0.000 description 44
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 24
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 23
238000004458 analytical method Methods 0.000 description 16
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 15
229910052740 iodine Inorganic materials 0.000 description 15
239000011630 iodine Substances 0.000 description 15
238000012360 testing method Methods 0.000 description 10
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 9
229910052757 nitrogen Inorganic materials 0.000 description 9
239000004809 Teflon Substances 0.000 description 6
229920006362 Teflon® Polymers 0.000 description 6
239000007789 gas Substances 0.000 description 6
229910001873 dinitrogen Inorganic materials 0.000 description 5
238000005070 sampling Methods 0.000 description 5
238000001179 sorption measurement Methods 0.000 description 5
239000012153 distilled water Substances 0.000 description 4
238000001914 filtration Methods 0.000 description 4
238000002347 injection Methods 0.000 description 4
239000007924 injection Substances 0.000 description 4
239000003153 chemical reaction reagent Substances 0.000 description 3
239000000470 constituent Substances 0.000 description 3
230000000875 corresponding effect Effects 0.000 description 3
239000011521 glass Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000011148 porous material Substances 0.000 description 3
239000000843 powder Substances 0.000 description 3
229910001220 stainless steel Inorganic materials 0.000 description 3
239000010935 stainless steel Substances 0.000 description 3
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
238000013019 agitation Methods 0.000 description 2
229910052802 copper Inorganic materials 0.000 description 2
239000010949 copper Substances 0.000 description 2
230000002596 correlated effect Effects 0.000 description 2
239000004744 fabric Substances 0.000 description 2
239000012535 impurity Substances 0.000 description 2
PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 2
238000011068 loading method Methods 0.000 description 2
239000000463 material Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
239000004033 plastic Substances 0.000 description 2
229920003023 plastic Polymers 0.000 description 2
-1 polyethylene Polymers 0.000 description 2
238000003825 pressing Methods 0.000 description 2
238000012545 processing Methods 0.000 description 2
239000000047 product Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000001228 spectrum Methods 0.000 description 2
238000003756 stirring Methods 0.000 description 2
238000012799 strong cation exchange Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
238000009210 therapy by ultrasound Methods 0.000 description 2
239000002699 waste material Substances 0.000 description 2
239000004677 Nylon Substances 0.000 description 1
229920002302 Nylon 6,6 Polymers 0.000 description 1
239000002033 PVDF binder Substances 0.000 description 1
239000004698 Polyethylene Substances 0.000 description 1
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
238000009825 accumulation Methods 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
238000003556 assay Methods 0.000 description 1
238000011088 calibration curve Methods 0.000 description 1
238000002788 crimping Methods 0.000 description 1
AAOVKJBEBIDNHE-UHFFFAOYSA-N diazepam Chemical group N=1CC(=O)N(C)C2=CC=C(Cl)C=C2C=1C1=CC=CC=C1 AAOVKJBEBIDNHE-UHFFFAOYSA-N 0.000 description 1
238000007599 discharging Methods 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
238000009826 distribution Methods 0.000 description 1
238000010828 elution Methods 0.000 description 1
238000011067 equilibration Methods 0.000 description 1
230000003203 everyday effect Effects 0.000 description 1
239000012530 fluid Substances 0.000 description 1
238000000892 gravimetry Methods 0.000 description 1
230000005484 gravity Effects 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
150000002605 large molecules Chemical class 0.000 description 1
238000012417 linear regression Methods 0.000 description 1
229920002521 macromolecule Polymers 0.000 description 1
239000012528 membrane Substances 0.000 description 1
238000002156 mixing Methods 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
238000012544 monitoring process Methods 0.000 description 1
229920001778 nylon Polymers 0.000 description 1
229920000573 polyethylene Polymers 0.000 description 1
239000004800 polyvinyl chloride Substances 0.000 description 1
229920000915 polyvinyl chloride Polymers 0.000 description 1
229920002981 polyvinylidene fluoride Polymers 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
230000002787 reinforcement Effects 0.000 description 1
229920002379 silicone rubber Polymers 0.000 description 1
239000004945 silicone rubber Substances 0.000 description 1
LXMSZDCAJNLERA-ZHYRCANASA-N spironolactone Chemical compound C([C@@H]1[C@]2(C)CC[C@@H]3[C@@]4(C)CCC(=O)C=C4C[C@H]([C@@H]13)SC(=O)C)C[C@@]21CCC(=O)O1 LXMSZDCAJNLERA-ZHYRCANASA-N 0.000 description 1
125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
239000006228 supernatant Substances 0.000 description 1
238000012546 transfer Methods 0.000 description 1
238000004506 ultrasonic cleaning Methods 0.000 description 1
238000002604 ultrasonography Methods 0.000 description 1
238000013022 venting Methods 0.000 description 1
238000005303 weighing Methods 0.000 description 1

Classifications

- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/088—Investigating volume, surface area, size or distribution of pores; Porosimetry
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/36—Control of physical parameters of the fluid carrier in high pressure liquid systems
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/74—Optical detectors
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/17—Nitrogen containing
- Y10T436/173845—Amine and quaternary ammonium
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/23—Carbon containing

Landscapes

Chemical & Material Sciences (AREA)
Immunology (AREA)
Health & Medical Sciences (AREA)
Analytical Chemistry (AREA)
Biochemistry (AREA)
General Health & Medical Sciences (AREA)
General Physics & Mathematics (AREA)
Physics & Mathematics (AREA)
Life Sciences & Earth Sciences (AREA)
Pathology (AREA)
Dispersion Chemistry (AREA)
Sampling And Sample Adjustment (AREA)
Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Peptides Or Proteins (AREA)
Pigments, Carbon Blacks, Or Wood Stains (AREA)
Battery Electrode And Active Subsutance (AREA)
Investigating Or Analysing Biological Materials (AREA)

LU87685A 1989-05-19 1990-02-23 Procede et appareil pour mesurer la surface specifique non poreuse du noir de carbone LU87685A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US35392889A	1989-05-19	1989-05-19
US07/423,693 US4970169A (en)	1989-05-19	1989-10-12	Method for measuring non-porous surface area of carbon black

Publications (1)

Publication Number	Publication Date
LU87685A1 true LU87685A1 (fr)	1990-07-24

Family

ID=26998155

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
LU87685A LU87685A1 (fr)	1989-05-19	1990-02-23	Procede et appareil pour mesurer la surface specifique non poreuse du noir de carbone

Country Status (24)

Country	Link
US (1)	US4970169A (de)
JP (1)	JPH0321848A (de)
KR (1)	KR940002497B1 (de)
CN (1)	CN1047388A (de)
AU (1)	AU5117190A (de)
BR (1)	BR9000997A (de)
CA (1)	CA2009703A1 (de)
DD (1)	DD299982A5 (de)
DE (1)	DE4005085A1 (de)
DK (1)	DK33390A (de)
ES (1)	ES2019531A6 (de)
FR (1)	FR2647216B1 (de)
GB (2)	GB9003397D0 (de)
HU (1)	HUT55541A (de)
IL (1)	IL93332A0 (de)
IT (1)	IT1240313B (de)
LU (1)	LU87685A1 (de)
MY (1)	MY105234A (de)
NL (1)	NL9000332A (de)
NZ (1)	NZ232447A (de)
PE (1)	PE14191A1 (de)
PT (1)	PT93120A (de)
SE (1)	SE9001175L (de)
YU (1)	YU33390A (de)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5161407A (en) *	1990-10-16	1992-11-10	Iowa State University Research Foundation, Inc.	Means and method of soil water desorption
US5431821A (en) *	1992-02-07	1995-07-11	The Ohio State University	Glassy carbon in separation processes
JP2000070395A (ja) *	1998-04-16	2000-03-07	Shigeru Ando	類焼防止シ―ト、類焼防止カバ―、消火シ―ト兼防災用被服
CN201687022U (zh)	2009-10-20	2010-12-29	株式会社小松制作所	铲斗及作业车辆
US8733152B2 (en) *	2010-01-19	2014-05-27	Bio-Rad Laboratories, Inc.	Automated analyzer with low-pressure in-line filtration
CN109269449B (zh) *	2018-10-12	2020-07-31	重庆大学	堆石料比表面积测试方法

1989
- 1989-10-12 US US07/423,693 patent/US4970169A/en not_active Expired - Fee Related
1990
- 1990-02-08 DK DK033390A patent/DK33390A/da not_active Application Discontinuation
- 1990-02-09 CA CA002009703A patent/CA2009703A1/en not_active Abandoned
- 1990-02-09 MY MYPI90000214A patent/MY105234A/en unknown
- 1990-02-09 IL IL93332A patent/IL93332A0/xx unknown
- 1990-02-09 HU HU90751A patent/HUT55541A/hu unknown
- 1990-02-09 NZ NZ232447A patent/NZ232447A/xx unknown
- 1990-02-12 PT PT93120A patent/PT93120A/pt not_active Application Discontinuation
- 1990-02-12 NL NL9000332A patent/NL9000332A/nl not_active Application Discontinuation
- 1990-02-13 FR FR9001695A patent/FR2647216B1/fr not_active Expired - Fee Related
- 1990-02-14 GB GB909003397A patent/GB9003397D0/en active Pending
- 1990-02-17 DE DE4005085A patent/DE4005085A1/de not_active Withdrawn
- 1990-02-19 IT IT19406A patent/IT1240313B/it active IP Right Grant
- 1990-02-20 ES ES9000496A patent/ES2019531A6/es not_active Expired - Fee Related
- 1990-02-20 YU YU33390A patent/YU33390A/sh unknown
- 1990-02-23 PE PE1990165658A patent/PE14191A1/es not_active Application Discontinuation
- 1990-02-23 LU LU87685A patent/LU87685A1/fr unknown
- 1990-02-27 JP JP2044700A patent/JPH0321848A/ja active Pending
- 1990-02-27 GB GB9004362A patent/GB2231966B/en not_active Expired - Fee Related
- 1990-03-02 DD DD338352A patent/DD299982A5/de unknown
- 1990-03-02 BR BR909000997A patent/BR9000997A/pt not_active Application Discontinuation
- 1990-03-09 AU AU51171/90A patent/AU5117190A/en not_active Abandoned
- 1990-03-10 CN CN90101245A patent/CN1047388A/zh active Pending
- 1990-03-30 SE SE9001175A patent/SE9001175L/xx not_active Application Discontinuation
- 1990-03-31 KR KR1019900004393A patent/KR940002497B1/ko not_active Expired - Lifetime

Also Published As

Publication number	Publication date
DK33390A (da)	1990-11-20
AU5117190A (en)	1990-11-22
IT1240313B (it)	1993-12-07
DK33390D0 (da)	1990-02-08
CA2009703A1 (en)	1990-11-19
MY105234A (en)	1994-08-30
HUT55541A (en)	1991-05-28
HU900751D0 (en)	1990-04-28
IT9019406A0 (it)	1990-02-19
ES2019531A6 (es)	1991-06-16
NL9000332A (nl)	1990-12-17
JPH0321848A (ja)	1991-01-30
GB9004362D0 (en)	1990-04-25
BR9000997A (pt)	1991-02-19
IT9019406A1 (it)	1991-08-19
KR940002497B1 (ko)	1994-03-25
US4970169A (en)	1990-11-13
SE9001175D0 (sv)	1990-03-30
GB9003397D0 (en)	1990-04-11
GB2231966A (en)	1990-11-28
IL93332A0 (en)	1990-11-29
DE4005085A1 (de)	1990-11-22
FR2647216B1 (fr)	1993-07-02
SE9001175L (sv)	1990-11-20
FR2647216A1 (fr)	1990-11-23
NZ232447A (en)	1991-02-26
PT93120A (pt)	1991-01-08
PE14191A1 (es)	1991-04-17
DD299982A5 (de)	1992-05-14
CN1047388A (zh)	1990-11-28
YU33390A (sh)	1992-07-20
GB2231966B (en)	1992-10-14
KR900018669A (ko)	1990-12-22

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EP0526370A1 (de)	1993-02-03	Automatisches Analysegerät für Proben
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LU87685A1 (fr)	1990-07-24	Procede et appareil pour mesurer la surface specifique non poreuse du noir de carbone
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FR2491624A1 (fr)	1982-04-09	Procede pour le fonctionnement d'un appareil d'analyse automatique
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US3545864A (en)	1970-12-08	Apparatus and method for determining gastro-enteral absorption quota
US5075080A (en)	1991-12-24	Apparatus for measuring the non-porous surface area of carbon black
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