MA48429B1 - Procédés de fabrication de solutions de sel de leuco-indigo à très faible teneur en aniline - Google Patents
Procédés de fabrication de solutions de sel de leuco-indigo à très faible teneur en anilineInfo
- Publication number
- MA48429B1 MA48429B1 MA48429A MA48429A MA48429B1 MA 48429 B1 MA48429 B1 MA 48429B1 MA 48429 A MA48429 A MA 48429A MA 48429 A MA48429 A MA 48429A MA 48429 B1 MA48429 B1 MA 48429B1
- Authority
- MA
- Morocco
- Prior art keywords
- leucoindigo
- processes
- solution
- salt solutions
- concentration
- Prior art date
Links
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 title abstract 5
- -1 aniline leucoindigo salt Chemical class 0.000 title abstract 2
- 239000012266 salt solution Substances 0.000 title 1
- VIFKLIUAPGUEBV-UHFFFAOYSA-N 2-(3-hydroxy-1h-indol-2-yl)-1h-indol-3-ol Chemical compound N1C2=CC=CC=C2C(O)=C1C1=C(O)C2=CC=CC=C2N1 VIFKLIUAPGUEBV-UHFFFAOYSA-N 0.000 abstract 4
- 239000000243 solution Substances 0.000 abstract 4
- AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methylaniline Chemical compound CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 abstract 2
- 150000004982 aromatic amines Chemical class 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/02—Bis-indole indigos
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0083—Solutions of dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B9/00—Esters or ester-salts of leuco compounds of vat dyestuffs
- C09B9/04—Esters or ester-salts of leuco compounds of vat dyestuffs of indigoid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/221—Reducing systems; Reducing catalysts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/22—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using vat dyestuffs including indigo
- D06P1/228—Indigo
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/6429—Compounds containing nitrogen bound to a six-membered aromatic carbocyclic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Indole Compounds (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
L'invention concerne une solution aqueuse de leuco-indigo qui comprend une amine aromatique sous la forme d'aniline ou d'aniline et de n-méthylaniline, ledit leuco-indigo se présentant sous la forme d'un sel de métal alcalin ; la concentration de l'amine aromatique étant inférieure à 40 ppm telle que déterminée selon la norme iso 14362-1:2017(e) ; et la concentration du sel de leuco-indigo étant dans une plage de concentration de 5 à 45 % en poids sur la base du poids total de la solution, et la solution étant stable à une température de 23 °c ; ou la concentration du sel de leuco-indigo étant dans une plage de concentration de 45 à 65 % en poids sur la base du poids total de la solution, et la solution étant stable à une température de 60 °c.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17185971.3A EP3441429B1 (fr) | 2017-08-11 | 2017-08-11 | Solutions aqueuses concentrées et purifiées de sel de leucoindigo |
| PCT/EP2018/071800 WO2019030396A1 (fr) | 2017-08-11 | 2018-08-10 | Procédés de fabrication de solutions de sel de leuco-indigo à très faible teneur en aniline |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MA48429A1 MA48429A1 (fr) | 2020-04-30 |
| MA48429B1 true MA48429B1 (fr) | 2020-11-30 |
Family
ID=59677025
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MA48429A MA48429B1 (fr) | 2017-08-11 | 2018-08-10 | Procédés de fabrication de solutions de sel de leuco-indigo à très faible teneur en aniline |
| MA48432A MA48432B1 (fr) | 2017-08-11 | 2018-08-10 | Solutions aqueuses concentrées purifiées de sel de leucoindigo |
| MA48431A MA48431B1 (fr) | 2017-08-11 | 2018-08-10 | Solution de sel de leucoindigo présentant une très faible teneur en aniline et son procédé de préparation |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MA48432A MA48432B1 (fr) | 2017-08-11 | 2018-08-10 | Solutions aqueuses concentrées purifiées de sel de leucoindigo |
| MA48431A MA48431B1 (fr) | 2017-08-11 | 2018-08-10 | Solution de sel de leucoindigo présentant une très faible teneur en aniline et son procédé de préparation |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP3441429B1 (fr) |
| AR (4) | AR112681A1 (fr) |
| ES (1) | ES2877121T3 (fr) |
| MA (3) | MA48429B1 (fr) |
| PT (1) | PT3441429T (fr) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7250762B2 (ja) * | 2017-08-11 | 2023-04-03 | アルフローマ アイピー ゲゼルシャフト ミット ベシュレンクテル ハフツング | 非常に低いアニリン含有量を有するロイコインジゴ塩溶液を製造する方法 |
| BR102019025172A2 (pt) * | 2019-11-28 | 2021-06-08 | Bann Química Ltda. | processo de purificação de soluções de sal de leucoíndigo e uso de um gás inerte |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4220804A1 (de) * | 1992-06-25 | 1994-01-05 | Basf Ag | Verfahren zur Reinigung von Indigo |
| TW251325B (fr) | 1993-03-30 | 1995-07-11 | Basf Ag | |
| DE19831291A1 (de) * | 1998-07-13 | 2000-01-20 | Basf Ag | Konzentrierte Lekoindigolösungen |
| AU2003260454A1 (en) | 2002-08-31 | 2004-04-30 | Dystar Textilfarben Gmbh And Co. Deutschland Kg | Method for the production of high-purity indigo |
-
2017
- 2017-08-11 ES ES17185971T patent/ES2877121T3/es active Active
- 2017-08-11 PT PT171859713T patent/PT3441429T/pt unknown
- 2017-08-11 EP EP17185971.3A patent/EP3441429B1/fr active Active
-
2018
- 2018-08-10 AR ARP180102289 patent/AR112681A1/es active IP Right Grant
- 2018-08-10 MA MA48429A patent/MA48429B1/fr unknown
- 2018-08-10 MA MA48432A patent/MA48432B1/fr unknown
- 2018-08-10 AR ARP180102288 patent/AR112680A1/es active IP Right Grant
- 2018-08-10 AR ARP180102287A patent/AR112936A1/es active IP Right Grant
- 2018-08-10 MA MA48431A patent/MA48431B1/fr unknown
- 2018-08-10 AR ARP180102290A patent/AR112733A1/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| AR112733A1 (es) | 2019-12-04 |
| MA48431B1 (fr) | 2020-11-30 |
| MA48432A1 (fr) | 2020-04-30 |
| AR112681A1 (es) | 2019-11-27 |
| EP3441429B1 (fr) | 2021-05-26 |
| AR112680A1 (es) | 2019-11-27 |
| MA48432B1 (fr) | 2021-04-30 |
| ES2877121T3 (es) | 2021-11-16 |
| AR112936A1 (es) | 2020-01-08 |
| PT3441429T (pt) | 2021-06-28 |
| MA48431A1 (fr) | 2020-04-30 |
| EP3441429A1 (fr) | 2019-02-13 |
| MA48429A1 (fr) | 2020-04-30 |
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