MX387774B - Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinicos. - Google Patents

Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinicos.

Info

Publication number
MX387774B
MX387774B MX2016017120A MX2016017120A MX387774B MX 387774 B MX387774 B MX 387774B MX 2016017120 A MX2016017120 A MX 2016017120A MX 2016017120 A MX2016017120 A MX 2016017120A MX 387774 B MX387774 B MX 387774B
Authority
MX
Mexico
Prior art keywords
alkoxy
preparation
hydroxypicolinic acids
hydroxypicolinonitrile
dibromo
Prior art date
Application number
MX2016017120A
Other languages
English (en)
Other versions
MX2016017120A (es
Inventor
Gregory T Whiteker
James M Renga
Nakyen Choy
Yuanming Zhu
Original Assignee
Corteva Agriscience Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Corteva Agriscience Llc filed Critical Corteva Agriscience Llc
Publication of MX2016017120A publication Critical patent/MX2016017120A/es
Publication of MX387774B publication Critical patent/MX387774B/es

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/33—Heterocyclic compounds
    • A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/435—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with one nitrogen as the only ring hetero atom
    • A61K31/44—Non condensed pyridines; Hydrogenated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/79—Acids; Esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/79—Acids; Esters
    • C07D213/803—Processes of preparation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • Public Health (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Pyridine Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Furan Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)

Abstract

4,6-dibromo-3-hidroxipilinonitrilo se puede preparar de furfural en una serie de etapas químicas seleccionadas de ciano-aminación, formación de sal de amina y bromación - reordenamiento. Los ácidos 4-alcoxi-3-hidroxipicolínicos se pueden preparar convenientemente de 4,6-dibromo-3-hidroxipicolinonitrilo en una serie de etapas químicas seleccionadas de sustitución de bromo, hidrolisis de nitrilo y reducción de halógeno.
MX2016017120A 2014-07-08 2015-07-08 Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinicos. MX387774B (es)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201462021881P 2014-07-08 2014-07-08
US201462021877P 2014-07-08 2014-07-08
US201462021876P 2014-07-08 2014-07-08
PCT/US2015/039569 WO2016007638A1 (en) 2014-07-08 2015-07-08 Process for the preparation of 4-alkoxy-3-hydroxypicolinic acids

Publications (2)

Publication Number Publication Date
MX2016017120A MX2016017120A (es) 2017-05-10
MX387774B true MX387774B (es) 2025-03-18

Family

ID=55064837

Family Applications (3)

Application Number Title Priority Date Filing Date
MX2016017120A MX387774B (es) 2014-07-08 2015-07-08 Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinicos.
MX2016017106A MX369327B (es) 2014-07-08 2015-07-08 Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinico s.
MX2016017127A MX373312B (es) 2014-07-08 2015-07-08 Proceso para la preparación de ácidos 4-alcoxi-3-hidroxipicolínicos.

Family Applications After (2)

Application Number Title Priority Date Filing Date
MX2016017106A MX369327B (es) 2014-07-08 2015-07-08 Proceso para la preparacion de acidos 4-alcoxi-3-hidroxipicolinico s.
MX2016017127A MX373312B (es) 2014-07-08 2015-07-08 Proceso para la preparación de ácidos 4-alcoxi-3-hidroxipicolínicos.

Country Status (16)

Country Link
US (4) US9475771B2 (es)
EP (3) EP3166611B1 (es)
JP (4) JP6513178B2 (es)
KR (3) KR102441177B1 (es)
CN (3) CN106573005B (es)
BR (3) BR112017000061B8 (es)
CA (3) CA2954284C (es)
CO (3) CO2017000049A2 (es)
DK (3) DK3166612T3 (es)
ES (3) ES2738401T3 (es)
IL (3) IL249893B (es)
MX (3) MX387774B (es)
PL (3) PL3166612T3 (es)
TW (5) TWI684587B (es)
WO (3) WO2016007634A1 (es)
ZA (1) ZA201700254B (es)

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AR123502A1 (es) 2020-09-15 2022-12-07 Pi Industries Ltd Nuevos compuestos de picolinamida para combatir hongos fitopatógenos
UY39423A (es) 2020-09-15 2022-03-31 Pi Industries Ltd Nuevos compuestos de picolinamida para combatir hongos fitopatógenos
UY40356A (es) 2022-07-18 2024-01-31 Pi Industries Ltd Un proceso para la síntesis de ácidos 4-alcoxi-3-hidroxipicolínicos e intermedios de los mismos.

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Also Published As

Publication number Publication date
IL249891A0 (en) 2017-03-30
JP2017523962A (ja) 2017-08-24
DK3166612T3 (da) 2019-09-23
CN106573005A (zh) 2017-04-19
CA2954276C (en) 2022-12-13
US20160009650A1 (en) 2016-01-14
US9718783B2 (en) 2017-08-01
TW201625571A (zh) 2016-07-16
PL3166611T3 (pl) 2021-04-06
IL249911A0 (en) 2017-03-30
MX2016017120A (es) 2017-05-10
JP6625115B2 (ja) 2019-12-25
BR112017000061B1 (pt) 2022-10-25
ES2807622T3 (es) 2021-02-23
CO2017000430A2 (es) 2017-04-28
MX2016017127A (es) 2017-05-10
KR102436286B1 (ko) 2022-08-26
TWI682923B (zh) 2020-01-21
JP6513178B2 (ja) 2019-05-15
PL3166612T3 (pl) 2019-12-31
PL3166927T3 (pl) 2020-10-19
JP2017523960A (ja) 2017-08-24
TWI684587B (zh) 2020-02-11
TW201943703A (zh) 2019-11-16
ZA201700254B (en) 2018-12-19
TWI720647B (zh) 2021-03-01
US20160009649A1 (en) 2016-01-14
US9475771B2 (en) 2016-10-25
CN106660957B (zh) 2019-11-29
JP2017521429A (ja) 2017-08-03
KR20170023942A (ko) 2017-03-06
CA2954284C (en) 2022-12-13
TW201625542A (zh) 2016-07-16
DK3166927T3 (da) 2020-07-27
CA2954276A1 (en) 2016-01-14
CA2954167C (en) 2023-01-03
EP3166611A1 (en) 2017-05-17
EP3166612A1 (en) 2017-05-17
EP3166611B1 (en) 2020-09-16
KR102441177B1 (ko) 2022-09-07
BR112016031007B8 (pt) 2022-08-23
IL249891B (en) 2020-07-30
WO2016007637A1 (en) 2016-01-14
EP3166611A4 (en) 2018-02-21
CN106659724A (zh) 2017-05-10
DK3166611T3 (da) 2020-12-07
US20170044105A1 (en) 2017-02-16
CN106573005B (zh) 2020-05-29
KR20170029501A (ko) 2017-03-15
BR112017000135B8 (pt) 2023-05-16
BR112017000135A2 (pt) 2017-11-07
CO2017000049A2 (es) 2017-05-10
CA2954167A1 (en) 2016-01-14
US9522887B2 (en) 2016-12-20
TW201625541A (zh) 2016-07-16
BR112017000061B8 (pt) 2023-05-16
US20160009676A1 (en) 2016-01-14
MX2016017106A (es) 2017-05-10
KR20170029506A (ko) 2017-03-15
TW202003481A (zh) 2020-01-16
EP3166927A4 (en) 2017-12-20
ES2738401T3 (es) 2020-01-22
JP6688278B2 (ja) 2020-04-28
IL249911B (en) 2020-02-27
EP3166927A1 (en) 2017-05-17
CN106659724B (zh) 2020-04-28
JP2020073575A (ja) 2020-05-14
CN106660957A (zh) 2017-05-10
IL249893B (en) 2020-02-27
EP3166612A4 (en) 2017-12-20
EP3166927B1 (en) 2020-04-22
BR112017000061A2 (pt) 2017-11-07
US9481651B2 (en) 2016-11-01
WO2016007634A1 (en) 2016-01-14
MX369327B (es) 2019-11-05
IL249893A0 (en) 2017-03-30
TWI689498B (zh) 2020-04-01
ES2836201T3 (es) 2021-06-24
BR112016031007B1 (pt) 2021-04-27
BR112017000135B1 (pt) 2022-08-09
KR102450085B1 (ko) 2022-10-04
WO2016007638A1 (en) 2016-01-14
MX373312B (es) 2020-05-20
CA2954284A1 (en) 2016-01-14
CO2017000446A2 (es) 2017-05-10
EP3166612B1 (en) 2019-06-12

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