MY161765A - Process for the preparation of primary amines by homogeneously catalyzed alcohol amination - Google Patents
Process for the preparation of primary amines by homogeneously catalyzed alcohol aminationInfo
- Publication number
- MY161765A MY161765A MYPI2013003245A MYPI2013003245A MY161765A MY 161765 A MY161765 A MY 161765A MY PI2013003245 A MYPI2013003245 A MY PI2013003245A MY PI2013003245 A MYPI2013003245 A MY PI2013003245A MY 161765 A MY161765 A MY 161765A
- Authority
- MY
- Malaysia
- Prior art keywords
- phase
- nonpolar
- product
- preparation
- primary amines
- Prior art date
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title abstract 4
- 238000005576 amination reaction Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 150000003141 primary amines Chemical class 0.000 title abstract 2
- 239000012071 phase Substances 0.000 abstract 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
- 239000003054 catalyst Substances 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 229910021529 ammonia Inorganic materials 0.000 abstract 2
- 238000006555 catalytic reaction Methods 0.000 abstract 2
- 230000008030 elimination Effects 0.000 abstract 1
- 238000003379 elimination reaction Methods 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000012454 non-polar solvent Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/04—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
- C07D207/20—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
PREPARING A PRIMARY AMINE BY ALCOHOL AMINATION OF ALCOHOL WITH AMMONIA AND ELIMINATION OF WATER INCLUDES REACTING, IN A HOMOGENEOUSLY CATALYZED REACTION, A MIXTURE OF ALCOHOL, AMMONIA, NONPOLAR SOLVENT, AND CATALYST, IN A LIQUID PHASE, TO OBTAIN A PRODUCT MIXTURE. THE PROCESS THEN INCLUDES PHASE SEPARATING THE PRODUCT MIXTURE INTO A POLAR PRODUCT PHASE AND A NONPOLAR PRODUCT PHASE, AND SEPARATING OFF THE NONPOLAR PRODUCT PHASE. AT LEAST SOME OF THE NONPOLAR PHASE RETURNS TO THE HOMOGENOUSLY CATALYZED REACTION. THE PROCESS FURTHER INCLUDES SEPARATING OFF AMINATION PRODUCT FROM THE POLAR PRODUCT PHASE. AT LEAST SOME OF THE CATALYST IS IN THE NONPOLAR PHASE, AND THE CATALYST ACCUMULATES IN THE NONPOLAR PHASE.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11157335 | 2011-03-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY161765A true MY161765A (en) | 2017-05-15 |
Family
ID=45771826
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2013003245A MY161765A (en) | 2011-03-08 | 2012-03-01 | Process for the preparation of primary amines by homogeneously catalyzed alcohol amination |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP2683680B1 (en) |
| JP (1) | JP5766307B2 (en) |
| CN (1) | CN103502199B (en) |
| AU (1) | AU2012224721A1 (en) |
| BR (1) | BR112013022548A2 (en) |
| CA (1) | CA2828330A1 (en) |
| ES (1) | ES2544933T3 (en) |
| HU (1) | HUE027438T2 (en) |
| MX (1) | MX2013010218A (en) |
| MY (1) | MY161765A (en) |
| RU (1) | RU2013144821A (en) |
| WO (1) | WO2012119930A1 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY161194A (en) * | 2011-03-08 | 2017-04-14 | Basf Se | Method for producing diamines, triamines and polyamines by homogeneously catalyzed alcohol amination |
| AU2012224719A1 (en) * | 2011-03-08 | 2013-09-19 | Basf Se | Method for producing alkanol amines obtained by homogeneously catalyzed alcohol amination |
| ES2543309T3 (en) * | 2011-03-08 | 2015-08-18 | Basf Se | Procedure for the preparation of primary amines by alcohol amination under homogeneous catalysis |
| US8981093B2 (en) | 2012-06-06 | 2015-03-17 | Basf Se | Process for preparing piperazine |
| EP2961731B1 (en) | 2013-02-28 | 2017-02-01 | Basf Se | Method for producing eda using so2-free hydrocyanic acid |
| EP3873877A1 (en) * | 2018-10-31 | 2021-09-08 | Basf Se | Process for producing hydroxymethyl-alcohols |
| EP4416129A4 (en) * | 2021-10-12 | 2025-12-10 | Huntsman Petrochemical Llc | METHOD FOR THE PREPARATION OF ALCOXYLATED ETHERAMINES AND USES THEREOF |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL137371C (en) | 1963-08-02 | |||
| US3708539A (en) | 1970-02-06 | 1973-01-02 | Union Oil Co | Condensation of ammonia or a primary or secondary amine with an alcohol |
| NL169595C (en) | 1970-05-21 | 1982-08-02 | Shell Int Research | PROCESS FOR PREPARING AMINS AND LUBRICATING OILS AND LIQUID ENGINE FUELS CONTAINING THESE. |
| US4709034A (en) * | 1986-02-14 | 1987-11-24 | Air Products And Chemicals, Inc. | Process for the synthesis of hydroxyalkyl amines and hydroxyalkyl piperazines |
| KR900001427B1 (en) | 1986-03-31 | 1990-03-09 | 미쓰비시전기주식회사 | Fuel controller |
| DE3611230A1 (en) | 1986-04-04 | 1987-10-08 | Basf Ag | POLYBUTYL AND POLYISOBUTYLAMINE, METHOD FOR THE PRODUCTION THEREOF AND THE FUEL AND LUBRICANT COMPOSITIONS CONTAINING THE SAME |
| GB8707304D0 (en) * | 1987-03-26 | 1987-04-29 | Bp Chem Int Ltd | Chemical process |
| US5138101A (en) * | 1991-07-19 | 1992-08-11 | Eastman Kodak Company | Recovery of high-boiling aldehydes from rhodium-catalyzed hydroformylation processes |
| DE4428004A1 (en) | 1994-08-08 | 1996-02-15 | Basf Ag | Process for the production of amines |
| US7196033B2 (en) | 2001-12-14 | 2007-03-27 | Huntsman Petrochemical Corporation | Advances in amination catalysis |
| RU2009104985A (en) | 2006-07-14 | 2010-08-27 | Басф Се (De) | METHOD FOR PRODUCING AMINE |
| EP2307431B1 (en) * | 2008-08-10 | 2012-12-26 | Yeda Research and Development Co. Ltd. | Process for preparing amines from alcohols and ammonia |
| ES2543309T3 (en) * | 2011-03-08 | 2015-08-18 | Basf Se | Procedure for the preparation of primary amines by alcohol amination under homogeneous catalysis |
| AU2012224719A1 (en) * | 2011-03-08 | 2013-09-19 | Basf Se | Method for producing alkanol amines obtained by homogeneously catalyzed alcohol amination |
| MY161194A (en) * | 2011-03-08 | 2017-04-14 | Basf Se | Method for producing diamines, triamines and polyamines by homogeneously catalyzed alcohol amination |
-
2012
- 2012-03-01 RU RU2013144821/04A patent/RU2013144821A/en not_active Application Discontinuation
- 2012-03-01 EP EP12706272.7A patent/EP2683680B1/en not_active Not-in-force
- 2012-03-01 CA CA2828330A patent/CA2828330A1/en not_active Abandoned
- 2012-03-01 WO PCT/EP2012/053585 patent/WO2012119930A1/en not_active Ceased
- 2012-03-01 MY MYPI2013003245A patent/MY161765A/en unknown
- 2012-03-01 ES ES12706272.7T patent/ES2544933T3/en active Active
- 2012-03-01 CN CN201280022071.0A patent/CN103502199B/en not_active Expired - Fee Related
- 2012-03-01 BR BR112013022548A patent/BR112013022548A2/en not_active IP Right Cessation
- 2012-03-01 AU AU2012224721A patent/AU2012224721A1/en not_active Abandoned
- 2012-03-01 MX MX2013010218A patent/MX2013010218A/en not_active Application Discontinuation
- 2012-03-01 JP JP2013557050A patent/JP5766307B2/en not_active Expired - Fee Related
- 2012-03-01 HU HUE12706272A patent/HUE027438T2/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| HUE027438T2 (en) | 2016-10-28 |
| WO2012119930A1 (en) | 2012-09-13 |
| JP5766307B2 (en) | 2015-08-19 |
| CN103502199B (en) | 2016-02-10 |
| EP2683680A1 (en) | 2014-01-15 |
| JP2014514267A (en) | 2014-06-19 |
| CN103502199A (en) | 2014-01-08 |
| AU2012224721A1 (en) | 2013-10-03 |
| BR112013022548A2 (en) | 2016-12-06 |
| CA2828330A1 (en) | 2012-09-13 |
| EP2683680B1 (en) | 2015-06-17 |
| MX2013010218A (en) | 2013-10-25 |
| ES2544933T3 (en) | 2015-09-07 |
| RU2013144821A (en) | 2015-04-20 |
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