NL1004214C2 - Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel. - Google Patents

Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel. Download PDF

Info

Publication number: NL1004214C2
Authority: NL; Netherlands
Prior art keywords: starch; modified starch; enzyme; gel; modified
Prior art date: 1996-10-07

Application number

NL1004214A

Other languages

English (en)

Dutch (nl)

Inventor

Gerrit Jan Willem Euverink

Doede Jacob Binnema

Original Assignee

Avebe Coop Verkoop Prod

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1996-10-07

Filing date

1996-10-07

Publication date

1998-04-10

1996-10-07 Priority to NL1004214A priority Critical patent/NL1004214C2/nl

1996-10-07 Application filed by Avebe Coop Verkoop Prod filed Critical Avebe Coop Verkoop Prod

1997-10-06 Priority to DK97943217T priority patent/DK0932444T3/da

1997-10-06 Priority to CA002267118A priority patent/CA2267118C/en

1997-10-06 Priority to PL97332627A priority patent/PL187354B1/pl

1997-10-06 Priority to PCT/NL1997/000552 priority patent/WO1998015347A1/en

1997-10-06 Priority to AU44740/97A priority patent/AU4474097A/en

1997-10-06 Priority to EP97943217A priority patent/EP0932444B1/en

1997-10-06 Priority to DE69710087T priority patent/DE69710087T2/de

1997-10-06 Priority to JP51741098A priority patent/JP4195511B2/ja

1997-10-06 Priority to AT97943217T priority patent/ATE212249T1/de

1997-10-06 Priority to RU99109031/04A priority patent/RU2193585C2/ru

1998-04-10 Application granted granted Critical

1998-04-10 Publication of NL1004214C2 publication Critical patent/NL1004214C2/nl

2002-04-03 Priority to US10/115,347 priority patent/US6864063B2/en

Links

229920000881 Modified starch Polymers 0.000 title claims abstract description 24
235000019426 modified starch Nutrition 0.000 title claims abstract description 24
239000004368 Modified starch Substances 0.000 title claims abstract description 22
229920002472 Starch Polymers 0.000 claims abstract description 49
235000019698 starch Nutrition 0.000 claims abstract description 48
239000008107 starch Substances 0.000 claims abstract description 43
102000004190 Enzymes Human genes 0.000 claims abstract description 24
108090000790 Enzymes Proteins 0.000 claims abstract description 24
230000000694 effects Effects 0.000 claims abstract description 15
229920000856 Amylose Polymers 0.000 claims abstract description 11
239000007864 aqueous solution Substances 0.000 claims abstract description 8
108010043797 4-alpha-glucanotransferase Proteins 0.000 claims abstract description 5
102000004357 Transferases Human genes 0.000 claims abstract description 3
108090000992 Transferases Proteins 0.000 claims abstract description 3
239000000126 substance Substances 0.000 claims abstract 2
230000002255 enzymatic effect Effects 0.000 claims description 8
244000061456 Solanum tuberosum Species 0.000 claims description 3
235000002595 Solanum tuberosum Nutrition 0.000 claims description 3
240000003183 Manihot esculenta Species 0.000 claims description 2
235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 2
239000000853 adhesive Substances 0.000 claims description 2
230000001070 adhesive effect Effects 0.000 claims description 2
239000002537 cosmetic Substances 0.000 claims description 2
239000003599 detergent Substances 0.000 claims description 2
238000005553 drilling Methods 0.000 claims description 2
239000003814 drug Substances 0.000 claims description 2
239000012530 fluid Substances 0.000 claims description 2
240000007594 Oryza sativa Species 0.000 claims 1
235000007164 Oryza sativa Nutrition 0.000 claims 1
241000209140 Triticum Species 0.000 claims 1
235000021307 Triticum Nutrition 0.000 claims 1
240000008042 Zea mays Species 0.000 claims 1
235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims 1
235000002017 Zea mays subsp mays Nutrition 0.000 claims 1
235000005822 corn Nutrition 0.000 claims 1
239000003349 gelling agent Substances 0.000 claims 1
235000009566 rice Nutrition 0.000 claims 1
239000003795 chemical substances by application Substances 0.000 abstract description 2
239000012736 aqueous medium Substances 0.000 abstract 1
108010055629 Glucosyltransferases Proteins 0.000 description 35
102000000340 Glucosyltransferases Human genes 0.000 description 35
229920001592 potato starch Polymers 0.000 description 20
239000000499 gel Substances 0.000 description 17
239000000243 solution Substances 0.000 description 14
238000006243 chemical reaction Methods 0.000 description 13
239000000463 material Substances 0.000 description 11
QKNYBSVHEMOAJP-UHFFFAOYSA-N 2-amino-2-(hydroxymethyl)propane-1,3-diol;hydron;chloride Chemical compound Cl.OCC(N)(CO)CO QKNYBSVHEMOAJP-UHFFFAOYSA-N 0.000 description 8
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
239000007858 starting material Substances 0.000 description 8
239000000047 product Substances 0.000 description 7
230000001603 reducing effect Effects 0.000 description 7
239000000725 suspension Substances 0.000 description 7
229920002245 Dextrose equivalent Polymers 0.000 description 6
238000000034 method Methods 0.000 description 6
229920000945 Amylopectin Polymers 0.000 description 5
238000005119 centrifugation Methods 0.000 description 5
230000004048 modification Effects 0.000 description 5
238000012986 modification Methods 0.000 description 5
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
241000589499 Thermus thermophilus Species 0.000 description 4
230000015572 biosynthetic process Effects 0.000 description 4
102000004169 proteins and genes Human genes 0.000 description 4
108090000623 proteins and genes Proteins 0.000 description 4
239000011780 sodium chloride Substances 0.000 description 4
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 3
102000014914 Carrier Proteins Human genes 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
239000012505 Superdex™ Substances 0.000 description 3
238000000862 absorption spectrum Methods 0.000 description 3
230000009471 action Effects 0.000 description 3
108091008324 binding proteins Proteins 0.000 description 3
210000004027 cell Anatomy 0.000 description 3
235000013339 cereals Nutrition 0.000 description 3
229910052740 iodine Inorganic materials 0.000 description 3
239000011630 iodine Substances 0.000 description 3
230000008569 process Effects 0.000 description 3
238000000746 purification Methods 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
239000006228 supernatant Substances 0.000 description 3
108010028688 Isoamylase Proteins 0.000 description 2
TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
239000002253 acid Substances 0.000 description 2
239000007900 aqueous suspension Substances 0.000 description 2
230000008859 change Effects 0.000 description 2
238000001816 cooling Methods 0.000 description 2
238000010828 elution Methods 0.000 description 2
230000007071 enzymatic hydrolysis Effects 0.000 description 2
238000006047 enzymatic hydrolysis reaction Methods 0.000 description 2
239000000284 extract Substances 0.000 description 2
238000002523 gelfiltration Methods 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
229920001542 oligosaccharide Polymers 0.000 description 2
150000002482 oligosaccharides Chemical class 0.000 description 2
230000003647 oxidation Effects 0.000 description 2
238000007254 oxidation reaction Methods 0.000 description 2
239000008188 pellet Substances 0.000 description 2
239000000843 powder Substances 0.000 description 2
239000007966 viscous suspension Substances 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
HNSDLXPSAYFUHK-UHFFFAOYSA-N 1,4-bis(2-ethylhexyl) sulfosuccinate Chemical compound CCCCC(CC)COC(=O)CC(S(O)(=O)=O)C(=O)OCC(CC)CCCC HNSDLXPSAYFUHK-UHFFFAOYSA-N 0.000 description 1
DBTMGCOVALSLOR-UHFFFAOYSA-N 32-alpha-galactosyl-3-alpha-galactosyl-galactose Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(OC2C(C(CO)OC(O)C2O)O)OC(CO)C1O DBTMGCOVALSLOR-UHFFFAOYSA-N 0.000 description 1
239000004382 Amylase Substances 0.000 description 1
241000894006 Bacteria Species 0.000 description 1
229920002261 Corn starch Polymers 0.000 description 1
JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
RXVWSYJTUUKTEA-UHFFFAOYSA-N D-maltotriose Natural products OC1C(O)C(OC(C(O)CO)C(O)C(O)C=O)OC(CO)C1OC1C(O)C(O)C(O)C(CO)O1 RXVWSYJTUUKTEA-UHFFFAOYSA-N 0.000 description 1
102000016911 Deoxyribonucleases Human genes 0.000 description 1
108010053770 Deoxyribonucleases Proteins 0.000 description 1
241000588724 Escherichia coli Species 0.000 description 1
241000206602 Eukaryota Species 0.000 description 1
210000000712 G cell Anatomy 0.000 description 1
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
125000001429 N-terminal alpha-amino-acid group Chemical group 0.000 description 1
229910021204 NaH2 PO4 Inorganic materials 0.000 description 1
229930006000 Sucrose Natural products 0.000 description 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
241000204652 Thermotoga Species 0.000 description 1
241000868182 Thermus thermophilus HB8 Species 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
238000005903 acid hydrolysis reaction Methods 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
235000019270 ammonium chloride Nutrition 0.000 description 1
238000005571 anion exchange chromatography Methods 0.000 description 1
239000002518 antifoaming agent Substances 0.000 description 1
229940041514 candida albicans extract Drugs 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
238000012512 characterization method Methods 0.000 description 1
229910001431 copper ion Inorganic materials 0.000 description 1
239000008120 corn starch Substances 0.000 description 1
229940099112 cornstarch Drugs 0.000 description 1
238000009295 crossflow filtration Methods 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
238000001212 derivatisation Methods 0.000 description 1
238000000502 dialysis Methods 0.000 description 1
ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 description 1
229910000396 dipotassium phosphate Inorganic materials 0.000 description 1
235000019797 dipotassium phosphate Nutrition 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000003480 eluent Substances 0.000 description 1
238000000855 fermentation Methods 0.000 description 1
230000004151 fermentation Effects 0.000 description 1
238000005187 foaming Methods 0.000 description 1
235000013305 food Nutrition 0.000 description 1
238000001641 gel filtration chromatography Methods 0.000 description 1
239000008103 glucose Substances 0.000 description 1
125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 1
239000008187 granular material Substances 0.000 description 1
239000001963 growth medium Substances 0.000 description 1
238000004128 high performance liquid chromatography Methods 0.000 description 1
238000011534 incubation Methods 0.000 description 1
229910001629 magnesium chloride Inorganic materials 0.000 description 1
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
FYGDTMLNYKFZSV-UHFFFAOYSA-N mannotriose Natural products OC1C(O)C(O)C(CO)OC1OC1C(CO)OC(OC2C(OC(O)C(O)C2O)CO)C(O)C1O FYGDTMLNYKFZSV-UHFFFAOYSA-N 0.000 description 1
239000000178 monomer Substances 0.000 description 1
229920001282 polysaccharide Polymers 0.000 description 1
229940116317 potato starch Drugs 0.000 description 1
230000008707 rearrangement Effects 0.000 description 1
230000009467 reduction Effects 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
238000000518 rheometry Methods 0.000 description 1
229940100486 rice starch Drugs 0.000 description 1
239000000523 sample Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000001509 sodium citrate Substances 0.000 description 1
NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
238000011282 treatment Methods 0.000 description 1
238000005406 washing Methods 0.000 description 1
229940100445 wheat starch Drugs 0.000 description 1
239000012138 yeast extract Substances 0.000 description 1
FYGDTMLNYKFZSV-BYLHFPJWSA-N β-1,4-galactotrioside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@H](CO)O[C@@H](O[C@@H]2[C@@H](O[C@@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-BYLHFPJWSA-N 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0052—Preparation of gels
- B01J13/0065—Preparation of gels containing an organic phase

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Dispersion Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Jellies, Jams, And Syrups (AREA)
Compositions Of Macromolecular Compounds (AREA)

NL1004214A 1996-10-07 1996-10-07 Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel. NL1004214C2 (nl)

Priority Applications (12)

Application Number	Priority Date	Filing Date	Title
NL1004214A NL1004214C2 (nl)	1996-10-07	1996-10-07	Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel.
CA002267118A CA2267118C (en)	1996-10-07	1997-10-06	Use of modified starch as an agent for forming a thermoreversible gel
PL97332627A PL187354B1 (pl)	1996-10-07	1997-10-06	Zastosowanie modyfikowanej skrobi jako środka do tworzenia termoodwracalnego żelu
PCT/NL1997/000552 WO1998015347A1 (en)	1996-10-07	1997-10-06	Use of modified starch as an agent for forming a thermoreversible gel
DK97943217T DK0932444T3 (da)	1996-10-07	1997-10-06	Anvendelse af modificeret stivelse som et middel til at danne en termoreversibel gel
AU44740/97A AU4474097A (en)	1996-10-07	1997-10-06	Use of modified starch as an agent for forming a thermoreversible gel
EP97943217A EP0932444B1 (en)	1996-10-07	1997-10-06	Use of modified starch as an agent for forming a thermoreversible gel
DE69710087T DE69710087T2 (de)	1996-10-07	1997-10-06	Verwendung von modifizierter stärke aus mittel zur bildung eines thermoreversiblen gels
JP51741098A JP4195511B2 (ja)	1996-10-07	1997-10-06	熱可逆性ゲルを形成するための作用剤としての修飾デンプンの使用
AT97943217T ATE212249T1 (de)	1996-10-07	1997-10-06	Verwendung von modifizierter stärke aus mittel zur bildung eines thermoreversiblen gels
RU99109031/04A RU2193585C2 (ru)	1996-10-07	1997-10-06	Агент для образования термообратимого геля и продукт в форме термообратимого геля
US10/115,347 US6864063B2 (en)	1996-10-07	2002-04-03	Use of modified starch as an agent for forming a thermoreversible gel

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL1004214		1996-10-07
NL1004214A NL1004214C2 (nl)	1996-10-07	1996-10-07	Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel.

Publications (1)

Publication Number	Publication Date
NL1004214C2 true NL1004214C2 (nl)	1998-04-10

Family

ID=19763633

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL1004214A NL1004214C2 (nl)	1996-10-07	1996-10-07	Toepassing van gemodificeerd zetmeel als middel voor het vormen van een thermoreversibele gel.

Country Status (12)

Country	Link
US (1)	US6864063B2 (da)
EP (1)	EP0932444B1 (da)
JP (1)	JP4195511B2 (da)
AT (1)	ATE212249T1 (da)
AU (1)	AU4474097A (da)
CA (1)	CA2267118C (da)
DE (1)	DE69710087T2 (da)
DK (1)	DK0932444T3 (da)
NL (1)	NL1004214C2 (da)
PL (1)	PL187354B1 (da)
RU (1)	RU2193585C2 (da)
WO (1)	WO1998015347A1 (da)

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- 1997-10-06 CA CA002267118A patent/CA2267118C/en not_active Expired - Lifetime
- 1997-10-06 AT AT97943217T patent/ATE212249T1/de active
- 1997-10-06 PL PL97332627A patent/PL187354B1/pl unknown
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- 1997-10-06 JP JP51741098A patent/JP4195511B2/ja not_active Expired - Fee Related
- 1997-10-06 RU RU99109031/04A patent/RU2193585C2/ru active
- 1997-10-06 DK DK97943217T patent/DK0932444T3/da active
- 1997-10-06 DE DE69710087T patent/DE69710087T2/de not_active Expired - Lifetime
2002
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Also Published As

Publication number	Publication date
EP0932444A1 (en)	1999-08-04
AU4474097A (en)	1998-05-05
PL332627A1 (en)	1999-09-27
ATE212249T1 (de)	2002-02-15
JP4195511B2 (ja)	2008-12-10
CA2267118C (en)	2005-08-16
WO1998015347A1 (en)	1998-04-16
EP0932444B1 (en)	2002-01-23
CA2267118A1 (en)	1998-04-16
JP2001501670A (ja)	2001-02-06
US20030007984A1 (en)	2003-01-09
RU2193585C2 (ru)	2002-11-27
DE69710087T2 (de)	2002-08-01
PL187354B1 (pl)	2004-06-30
DE69710087D1 (de)	2002-03-14
US6864063B2 (en)	2005-03-08
DK0932444T3 (da)	2002-04-02

Legal Events

Date	Code	Title	Description
1998-06-02	PD2B	A search report has been drawn up
2006-10-02	TD	Modifications of names of proprietors of patents	Owner name: COOEPERATIE AVEBE U.A. Effective date: 20060711
2012-08-22	PLEX	Lifting of former pledge	Effective date: 20120814
2016-10-12	MK	Patent expired because of reaching the maximum lifetime of a patent	Effective date: 20161006

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