NL8502060A - Werkwijze voor het verkrijgen van een in water onoplosbare organische stikstofbase uitgaande van een waterige oplossing van alkalimetaalbicarbonaat en het chloorhydraat van genoemde base alsmede werkwijze voor de bereiding van natriumbicarbonaat. - Google Patents

Werkwijze voor het verkrijgen van een in water onoplosbare organische stikstofbase uitgaande van een waterige oplossing van alkalimetaalbicarbonaat en het chloorhydraat van genoemde base alsmede werkwijze voor de bereiding van natriumbicarbonaat. Download PDF

Info

Publication number: NL8502060A
Authority: NL; Netherlands
Prior art keywords: aqueous; solution; chlorohydrate; organic; amine
Prior art date: 1984-07-17

Application number

NL8502060A

Other languages

English (en)

Dutch (nl)

Original Assignee

Solvay

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-07-17

Filing date

1985-07-17

Publication date

1986-02-17

1985-07-17 Application filed by Solvay filed Critical Solvay

1986-02-17 Publication of NL8502060A publication Critical patent/NL8502060A/nl

Links

238000000034 method Methods 0.000 title claims description 37
239000007864 aqueous solution Substances 0.000 title claims description 36
229910052783 alkali metal Inorganic materials 0.000 title claims description 17
238000002360 preparation method Methods 0.000 title claims description 12
150000001340 alkali metals Chemical class 0.000 title description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 title description 2
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 title 2
QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 title 1
125000001309 chloro group Chemical class Cl* 0.000 title 1
229910052757 nitrogen Inorganic materials 0.000 title 1
150000001412 amines Chemical class 0.000 claims description 60
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 56
239000000243 solution Substances 0.000 claims description 55
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 47
239000002585 base Substances 0.000 claims description 35
125000001477 organic nitrogen group Chemical group 0.000 claims description 30
235000017557 sodium bicarbonate Nutrition 0.000 claims description 28
229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 28
235000002639 sodium chloride Nutrition 0.000 claims description 25
239000011780 sodium chloride Substances 0.000 claims description 25
239000003795 chemical substances by application Substances 0.000 claims description 20
239000000203 mixture Substances 0.000 claims description 20
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 19
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 18
-1 alkali metal bicarbonate Chemical class 0.000 claims description 14
238000010908 decantation Methods 0.000 claims description 14
239000008346 aqueous phase Substances 0.000 claims description 13
239000012452 mother liquor Substances 0.000 claims description 12
239000007789 gas Substances 0.000 claims description 11
239000001569 carbon dioxide Substances 0.000 claims description 9
229910002092 carbon dioxide Inorganic materials 0.000 claims description 9
239000007788 liquid Substances 0.000 claims description 7
239000007900 aqueous suspension Substances 0.000 claims description 6
239000002904 solvent Substances 0.000 claims description 6
125000004432 carbon atom Chemical group C* 0.000 claims description 5
150000007529 inorganic bases Chemical class 0.000 claims description 5
239000012071 phase Substances 0.000 claims description 5
239000011541 reaction mixture Substances 0.000 claims description 5
150000003973 alkyl amines Chemical class 0.000 claims description 4
239000007787 solid Substances 0.000 claims description 4
239000012074 organic phase Substances 0.000 claims description 3
150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
238000006243 chemical reaction Methods 0.000 description 10
239000003960 organic solvent Substances 0.000 description 10
229920006395 saturated elastomer Polymers 0.000 description 7
238000002425 crystallisation Methods 0.000 description 6
230000008025 crystallization Effects 0.000 description 6
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
150000003141 primary amines Chemical class 0.000 description 5
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
229910052799 carbon Inorganic materials 0.000 description 4
235000015497 potassium bicarbonate Nutrition 0.000 description 4
229910000028 potassium bicarbonate Inorganic materials 0.000 description 4
239000011736 potassium bicarbonate Substances 0.000 description 4
AAIUWVOMXTVLRG-UHFFFAOYSA-N 8,8-dimethylnonan-1-amine Chemical compound CC(C)(C)CCCCCCCN AAIUWVOMXTVLRG-UHFFFAOYSA-N 0.000 description 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
229910001514 alkali metal chloride Inorganic materials 0.000 description 3
238000005868 electrolysis reaction Methods 0.000 description 3
230000005484 gravity Effects 0.000 description 3
235000008733 Citrus aurantifolia Nutrition 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
235000011941 Tilia x europaea Nutrition 0.000 description 2
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
239000000920 calcium hydroxide Substances 0.000 description 2
229910001861 calcium hydroxide Inorganic materials 0.000 description 2
230000001143 conditioned effect Effects 0.000 description 2
239000013078 crystal Substances 0.000 description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
229910000041 hydrogen chloride Inorganic materials 0.000 description 2
239000004571 lime Substances 0.000 description 2
238000002156 mixing Methods 0.000 description 2
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
239000008096 xylene Substances 0.000 description 2
HYFLWBNQFMXCPA-UHFFFAOYSA-N 1-ethyl-2-methylbenzene Chemical class CCC1=CC=CC=C1C HYFLWBNQFMXCPA-UHFFFAOYSA-N 0.000 description 1
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
150000007824 aliphatic compounds Chemical class 0.000 description 1
239000003513 alkali Substances 0.000 description 1
229910052784 alkaline earth metal Inorganic materials 0.000 description 1
229910001617 alkaline earth metal chloride Inorganic materials 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
OCKPCBLVNKHBMX-UHFFFAOYSA-N butylbenzene Chemical class CCCCC1=CC=CC=C1 OCKPCBLVNKHBMX-UHFFFAOYSA-N 0.000 description 1
238000001354 calcination Methods 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
230000001747 exhibiting effect Effects 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000000265 homogenisation Methods 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
150000002466 imines Chemical class 0.000 description 1
239000000463 material Substances 0.000 description 1
239000012528 membrane Substances 0.000 description 1
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
229910052753 mercury Inorganic materials 0.000 description 1
238000005065 mining Methods 0.000 description 1
150000007530 organic bases Chemical class 0.000 description 1
230000035699 permeability Effects 0.000 description 1
239000001103 potassium chloride Substances 0.000 description 1
WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
235000011164 potassium chloride Nutrition 0.000 description 1
150000003242 quaternary ammonium salts Chemical class 0.000 description 1
239000000376 reactant Substances 0.000 description 1
230000001172 regenerating effect Effects 0.000 description 1
238000012827 research and development Methods 0.000 description 1
239000012047 saturated solution Substances 0.000 description 1
150000003335 secondary amines Chemical class 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000002002 slurry Substances 0.000 description 1
KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
229910001948 sodium oxide Inorganic materials 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/16—Preparation from compounds of sodium or potassium with amines and carbon dioxide

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Removal Of Specific Substances (AREA)
Treatment Of Water By Oxidation Or Reduction (AREA)
Fertilizers (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

NL8502060A 1984-07-17 1985-07-17 Werkwijze voor het verkrijgen van een in water onoplosbare organische stikstofbase uitgaande van een waterige oplossing van alkalimetaalbicarbonaat en het chloorhydraat van genoemde base alsmede werkwijze voor de bereiding van natriumbicarbonaat. NL8502060A (nl)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
FR8411424		1984-07-17
FR8411424A FR2567878B1 (fr)	1984-07-17	1984-07-17	Procede pour l'obtention d'une base organique azotee insoluble dans l'eau, au depart d'une solution aqueuse de bicarbonate de metal alcalin et de chlorhydrate de ladite base, et procede de fabrication de bicarbonate de sodium

Publications (1)

Publication Number	Publication Date
NL8502060A true NL8502060A (nl)	1986-02-17

Family

ID=9306264

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8502060A NL8502060A (nl)	1984-07-17	1985-07-17	Werkwijze voor het verkrijgen van een in water onoplosbare organische stikstofbase uitgaande van een waterige oplossing van alkalimetaalbicarbonaat en het chloorhydraat van genoemde base alsmede werkwijze voor de bereiding van natriumbicarbonaat.

Country Status (19)

Country	Link
US (1)	US4677229A (it)
JP (1)	JPS6156157A (it)
AT (1)	AT383591B (it)
AU (1)	AU4485785A (it)
BE (1)	BE902854A (it)
BR (1)	BR8503385A (it)
DE (1)	DE3525573A1 (it)
ES (1)	ES8607208A1 (it)
FR (1)	FR2567878B1 (it)
GB (1)	GB2162176A (it)
IL (1)	IL75759A0 (it)
IT (1)	IT1187690B (it)
LU (1)	LU86005A1 (it)
MA (1)	MA20489A1 (it)
NL (1)	NL8502060A (it)
NO (1)	NO852837L (it)
PT (1)	PT80814B (it)
SE (1)	SE8503478L (it)
ZA (1)	ZA855161B (it)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3443889A (en) *	1964-08-17	1969-05-13	Kaiser Aluminium Chem Corp	Method of synthesis of alkali metal salts
JPS5734020A (en) *	1980-08-06	1982-02-24	Toyo Soda Mfg Co Ltd	Recovery of ammonia

1984
- 1984-07-17 FR FR8411424A patent/FR2567878B1/fr not_active Expired
1985
- 1985-07-09 ZA ZA855161A patent/ZA855161B/xx unknown
- 1985-07-10 IL IL75759A patent/IL75759A0/xx unknown
- 1985-07-11 BE BE1/011295A patent/BE902854A/fr not_active IP Right Cessation
- 1985-07-12 AU AU44857/85A patent/AU4485785A/en not_active Abandoned
- 1985-07-15 SE SE8503478A patent/SE8503478L/ not_active Application Discontinuation
- 1985-07-15 PT PT80814A patent/PT80814B/pt unknown
- 1985-07-15 US US06/754,972 patent/US4677229A/en not_active Expired - Fee Related
- 1985-07-15 LU LU86005A patent/LU86005A1/fr unknown
- 1985-07-16 ES ES545249A patent/ES8607208A1/es not_active Expired
- 1985-07-16 BR BR8503385A patent/BR8503385A/pt unknown
- 1985-07-16 NO NO852837A patent/NO852837L/no unknown
- 1985-07-16 MA MA20714A patent/MA20489A1/fr unknown
- 1985-07-16 JP JP60156847A patent/JPS6156157A/ja active Pending
- 1985-07-16 GB GB08517879A patent/GB2162176A/en not_active Withdrawn
- 1985-07-16 AT AT0210085A patent/AT383591B/de not_active IP Right Cessation
- 1985-07-17 NL NL8502060A patent/NL8502060A/nl not_active Application Discontinuation
- 1985-07-17 IT IT21613/85A patent/IT1187690B/it active
- 1985-07-17 DE DE19853525573 patent/DE3525573A1/de not_active Withdrawn

Also Published As

Publication number	Publication date
SE8503478D0 (sv)	1985-07-15
FR2567878B1 (fr)	1986-12-05
FR2567878A1 (fr)	1986-01-24
JPS6156157A (ja)	1986-03-20
DE3525573A1 (de)	1986-01-23
SE8503478L (sv)	1986-01-18
ES545249A0 (es)	1986-05-16
PT80814A (fr)	1985-08-01
ES8607208A1 (es)	1986-05-16
PT80814B (fr)	1987-03-23
IT1187690B (it)	1987-12-23
IL75759A0 (en)	1985-11-29
AU4485785A (en)	1986-01-23
IT8521613A0 (it)	1985-07-17
BR8503385A (pt)	1986-04-08
ATA210085A (de)	1986-12-15
US4677229A (en)	1987-06-30
NO852837L (no)	1986-01-20
MA20489A1 (fr)	1986-04-01
GB2162176A (en)	1986-01-29
LU86005A1 (fr)	1986-02-12
ZA855161B (en)	1986-03-26
GB8517879D0 (en)	1985-08-21
AT383591B (de)	1987-07-27
BE902854A (fr)	1986-01-13

Legal Events

Date	Code	Title	Description
1992-08-03	BA	A request for search or an international-type search has been filed
1992-09-01	BB	A search report has been drawn up
1993-01-04	BC	A request for examination has been filed
1994-08-16	DNT	Communications of changes of names of applicants whose applications have been laid open to public inspection	Free format text: SOLVAY (SOCIETE ANONYME)
1997-04-01	BV	The patent application has lapsed

Publication	Publication Date	Title
US4283372A (en)	1981-08-11	Recovery of alkali values from sodium bicarbonate-containing ore with ammonia
IL24158A (en)	1969-09-25	Method for preparing metal salts
EP0248256A2 (en)	1987-12-09	Process for the manufacture of monopotassium phosphate
GB1519571A (en)	1978-08-02	Brine purification process
US4718995A (en)	1988-01-12	Recovery of tungsten, scandium, iron, and manganese from tungsten bearing material
JPH0124849B2 (it)	1989-05-15
PT85176B (en)	1990-01-04	Reduction of acid consumers
NL8502060A (nl)	1986-02-17	Werkwijze voor het verkrijgen van een in water onoplosbare organische stikstofbase uitgaande van een waterige oplossing van alkalimetaalbicarbonaat en het chloorhydraat van genoemde base alsmede werkwijze voor de bereiding van natriumbicarbonaat.
CA2288156A1 (en)	1998-11-05	Process for recovering caprolactam from a neutralized rearrangement mixture
EP0086969B1 (en)	1985-07-24	Selective removal of catechol from 2-methallyloxyphenol
NL8402710A (nl)	1985-04-01	Werkwijze voor het bereiden van een waterige natriumchloride oplossing en werkwijze voor het bereiden van natriumcarbonaat.
US4668495A (en)	1987-05-26	Process for obtaining potassium nitrate from potassium chloride and nitric acid
EP0230686B1 (fr)	1991-02-27	Procédé pour la préparation d'une solution aqueuse de chlorure de sodium et procédé pour la production de bicarbonate de sodium
EP0171106B1 (fr)	1988-05-18	Procédé pour l'obtention d'une base organique azotée insoluble dans l'eau, au départ d'un chlorhydrate hydrosoluble de ladite base et procédé de fabrication de bicarbonate de sodium
NL8001653A (nl)	1980-09-23	Werkwijze ter bereiding van magnesiumchloride.
JPH02235863A (ja)	1990-09-18	Ｎ―メチル―２―ピロリドンの回収
US3694465A (en)	1972-09-26	Method for concentration of aqueous tetrahydrofuran solutions by extraction with aqueous alkali metal hydroxide
Loupy et al.	1989	Organic Chemistry Without Solvent. Improvements to the One Step Preparation of Dibenzyl Sulphones
DE3780758T2 (de)	1993-02-25	Verfahren fuer die extraktion einer organischen fluessigkeit, die eine azotierte organische base aus einer waessrigen suspension von mineralischen teilchen enthaelt und verfahren zur herstellung von alkalimetall-bikarbonat.
US4914235A (en)	1990-04-03	Process for obtaining guanidine hydrohalides from by-product mixtures obtained in the production of mercaptoalkylsilanes
NL8401364A (nl)	1984-11-16	Werkwijze en inrichting voor het bereiden van een organische oplossing van een in water onoplosbare organische base.
WO2001027134A1 (en)	2001-04-19	Process for extracting estrogens from pregnant mare urine (pmu)
JP2879582B2 (ja)	1999-04-05	シアン化第２金酸塩の精製方法
US3433583A (en)	1969-03-18	Process for removal of salts from aqueous solutions with solid methylenedianiline
US3159642A (en)	1964-12-01	Process for purification of bipyridyl