NO129344B - - Google Patents

Download PDF

Info

Publication number: NO129344B
Authority: NO; Norway
Prior art keywords: acid; hydrogen peroxide; reaction medium; alkanesulfonic; methanesulfonic acid
Prior art date: 1967-03-01

Application number

NO00751/68A

Other languages

English (en)

Norwegian (no)

Inventor

D Nielsen

Original Assignee

Ppg Industries Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1967-03-01

Filing date

1968-02-29

Publication date

1974-04-01

1968-02-29 Application filed by Ppg Industries Inc filed Critical Ppg Industries Inc

1974-04-01 Publication of NO129344B publication Critical patent/NO129344B/no

Links

MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 82
AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 claims description 77
239000002253 acid Substances 0.000 claims description 46
229940098779 methanesulfonic acid Drugs 0.000 claims description 38
239000012429 reaction media Substances 0.000 claims description 26
LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 claims description 21
238000000034 method Methods 0.000 claims description 20
150000007513 acids Chemical class 0.000 claims description 18
238000006243 chemical reaction Methods 0.000 claims description 15
238000004519 manufacturing process Methods 0.000 claims description 15
150000004965 peroxy acids Chemical class 0.000 claims description 15
WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 claims description 13
QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 claims description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
239000000203 mixture Substances 0.000 claims description 9
-1 alkyl mercaptans Chemical class 0.000 claims description 7
KXEMXOYVVPLGSD-UHFFFAOYSA-N benzene-1,3-dicarboperoxoic acid Chemical compound OOC(=O)C1=CC=CC(C(=O)OO)=C1 KXEMXOYVVPLGSD-UHFFFAOYSA-N 0.000 claims description 6
150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 5
239000007788 liquid Substances 0.000 claims description 5
125000004432 carbon atom Chemical group C* 0.000 claims description 4
239000011541 reaction mixture Substances 0.000 claims description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 2
230000003647 oxidation Effects 0.000 claims description 2
238000007254 oxidation reaction Methods 0.000 claims description 2
150000004967 organic peroxy acids Chemical class 0.000 description 8
230000015572 biosynthetic process Effects 0.000 description 7
238000001914 filtration Methods 0.000 description 4
150000007524 organic acids Chemical class 0.000 description 4
238000005502 peroxidation Methods 0.000 description 4
SCKXCAADGDQQCS-UHFFFAOYSA-N Performic acid Chemical compound OOC=O SCKXCAADGDQQCS-UHFFFAOYSA-N 0.000 description 3
125000000217 alkyl group Chemical group 0.000 description 3
239000000306 component Substances 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
CETBSQOFQKLHHZ-UHFFFAOYSA-N Diethyl disulfide Chemical compound CCSSCC CETBSQOFQKLHHZ-UHFFFAOYSA-N 0.000 description 2
BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 2
125000003118 aryl group Chemical group 0.000 description 2
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
238000004821 distillation Methods 0.000 description 2
150000002019 disulfides Chemical class 0.000 description 2
POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
230000000694 effects Effects 0.000 description 2
DNJIEGIFACGWOD-UHFFFAOYSA-N ethanethiol Chemical compound CCS DNJIEGIFACGWOD-UHFFFAOYSA-N 0.000 description 2
235000005985 organic acids Nutrition 0.000 description 2
XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000000047 product Substances 0.000 description 2
SUVIGLJNEAMWEG-UHFFFAOYSA-N propane-1-thiol Chemical compound CCCS SUVIGLJNEAMWEG-UHFFFAOYSA-N 0.000 description 2
238000004064 recycling Methods 0.000 description 2
CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
238000000926 separation method Methods 0.000 description 2
239000007787 solid Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000005406 washing Methods 0.000 description 2
SLAMLWHELXOEJZ-UHFFFAOYSA-N 2-nitrobenzoic acid Chemical compound OC(=O)C1=CC=CC=C1[N+]([O-])=O SLAMLWHELXOEJZ-UHFFFAOYSA-N 0.000 description 1
ADCUEPOHPCPMCE-UHFFFAOYSA-N 4-cyanobenzoic acid Chemical compound OC(=O)C1=CC=C(C#N)C=C1 ADCUEPOHPCPMCE-UHFFFAOYSA-N 0.000 description 1
ZEYHEAKUIGZSGI-UHFFFAOYSA-N 4-methoxybenzoic acid Chemical compound COC1=CC=C(C(O)=O)C=C1 ZEYHEAKUIGZSGI-UHFFFAOYSA-N 0.000 description 1
OTLNPYWUJOZPPA-UHFFFAOYSA-N 4-nitrobenzoic acid Chemical compound OC(=O)C1=CC=C([N+]([O-])=O)C=C1 OTLNPYWUJOZPPA-UHFFFAOYSA-N 0.000 description 1
KDVYCTOWXSLNNI-UHFFFAOYSA-N 4-t-Butylbenzoic acid Chemical compound CC(C)(C)C1=CC=C(C(O)=O)C=C1 KDVYCTOWXSLNNI-UHFFFAOYSA-N 0.000 description 1
239000005711 Benzoic acid Substances 0.000 description 1
CUDSBWGCGSUXDB-UHFFFAOYSA-N Dibutyl disulfide Chemical class CCCCSSCCCC CUDSBWGCGSUXDB-UHFFFAOYSA-N 0.000 description 1
239000005639 Lauric acid Substances 0.000 description 1
235000021355 Stearic acid Nutrition 0.000 description 1
UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
230000002411 adverse Effects 0.000 description 1
150000001335 aliphatic alkanes Chemical class 0.000 description 1
125000001931 aliphatic group Chemical group 0.000 description 1
235000010233 benzoic acid Nutrition 0.000 description 1
239000007844 bleaching agent Substances 0.000 description 1
WQAQPCDUOCURKW-UHFFFAOYSA-N butanethiol Chemical class CCCCS WQAQPCDUOCURKW-UHFFFAOYSA-N 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000000470 constituent Substances 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
150000001991 dicarboxylic acids Chemical class 0.000 description 1
CCIVGXIOQKPBKL-UHFFFAOYSA-N ethanesulfonic acid Chemical group CCS(O)(=O)=O CCIVGXIOQKPBKL-UHFFFAOYSA-N 0.000 description 1
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
239000007789 gas Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
150000002763 monocarboxylic acids Chemical class 0.000 description 1
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
239000012071 phase Substances 0.000 description 1
150000003022 phthalic acids Chemical class 0.000 description 1
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000011084 recovery Methods 0.000 description 1
239000008117 stearic acid Substances 0.000 description 1
239000004753 textile Substances 0.000 description 1
230000004584 weight gain Effects 0.000 description 1
235000019786 weight gain Nutrition 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Detergent Compositions (AREA)

NO00751/68A 1967-03-01 1968-02-29 NO129344B (fr)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US61957667A	1967-03-01	1967-03-01

Publications (1)

Publication Number	Publication Date
NO129344B true NO129344B (fr)	1974-04-01

Family

ID=24482468

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO00751/68A NO129344B (fr)	1967-03-01	1968-02-29

Country Status (9)

Country	Link
US (1)	US3509206A (fr)
CH (1)	CH484041A (fr)
DE (1)	DE1668585B2 (fr)
DK (1)	DK128605B (fr)
FR (1)	FR1556567A (fr)
GB (1)	GB1171273A (fr)
NL (1)	NL6802005A (fr)
NO (1)	NO129344B (fr)
SE (1)	SE358150B (fr)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2504235C3 (de) *	1975-02-01	1979-04-19	Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt	Verfahren zur Herstellung von Alkylsulfonsäuren
US4035242A (en) *	1975-09-29	1977-07-12	Ppg Industries, Inc.	Distillative purification of alkane sulfonic acids
US4450047A (en) *	1983-01-28	1984-05-22	Penwalt Corporation	Process for recovering anhydrous alkanesulfonic acids by reduced pressure, falling film evaporation
US4938846A (en) *	1986-12-08	1990-07-03	Atochem, North America, Inc.	Preparation of anhydrous alkanesulfonic acid
US4956494A (en) *	1987-10-26	1990-09-11	Pennwalt Corporation	Oxidation of thiols, disulfides and thiolsulfonates
US5485351A (en) *	1989-06-09	1996-01-16	Labinal Components And Systems, Inc.	Socket assembly for integrated circuit chip package
US5127837A (en) *	1989-06-09	1992-07-07	Labinal Components And Systems, Inc.	Electrical connectors and IC chip tester embodying same
DE10297842T5 (de) *	2002-12-27	2005-10-27	Council Of Scientific And Industrial Research	Verfahren zur Herstellung von Alkansulfonsäure
CA3074199A1 (fr)	2020-02-28	2021-08-28	Fluid Energy Group Ltd.	Acide sulfurique modifie et utilisations connexes
CA3074198A1 (fr) *	2020-02-28	2021-08-28	Fluid Energy Group Ltd.	Acide methanesulfonique modifie et utilisations connexes

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB522840A (en) *	1937-12-18	1940-06-28	Du Pont	Manufacture of surface-active compounds
US2667507A (en) *	1950-08-31	1954-01-26	Celanese Corp	Preparation of disulfonic acids
USB61008I5 (fr) *	1958-04-03
US3143562A (en) *	1961-03-27	1964-08-04	Leonard S Silbert	Preparation of aromatic peroxy acids
US3079411A (en) *	1961-04-24	1963-02-26	Leonard S Silbert	Preparation of long-chain aliphatic peroxy acids

1967
- 1967-03-01 US US619576A patent/US3509206A/en not_active Expired - Lifetime
1968
- 1968-02-13 NL NL6802005A patent/NL6802005A/xx unknown
- 1968-02-17 DE DE1668585A patent/DE1668585B2/de active Granted
- 1968-02-21 CH CH252268A patent/CH484041A/fr not_active IP Right Cessation
- 1968-02-26 FR FR141245A patent/FR1556567A/fr not_active Expired
- 1968-02-28 SE SE02591/68A patent/SE358150B/xx unknown
- 1968-02-29 NO NO00751/68A patent/NO129344B/no unknown
- 1968-02-29 DK DK80168AA patent/DK128605B/da unknown
- 1968-02-29 GB GB9760/68A patent/GB1171273A/en not_active Expired

Also Published As

Publication number	Publication date
US3509206A (en)	1970-04-28
DE1668585B2 (de)	1975-11-13
FR1556567A (fr)	1969-02-07
DK128605B (da)	1974-06-04
SE358150B (fr)	1973-07-23
CH484041A (fr)	1970-01-15
NL6802005A (fr)	1968-09-02
GB1171273A (en)	1969-11-19
DE1668585A1 (de)	1971-06-03

Publication	Publication Date	Title
DE2812573A1 (de)	1978-10-05	Peroxycarbonsaeuren und verfahren zu deren herstellung
NO139465B (no)	1978-12-11	Ski med loepeflatebelegg.
EP0055951B1 (fr)	1984-05-30	Procédé pour la préparation de l'anthraquinone et de ses dérivés substitués
ES2927541T3 (es)	2022-11-08	Proceso para producir sulfona de 4,4-diclorodifenilo
US3509206A (en)	1970-04-28	Alkanesulfonic acid preparation
EP0553797A1 (fr)	1993-08-04	Préparation de polysulfures de haute pureté
FI80672B (fi)	1990-03-30	Foerfarande foer framstaellning av para-acyloxibensensulfonater medelst syrakatalys.
KR0139295B1 (ko)	1998-05-15	N - 아미드계 헤테로 원자를 갖는 신규 헤테로환식 퍼옥시산
US4381222A (en)	1983-04-26	Process for the distillative separation of tertiary alkyl hydroperoxides and ditertiary alkyl peroxides
US3231605A (en)	1966-01-25	Method for distilling and recovering organic peroxy acids
US6603036B2 (en)	2003-08-05	Process for the manufacture of 2-ethylhexyl acrylate
EP0378873B1 (fr)	1993-02-03	Régénération d'acide sulfurique épuisée au moyen d'eau oxygénée
CA1203371A (fr)	1986-04-22	Preparation de solutions anhydres d'hydroperoxyde organique
FR2439184A1 (fr)	1980-05-16
FR2649099A1 (fr)	1991-01-04	Procede de purification des trifluoromethanesulfinate et sulfonate de sodium
US4866190A (en)	1989-09-12	Process for the preparation of perhaloalkanesulfinic and -sulfonic acids, perhaloalkanesulfinic and -sulfonic acid salts and other derivatives of these acids
US4966731A (en)	1990-10-30	Process for preparing sulfonyl acids
US5396003A (en)	1995-03-07	Recovery and purification of 1,1,2-trichloroethane for reuse in the production of ioversol
JPS63196539A (ja)	1988-08-15	高純度のテトラクロロ−１，４−ベンゾキノンの製造方法
JP2022548557A (ja)	2022-11-21	過酸化水素水溶液の製造方法
JPS60105690A (ja)	1985-06-11	蔗糖脂肪酸エステルの精製方法
US3014070A (en)	1961-12-19	Dibasic acid treating process
JPH0782247A (ja)	1995-03-28	第３級ブチルハイドロパーオキシド含有混合物の製造方法
DE3539036A1 (de)	1987-05-07	In 2-stellung substituierte diperoxyglutarsaeuren, ein verfahren zur herstellung und ihre verwendung
US1863698A (en)	1932-06-21	Process of purifying and concentrating acetic acid