NO20023633L - Fremgangsmåte for tilvirkning av piperonal - Google Patents
Fremgangsmåte for tilvirkning av piperonalInfo
- Publication number
- NO20023633L NO20023633L NO20023633A NO20023633A NO20023633L NO 20023633 L NO20023633 L NO 20023633L NO 20023633 A NO20023633 A NO 20023633A NO 20023633 A NO20023633 A NO 20023633A NO 20023633 L NO20023633 L NO 20023633L
- Authority
- NO
- Norway
- Prior art keywords
- acid
- organic solvent
- piperonal
- methylenedioxymandelic
- layer
- Prior art date
Links
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 title abstract 6
- 229940081310 piperonal Drugs 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000003960 organic solvent Substances 0.000 abstract 4
- CLUJFRCEPFNVHW-UHFFFAOYSA-N 3,4-methylenedioxymandelic acid Chemical compound OC(=O)C(O)C1=CC=C2OCOC2=C1 CLUJFRCEPFNVHW-UHFFFAOYSA-N 0.000 abstract 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 2
- HHLFWLYXYJOTON-UHFFFAOYSA-N glyoxylic acid Chemical compound OC(=O)C=O HHLFWLYXYJOTON-UHFFFAOYSA-N 0.000 abstract 2
- 229910017604 nitric acid Inorganic materials 0.000 abstract 2
- FTNJQNQLEGKTGD-UHFFFAOYSA-N 1,3-benzodioxole Chemical compound C1=CC=C2OCOC2=C1 FTNJQNQLEGKTGD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 238000007259 addition reaction Methods 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/44—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D317/46—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
- C07D317/48—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
- C07D317/50—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to atoms of the carbocyclic ring
- C07D317/54—Radicals substituted by oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Hydrogenated Pyridines (AREA)
- Plural Heterocyclic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2000024638 | 2000-02-02 | ||
| PCT/JP2001/000739 WO2001057016A1 (en) | 2000-02-02 | 2001-02-02 | Process for preparing piperonal |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20023633D0 NO20023633D0 (no) | 2002-07-31 |
| NO20023633L true NO20023633L (no) | 2002-08-28 |
| NO327235B1 NO327235B1 (no) | 2009-05-18 |
Family
ID=18550592
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20023633A NO327235B1 (no) | 2000-02-02 | 2002-07-31 | Fremgangsmate for tilvirkning av piperonal |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6686482B2 (no) |
| EP (1) | EP1253147B1 (no) |
| CN (1) | CN1159309C (no) |
| AT (1) | ATE273969T1 (no) |
| NO (1) | NO327235B1 (no) |
| TW (1) | TWI291954B (no) |
| WO (1) | WO2001057016A1 (no) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100335476C (zh) * | 2005-12-14 | 2007-09-05 | 四川大学 | 以对甲基苯酚为原料制备洋茉莉醛的方法 |
| JP5494488B2 (ja) * | 2008-10-07 | 2014-05-14 | 宇部興産株式会社 | 芳香族アルデヒド化合物の製造法 |
| CN101659650B (zh) * | 2009-09-24 | 2012-09-05 | 上海力智生化科技有限公司 | 一锅法制备洋茉莉醛的方法 |
| CN101899033B (zh) * | 2010-04-29 | 2012-05-23 | 东营益盟盛化工有限公司 | 洋茉莉醛的化学合成制备方法 |
| CN103724316B (zh) * | 2013-12-20 | 2016-02-10 | 暨南大学 | 芝麻酚中间产物胡椒醛的制备方法与应用 |
| CN103923056B (zh) * | 2014-04-30 | 2016-05-25 | 成都建中香料香精有限公司 | 3,4-亚甲基二氧基苯甲醛的合成方法 |
| CN104151285A (zh) * | 2014-08-14 | 2014-11-19 | 江苏亚泰化工有限公司 | 一种制备3,4-亚甲二氧基杏仁酸的方法 |
| CN105777705B (zh) * | 2016-04-01 | 2018-09-21 | 福建仁宏医药化工有限公司 | 一种洋茉莉醛中间体合成反应后期处理方法 |
| CN105777704A (zh) * | 2016-04-01 | 2016-07-20 | 衢州信步化工科技有限公司 | 一种洋茉莉醛的双塔连续化精馏工艺 |
| CN105693688B (zh) * | 2016-04-01 | 2019-07-05 | 福建仁宏医药化工有限公司 | 一种洋茉莉醛中间体3,4-亚甲二氧基苯乙醇酸的反应处理方法 |
| CN106349209A (zh) * | 2016-08-25 | 2017-01-25 | 宿迁市万和泰化工有限公司 | 一种洋茉莉醛的合成工艺 |
| CN106349208A (zh) * | 2016-08-25 | 2017-01-25 | 宿迁市万和泰化工有限公司 | 一种洋茉莉醛的制备方法 |
| CN117143069A (zh) * | 2023-09-07 | 2023-12-01 | 玉溪健坤生物药业有限公司 | 一种3,4-亚甲二氧基苯乙醇酸及胡椒醛的制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2754490A1 (de) | 1977-12-07 | 1979-06-13 | Haarmann & Reimer Gmbh | Verfahren zur herstellung von 3,4-methylendioxymandelsaeure |
| JP3282372B2 (ja) | 1994-06-07 | 2002-05-13 | 宇部興産株式会社 | ピペロナールの製法 |
| JPH0899971A (ja) | 1994-09-30 | 1996-04-16 | Ube Ind Ltd | ピペロナールの精製方法 |
-
2001
- 2001-01-31 TW TW090101857A patent/TWI291954B/zh not_active IP Right Cessation
- 2001-02-02 WO PCT/JP2001/000739 patent/WO2001057016A1/ja not_active Ceased
- 2001-02-02 AT AT01904315T patent/ATE273969T1/de active
- 2001-02-02 CN CNB018043488A patent/CN1159309C/zh not_active Expired - Fee Related
- 2001-02-02 EP EP01904315A patent/EP1253147B1/en not_active Expired - Lifetime
- 2001-02-02 US US10/182,485 patent/US6686482B2/en not_active Expired - Fee Related
-
2002
- 2002-07-31 NO NO20023633A patent/NO327235B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| NO20023633D0 (no) | 2002-07-31 |
| US6686482B2 (en) | 2004-02-03 |
| EP1253147B1 (en) | 2004-08-18 |
| EP1253147A4 (en) | 2003-05-28 |
| US20030013897A1 (en) | 2003-01-16 |
| EP1253147A1 (en) | 2002-10-30 |
| CN1400972A (zh) | 2003-03-05 |
| WO2001057016A1 (en) | 2001-08-09 |
| CN1159309C (zh) | 2004-07-28 |
| ATE273969T1 (de) | 2004-09-15 |
| TWI291954B (no) | 2008-01-01 |
| NO327235B1 (no) | 2009-05-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM1K | Lapsed by not paying the annual fees |