NO314169B1 - Fremgangsmåte ved behandling av en katalysator, samt en form for fremstilling av hydrogenperoksyd - Google Patents

Fremgangsmåte ved behandling av en katalysator, samt en form for fremstilling av hydrogenperoksyd Download PDF

Info

Publication number: NO314169B1
Authority: NO; Norway
Prior art keywords: catalyst; acid; hydrogenation; hydrogen peroxide; anthraquinones
Prior art date: 1995-12-04

Application number

NO19965069A

Other languages

English (en)

Norwegian (no)

Other versions

NO965069L (no

NO965069D0 (no

Inventor

Mats Nystroem

Mikael Siverstroem

Original Assignee

Eka Chemicals Ab

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1995-12-04

Filing date

1996-11-28

Publication date

2003-02-10

1996-11-28 Application filed by Eka Chemicals Ab filed Critical Eka Chemicals Ab

1996-11-28 Publication of NO965069D0 publication Critical patent/NO965069D0/no

1997-06-05 Publication of NO965069L publication Critical patent/NO965069L/no

2003-02-10 Publication of NO314169B1 publication Critical patent/NO314169B1/no

Links

239000003054 catalyst Substances 0.000 title claims description 54
238000000034 method Methods 0.000 title claims description 32
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims description 28
230000008569 process Effects 0.000 title claims description 6
239000002253 acid Substances 0.000 claims description 20
238000005984 hydrogenation reaction Methods 0.000 claims description 19
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 12
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
150000004056 anthraquinones Chemical class 0.000 claims description 12
238000004519 manufacturing process Methods 0.000 claims description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
230000000694 effects Effects 0.000 claims description 9
239000003960 organic solvent Substances 0.000 claims description 9
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 8
KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 8
229910017604 nitric acid Inorganic materials 0.000 claims description 8
239000012224 working solution Substances 0.000 claims description 8
150000007513 acids Chemical class 0.000 claims description 7
239000000203 mixture Substances 0.000 claims description 7
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 6
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 6
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 5
230000003213 activating effect Effects 0.000 claims description 5
239000011149 active material Substances 0.000 claims description 5
PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims description 4
229910052763 palladium Inorganic materials 0.000 claims description 4
KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 3
230000004913 activation Effects 0.000 claims description 3
125000001931 aliphatic group Chemical group 0.000 claims description 3
125000003118 aryl group Chemical group 0.000 claims description 3
229930195733 hydrocarbon Natural products 0.000 claims description 3
150000002430 hydrocarbons Chemical class 0.000 claims description 3
229910052500 inorganic mineral Inorganic materials 0.000 claims description 3
239000011707 mineral Substances 0.000 claims description 3
229910052697 platinum Inorganic materials 0.000 claims description 3
229910052703 rhodium Inorganic materials 0.000 claims description 3
239000010948 rhodium Substances 0.000 claims description 3
MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims description 3
229910052707 ruthenium Inorganic materials 0.000 claims description 3
238000010306 acid treatment Methods 0.000 claims description 2
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
229910052759 nickel Inorganic materials 0.000 claims description 2
235000006408 oxalic acid Nutrition 0.000 claims description 2
230000003647 oxidation Effects 0.000 claims description 2
238000007254 oxidation reaction Methods 0.000 claims description 2
238000005406 washing Methods 0.000 claims description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
-1 alkyl anthraquinones Chemical class 0.000 description 6
239000002904 solvent Substances 0.000 description 6
239000008367 deionised water Substances 0.000 description 5
229910021641 deionized water Inorganic materials 0.000 description 5
235000011007 phosphoric acid Nutrition 0.000 description 5
AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 4
QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
238000001035 drying Methods 0.000 description 4
YTZKOQUCBOVLHL-UHFFFAOYSA-N tert-butylbenzene Chemical compound CC(C)(C)C1=CC=CC=C1 YTZKOQUCBOVLHL-UHFFFAOYSA-N 0.000 description 4
150000005208 1,4-dihydroxybenzenes Chemical class 0.000 description 3
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
229910052749 magnesium Inorganic materials 0.000 description 3
239000011777 magnesium Substances 0.000 description 3
FYGHSUNMUKGBRK-UHFFFAOYSA-N 1,2,3-trimethylbenzene Chemical compound CC1=CC=CC(C)=C1C FYGHSUNMUKGBRK-UHFFFAOYSA-N 0.000 description 2
AXHVNJGQOJFMHT-UHFFFAOYSA-N 1-tert-butyl-2-methylbenzene Chemical compound CC1=CC=CC=C1C(C)(C)C AXHVNJGQOJFMHT-UHFFFAOYSA-N 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 2
239000004411 aluminium Substances 0.000 description 2
229910052782 aluminium Inorganic materials 0.000 description 2
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
229910021529 ammonia Inorganic materials 0.000 description 2
239000007864 aqueous solution Substances 0.000 description 2
230000008901 benefit Effects 0.000 description 2
150000001555 benzenes Chemical class 0.000 description 2
238000009835 boiling Methods 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
150000004649 carbonic acid derivatives Chemical class 0.000 description 2
239000012876 carrier material Substances 0.000 description 2
239000007788 liquid Substances 0.000 description 2
TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
239000002245 particle Substances 0.000 description 2
VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 2
150000004053 quinones Chemical class 0.000 description 2
229910052814 silicon oxide Inorganic materials 0.000 description 2
239000000243 solution Substances 0.000 description 2
230000003068 static effect Effects 0.000 description 2
239000010936 titanium Substances 0.000 description 2
229910052719 titanium Inorganic materials 0.000 description 2
150000003613 toluenes Chemical class 0.000 description 2
229910052726 zirconium Inorganic materials 0.000 description 2
SJEBAWHUJDUKQK-UHFFFAOYSA-N 2-ethylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(CC)=CC=C3C(=O)C2=C1 SJEBAWHUJDUKQK-UHFFFAOYSA-N 0.000 description 1
HTNXCDCAXMXXMR-UHFFFAOYSA-N 2-hex-1-enylanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C=CCCCC)=CC=C3C(=O)C2=C1 HTNXCDCAXMXXMR-UHFFFAOYSA-N 0.000 description 1
UMWZLYTVXQBTTE-UHFFFAOYSA-N 2-pentylanthracene-9,10-dione Chemical class C1=CC=C2C(=O)C3=CC(CCCCC)=CC=C3C(=O)C2=C1 UMWZLYTVXQBTTE-UHFFFAOYSA-N 0.000 description 1
YTPSFXZMJKMUJE-UHFFFAOYSA-N 2-tert-butylanthracene-9,10-dione Chemical compound C1=CC=C2C(=O)C3=CC(C(C)(C)C)=CC=C3C(=O)C2=C1 YTPSFXZMJKMUJE-UHFFFAOYSA-N 0.000 description 1
ZMGMDXCADSRNCX-UHFFFAOYSA-N 5,6-dihydroxy-1,3-diazepan-2-one Chemical class OC1CNC(=O)NCC1O ZMGMDXCADSRNCX-UHFFFAOYSA-N 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
239000007868 Raney catalyst Substances 0.000 description 1
229910000564 Raney nickel Inorganic materials 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
229910052783 alkali metal Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
229910052784 alkaline earth metal Inorganic materials 0.000 description 1
150000001342 alkaline earth metals Chemical class 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
125000005600 alkyl phosphonate group Chemical group 0.000 description 1
150000001408 amides Chemical class 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
229910052788 barium Inorganic materials 0.000 description 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
239000011575 calcium Substances 0.000 description 1
239000004202 carbamide Substances 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
230000009849 deactivation Effects 0.000 description 1
230000007423 decrease Effects 0.000 description 1
239000000374 eutectic mixture Substances 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
LJOQGZACKSYWCH-WZBLMQSHSA-N hydroquinine Chemical compound C1=C(OC)C=C2C([C@@H](O)[C@@H]3C[C@@H]4CCN3C[C@@H]4CC)=CC=NC2=C1 LJOQGZACKSYWCH-WZBLMQSHSA-N 0.000 description 1
229960004251 hydroquinine Drugs 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
239000000463 material Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
150000001247 metal acetylides Chemical class 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
229910000510 noble metal Inorganic materials 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
235000005985 organic acids Nutrition 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
239000003495 polar organic solvent Substances 0.000 description 1
230000007420 reactivation Effects 0.000 description 1
150000004760 silicates Chemical class 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
229910052712 strontium Inorganic materials 0.000 description 1
CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
- B01J38/60—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/90—Regeneration or reactivation
- B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/06—Washing
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

NO19965069A 1995-12-04 1996-11-28 Fremgangsmåte ved behandling av en katalysator, samt en form for fremstilling av hydrogenperoksyd NO314169B1 (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
SE9504327A SE9504327D0 (sv)	1995-12-04	1995-12-04	Method of treating a catalyst

Publications (3)

Publication Number	Publication Date
NO965069D0 NO965069D0 (no)	1996-11-28
NO965069L NO965069L (no)	1997-06-05
NO314169B1 true NO314169B1 (no)	2003-02-10

Family

ID=20400456

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO19965069A NO314169B1 (no)	1995-12-04	1996-11-28	Fremgangsmåte ved behandling av en katalysator, samt en form for fremstilling av hydrogenperoksyd

Country Status (10)

Country	Link
US (1)	US5985235A (de)
EP (1)	EP0778085B1 (de)
JP (1)	JP3408937B2 (de)
AT (1)	ATE193227T1 (de)
CA (1)	CA2191687C (de)
DE (1)	DE69608528T2 (de)
ES (1)	ES2145969T3 (de)
NO (1)	NO314169B1 (de)
PT (1)	PT778085E (de)
SE (1)	SE9504327D0 (de)

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DE10048844A1 (de) *	2000-10-02	2002-04-11	Basf Ag	Verfahren zur Herstellung von Platinmetall-Katalysatoren
EP1350761A1 (de)	2002-03-28	2003-10-08	Degussa AG	Verfahren zur Herstellung von Wasserstoffperoxid
CN101296860B (zh) *	2005-08-31	2012-08-29	Fmc有限公司	在微反应器中通过加氢自动氧化生产过氧化氢
JP5098215B2 (ja)	2006-05-01	2012-12-12	三菱瓦斯化学株式会社	水素化触媒の賦活方法およびそれを含む過酸化水素の製造方法
KR102055389B1 (ko) *	2013-11-26	2019-12-12	에스케이이노베이션 주식회사	황산 처리된 Pt-Pd 담지 고분자 전해질 다층박막 촉매의 제조방법
CN113135818B (zh) *	2020-01-20	2022-07-12	中国石油化工股份有限公司	一种烷基蒽醌氢化的方法
CN115445621B (zh) *	2022-08-26	2023-08-22	中触媒新材料股份有限公司	一种蒽醌法生产双氧水用镍基催化剂的制备方法及应用
CN117548043B (zh) *	2024-01-09	2024-04-02	黎明化工研究设计院有限责任公司	一种蒽醌法生产过氧化氢的流化床氢化装置及其使用方法

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GB9114314D0 (en) *	1991-07-02	1991-08-21	British Petroleum Co Plc	Catalyst treatment for fisher-tropsch process
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FI94515B (fi)	1994-03-04	1995-06-15	Finnish Chemicals Oy	Menetelmä hydrauskatalyytin reaktivoimiseksi
US5654254A (en) *	1995-06-23	1997-08-05	Phillips Petroleum Company	Preparation of hydrocarbon isomerization catalyst

1995
- 1995-12-04 SE SE9504327A patent/SE9504327D0/xx unknown
1996
- 1996-11-18 PT PT96203217T patent/PT778085E/pt unknown
- 1996-11-18 EP EP96203217A patent/EP0778085B1/de not_active Expired - Lifetime
- 1996-11-18 AT AT96203217T patent/ATE193227T1/de active
- 1996-11-18 DE DE69608528T patent/DE69608528T2/de not_active Expired - Lifetime
- 1996-11-18 ES ES96203217T patent/ES2145969T3/es not_active Expired - Lifetime
- 1996-11-28 NO NO19965069A patent/NO314169B1/no not_active IP Right Cessation
- 1996-11-29 CA CA002191687A patent/CA2191687C/en not_active Expired - Fee Related
- 1996-12-03 JP JP33630196A patent/JP3408937B2/ja not_active Expired - Lifetime
- 1996-12-03 US US08/759,807 patent/US5985235A/en not_active Expired - Lifetime

Also Published As

Publication number	Publication date
EP0778085B1 (de)	2000-05-24
PT778085E (pt)	2000-08-31
SE9504327D0 (sv)	1995-12-04
US5985235A (en)	1999-11-16
JPH09173872A (ja)	1997-07-08
CA2191687C (en)	2001-06-05
CA2191687A1 (en)	1997-06-05
ATE193227T1 (de)	2000-06-15
NO965069L (no)	1997-06-05
EP0778085A1 (de)	1997-06-11
ES2145969T3 (es)	2000-07-16
JP3408937B2 (ja)	2003-05-19
NO965069D0 (no)	1996-11-28
DE69608528D1 (de)	2000-06-29
DE69608528T2 (de)	2001-01-18

Legal Events

Date	Code	Title	Description
2015-06-22	MM1K	Lapsed by not paying the annual fees

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