NO761110L - - Google Patents

Info

Publication number: NO761110L
Authority: NO; Norway
Prior art keywords: product; polymer; saponified; block copolymer; weight
Prior art date: 1975-04-01

Application number

NO761110A

Other languages

English (en)

Norwegian (no)

Inventor

D M Mcclain

B L Vest

Original Assignee

Nat Distillers Chem Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-04-01

Filing date

1976-03-31

Publication date

1976-10-04

1976-03-31 Application filed by Nat Distillers Chem Corp filed Critical Nat Distillers Chem Corp

1976-10-04 Publication of NO761110L publication Critical patent/NO761110L/no

Links

238000000034 method Methods 0.000 claims description 52
239000006185 dispersion Substances 0.000 claims description 38
229920000642 polymer Polymers 0.000 claims description 33
238000007127 saponification reaction Methods 0.000 claims description 33
239000002245 particle Substances 0.000 claims description 30
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 25
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
239000002270 dispersing agent Substances 0.000 claims description 24
229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 claims description 21
238000003756 stirring Methods 0.000 claims description 20
150000003839 salts Chemical class 0.000 claims description 18
239000005038 ethylene vinyl acetate Substances 0.000 claims description 16
-1 oxyethylene-oxypropylene Chemical group 0.000 claims description 16
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 14
229920001400 block copolymer Polymers 0.000 claims description 14
150000007529 inorganic bases Chemical class 0.000 claims description 11
DQXBYHZEEUGOBF-UHFFFAOYSA-N but-3-enoic acid;ethene Chemical compound C=C.OC(=O)CC=C DQXBYHZEEUGOBF-UHFFFAOYSA-N 0.000 claims description 9
238000000354 decomposition reaction Methods 0.000 claims description 8
150000001768 cations Chemical class 0.000 claims description 7
238000005406 washing Methods 0.000 claims description 7
238000001816 cooling Methods 0.000 claims description 5
230000015572 biosynthetic process Effects 0.000 claims description 4
125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 claims 1
239000000047 product Substances 0.000 description 42
239000000843 powder Substances 0.000 description 12
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical group CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 11
239000012798 spherical particle Substances 0.000 description 10
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 9
229920001577 copolymer Polymers 0.000 description 9
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 8
239000002585 base Substances 0.000 description 8
239000003795 chemical substances by application Substances 0.000 description 7
230000007062 hydrolysis Effects 0.000 description 7
238000006460 hydrolysis reaction Methods 0.000 description 7
229920005989 resin Polymers 0.000 description 7
239000011347 resin Substances 0.000 description 7
RVGRUAULSDPKGF-UHFFFAOYSA-N Poloxamer Chemical compound C1CO1.CC1CO1 RVGRUAULSDPKGF-UHFFFAOYSA-N 0.000 description 6
238000006136 alcoholysis reaction Methods 0.000 description 6
239000000203 mixture Substances 0.000 description 6
229910052708 sodium Inorganic materials 0.000 description 6
239000011734 sodium Substances 0.000 description 6
239000012736 aqueous medium Substances 0.000 description 5
238000000576 coating method Methods 0.000 description 5
238000009826 distribution Methods 0.000 description 5
239000007788 liquid Substances 0.000 description 5
239000002904 solvent Substances 0.000 description 5
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
239000004094 surface-active agent Substances 0.000 description 4
WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
150000001875 compounds Chemical class 0.000 description 3
239000012153 distilled water Substances 0.000 description 3
230000000694 effects Effects 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
238000001914 filtration Methods 0.000 description 3
238000002844 melting Methods 0.000 description 3
230000008018 melting Effects 0.000 description 3
229920001451 polypropylene glycol Polymers 0.000 description 3
239000007787 solid Substances 0.000 description 3
239000000243 solution Substances 0.000 description 3
229920005992 thermoplastic resin Polymers 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
SOGAXMICEFXMKE-UHFFFAOYSA-N Butylmethacrylate Chemical compound CCCCOC(=O)C(C)=C SOGAXMICEFXMKE-UHFFFAOYSA-N 0.000 description 2
229920005682 EO-PO block copolymer Polymers 0.000 description 2
BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 description 2
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
238000006243 chemical reaction Methods 0.000 description 2
239000011362 coarse particle Substances 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
230000001419 dependent effect Effects 0.000 description 2
239000012467 final product Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
230000001788 irregular Effects 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
239000002609 medium Substances 0.000 description 2
239000000155 melt Substances 0.000 description 2
239000002736 nonionic surfactant Substances 0.000 description 2
238000010422 painting Methods 0.000 description 2
239000008188 pellet Substances 0.000 description 2
239000004014 plasticizer Substances 0.000 description 2
229920000573 polyethylene Polymers 0.000 description 2
229920000098 polyolefin Polymers 0.000 description 2
238000011084 recovery Methods 0.000 description 2
230000001105 regulatory effect Effects 0.000 description 2
238000005245 sintering Methods 0.000 description 2
239000001632 sodium acetate Substances 0.000 description 2
235000017281 sodium acetate Nutrition 0.000 description 2
239000000758 substrate Substances 0.000 description 2
239000000725 suspension Substances 0.000 description 2
229920002554 vinyl polymer Polymers 0.000 description 2
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
239000004705 High-molecular-weight polyethylene Substances 0.000 description 1
VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
SUZRRICLUFMAQD-UHFFFAOYSA-N N-methyltaurine Natural products CNCCS(O)(=O)=O SUZRRICLUFMAQD-UHFFFAOYSA-N 0.000 description 1
229920002065 Pluronic® P 105 Polymers 0.000 description 1
229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
239000004698 Polyethylene Substances 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
159000000021 acetate salts Chemical class 0.000 description 1
125000003668 acetyloxy group Chemical group [H]C([H])([H])C(=O)O[*] 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000013543 active substance Substances 0.000 description 1
125000002252 acyl group Chemical group 0.000 description 1
239000000853 adhesive Substances 0.000 description 1
230000001070 adhesive effect Effects 0.000 description 1
238000013019 agitation Methods 0.000 description 1
238000003915 air pollution Methods 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
150000001447 alkali salts Chemical class 0.000 description 1
150000008055 alkyl aryl sulfonates Chemical class 0.000 description 1
150000008052 alkyl sulfonates Chemical class 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
238000010923 batch production Methods 0.000 description 1
CQEYYJKEWSMYFG-UHFFFAOYSA-N butyl acrylate Chemical compound CCCCOC(=O)C=C CQEYYJKEWSMYFG-UHFFFAOYSA-N 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
239000000969 carrier Substances 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
238000005520 cutting process Methods 0.000 description 1
238000010908 decantation Methods 0.000 description 1
230000008021 deposition Effects 0.000 description 1
JBSLOWBPDRZSMB-BQYQJAHWSA-N dibutyl (e)-but-2-enedioate Chemical compound CCCCOC(=O)\C=C\C(=O)OCCCC JBSLOWBPDRZSMB-BQYQJAHWSA-N 0.000 description 1
ZEFVHSWKYCYFFL-UHFFFAOYSA-N diethyl 2-methylidenebutanedioate Chemical compound CCOC(=O)CC(=C)C(=O)OCC ZEFVHSWKYCYFFL-UHFFFAOYSA-N 0.000 description 1
CYWQFUQJVLRILO-UHFFFAOYSA-N diethyl 2-methylidenepentanedioate Chemical compound CCOC(=O)CCC(=C)C(=O)OCC CYWQFUQJVLRILO-UHFFFAOYSA-N 0.000 description 1
IEPRKVQEAMIZSS-AATRIKPKSA-N diethyl fumarate Chemical compound CCOC(=O)\C=C\C(=O)OCC IEPRKVQEAMIZSS-AATRIKPKSA-N 0.000 description 1
URLYMBMJTPDVEP-UHFFFAOYSA-N dimethyl 2-methylidenepentanedioate Chemical compound COC(=O)CCC(=C)C(=O)OC URLYMBMJTPDVEP-UHFFFAOYSA-N 0.000 description 1
LDCRTTXIJACKKU-ARJAWSKDSA-N dimethyl maleate Chemical compound COC(=O)\C=C/C(=O)OC LDCRTTXIJACKKU-ARJAWSKDSA-N 0.000 description 1
239000000975 dye Substances 0.000 description 1
238000007610 electrostatic coating method Methods 0.000 description 1
239000000839 emulsion Substances 0.000 description 1
150000002168 ethanoic acid esters Chemical class 0.000 description 1
229920001038 ethylene copolymer Polymers 0.000 description 1
238000000605 extraction Methods 0.000 description 1
230000002349 favourable effect Effects 0.000 description 1
239000000835 fiber Substances 0.000 description 1
239000010419 fine particle Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
239000008187 granular material Substances 0.000 description 1
GGQOPZKTDHXXON-UHFFFAOYSA-N hexane;methanol Chemical compound OC.CCCCCC GGQOPZKTDHXXON-UHFFFAOYSA-N 0.000 description 1
230000003301 hydrolyzing effect Effects 0.000 description 1
239000004816 latex Substances 0.000 description 1
229920000126 latex Polymers 0.000 description 1
239000000463 material Substances 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
239000012046 mixed solvent Substances 0.000 description 1
239000000178 monomer Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
239000012071 phase Substances 0.000 description 1
239000000049 pigment Substances 0.000 description 1
229920001983 poloxamer Polymers 0.000 description 1
230000000379 polymerizing effect Effects 0.000 description 1
150000003138 primary alcohols Chemical class 0.000 description 1
NHARPDSAXCBDDR-UHFFFAOYSA-N propyl 2-methylprop-2-enoate Chemical compound CCCOC(=O)C(C)=C NHARPDSAXCBDDR-UHFFFAOYSA-N 0.000 description 1
PNXMTCDJUBJHQJ-UHFFFAOYSA-N propyl prop-2-enoate Chemical compound CCCOC(=O)C=C PNXMTCDJUBJHQJ-UHFFFAOYSA-N 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
238000010008 shearing Methods 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
238000001694 spray drying Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
238000005809 transesterification reaction Methods 0.000 description 1
239000011882 ultra-fine particle Substances 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/12—Hydrolysis
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2810/00—Chemical modification of a polymer
- C08F2810/50—Chemical modification of a polymer wherein the polymer is a copolymer and the modification is taking place only on one or more of the monomers present in minority

Landscapes

Chemical & Material Sciences (AREA)
General Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Processes Of Treating Macromolecular Substances (AREA)

NO761110A 1975-04-01 1976-03-31 NO761110L (es)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US05/564,200 US4027079A (en)	1975-04-01	1975-04-01	Finely divided saponified ethylene-vinyl acetate interpolymers

Publications (1)

Publication Number	Publication Date
NO761110L true NO761110L (es)	1976-10-04

Family

ID=24253544

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO761110A NO761110L (es)	1975-04-01	1976-03-31

Country Status (16)

Country	Link
US (1)	US4027079A (es)
JP (1)	JPS51122190A (es)
AU (1)	AU1249276A (es)
BE (1)	BE840290A (es)
BR (1)	BR7601957A (es)
DE (1)	DE2614070A1 (es)
DK (1)	DK144276A (es)
ES (1)	ES446594A1 (es)
FI (1)	FI760883A7 (es)
FR (1)	FR2306220A1 (es)
GB (1)	GB1548653A (es)
IT (1)	IT1058897B (es)
LU (1)	LU74673A1 (es)
NL (1)	NL7603407A (es)
NO (1)	NO761110L (es)
SE (1)	SE7603854L (es)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS51126291A (en) *	1975-04-25	1976-11-04	Toyo Soda Mfg Co Ltd	Process for preparing a saponfied ethyhlenevinyl acetate copolymer hav ing high whiteness
US4104453A (en) *	1977-07-05	1978-08-01	National Distillers And Chemical Corporation	Melt dispersion saponification of ethylene-vinyl acetate polymer
US4151134A (en) *	1977-08-15	1979-04-24	National Distillers And Chemical Corporation	Process for simultaneously dispersing and saponifying ethylene-vinyl acetate copolymer
DE2830328C2 (de) *	1978-07-10	1982-09-16	Ruhrchemie Ag, 4200 Oberhausen	Mischpolymerisate des Äthylens und ihre Verwendung zur Herstellung von Schaumstoffen
US4309525A (en) *	1979-05-21	1982-01-05	Takeda Chemical Industries, Ltd.	Production of sphere-formed powdery copolymers
US4389506A (en) *	1981-06-29	1983-06-21	E. I. Du Pont De Nemours And Company	Polyvinyl alcohol dust suppression by admixing polyglycol
US5753753A (en) *	1997-02-19	1998-05-19	Air Products And Chemicals, Inc.	Hydrolysis of polyvinyl aklaenoates
DE10321942A1 (de) *	2003-05-15	2004-12-09	Wacker Polymer Systems Gmbh & Co. Kg	Verfahren zur Herstellung von pulverförmigen Ethylen-Vinylalkohol-Mischpolymerisaten
US8247155B2 (en) *	2008-01-16	2012-08-21	Penn Color, Inc.	Production of toner for use in printing applications
US8652745B2 (en)	2008-01-16	2014-02-18	Penn Color, Inc.	Ink toner particles with controlled surface morphology

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE88404C (es) *
US2467774A (en) *	1945-02-16	1949-04-19	Du Pont	Process of hydrolyzing vinyl ester polymers
US3422049A (en) *	1961-12-20	1969-01-14	Nat Distillers Chem Corp	Process of preparing finely divided thermoplastic resins
US3547858A (en) *	1967-05-19	1970-12-15	Monsanto Chemicals	Hydrolysis of esters in the molten state

1975
- 1975-04-01 US US05/564,200 patent/US4027079A/en not_active Expired - Lifetime
1976
- 1976-03-30 DK DK144276A patent/DK144276A/da not_active IP Right Cessation
- 1976-03-30 FR FR7609218A patent/FR2306220A1/fr active Granted
- 1976-03-30 AU AU12492/76A patent/AU1249276A/en not_active Expired
- 1976-03-31 GB GB13000/76A patent/GB1548653A/en not_active Expired
- 1976-03-31 SE SE7603854A patent/SE7603854L/xx unknown
- 1976-03-31 IT IT21774/76A patent/IT1058897B/it active
- 1976-03-31 NO NO761110A patent/NO761110L/no unknown
- 1976-03-31 BR BR7601957A patent/BR7601957A/pt unknown
- 1976-03-31 LU LU74673A patent/LU74673A1/xx unknown
- 1976-04-01 FI FI760883A patent/FI760883A7/fi not_active Application Discontinuation
- 1976-04-01 JP JP51035211A patent/JPS51122190A/ja active Pending
- 1976-04-01 ES ES446594A patent/ES446594A1/es not_active Expired
- 1976-04-01 NL NL7603407A patent/NL7603407A/xx not_active Application Discontinuation
- 1976-04-01 DE DE19762614070 patent/DE2614070A1/de not_active Withdrawn
- 1976-04-01 BE BE165772A patent/BE840290A/xx unknown

Also Published As

Publication number	Publication date
SE7603854L (sv)	1976-10-02
IT1058897B (it)	1982-05-10
FR2306220B1 (es)	1980-08-14
US4027079A (en)	1977-05-31
DE2614070A1 (de)	1976-10-14
AU1249276A (en)	1977-10-20
DK144276A (da)	1976-10-02
BE840290A (fr)	1976-10-01
ES446594A1 (es)	1977-06-16
GB1548653A (en)	1979-07-18
FI760883A7 (es)	1976-10-02
BR7601957A (pt)	1976-10-05
JPS51122190A (en)	1976-10-26
FR2306220A1 (fr)	1976-10-29
NL7603407A (nl)	1976-10-05
LU74673A1 (es)	1976-09-01

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US4104453A (en)	1978-08-01	Melt dispersion saponification of ethylene-vinyl acetate polymer
NO761946L (es)	1976-12-10
US3347811A (en)	1967-10-17	Process for preparing aqueous dispersions of ethylene copolymers
GB1583235A (en)	1981-01-21	Process for preparing bead polymers
US4027079A (en)	1977-05-31	Finely divided saponified ethylene-vinyl acetate interpolymers
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US4148766A (en)	1979-04-10	Polymer dispersion process
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