NO780291L - Fremgangsmaate til fremstilling av vinylkloridpolymerisater - Google Patents

Fremgangsmaate til fremstilling av vinylkloridpolymerisater

Info

Publication number: NO780291L
Authority: NO; Norway
Prior art keywords: atoms; polymerization; coating; active substance; hydrazone
Prior art date: 1977-01-27

Application number

NO780291A

Other languages

English (en)

Norwegian (no)

Inventor

Edgar Fischer

Johannes Brandrup

Juergen Weinlich

Original Assignee

Hoechst Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1977-01-27

Filing date

1978-01-26

Publication date

1978-07-28

1978-01-26 Application filed by Hoechst Ag filed Critical Hoechst Ag

1978-07-28 Publication of NO780291L publication Critical patent/NO780291L/no

Links

238000000034 method Methods 0.000 title claims abstract description 39
BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 title claims abstract description 23
229920000642 polymer Polymers 0.000 claims abstract description 23
230000008569 process Effects 0.000 claims abstract description 6
238000000576 coating method Methods 0.000 claims description 52
238000006116 polymerization reaction Methods 0.000 claims description 52
239000013543 active substance Substances 0.000 claims description 44
239000011248 coating agent Substances 0.000 claims description 42
125000004432 carbon atom Chemical group C* 0.000 claims description 30
239000000203 mixture Substances 0.000 claims description 22
239000001257 hydrogen Substances 0.000 claims description 15
229910052739 hydrogen Inorganic materials 0.000 claims description 15
150000001875 compounds Chemical class 0.000 claims description 14
239000000178 monomer Substances 0.000 claims description 14
239000012876 carrier material Substances 0.000 claims description 12
239000003995 emulsifying agent Substances 0.000 claims description 10
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical group [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 8
125000000217 alkyl group Chemical group 0.000 claims description 7
239000006185 dispersion Substances 0.000 claims description 7
150000002431 hydrogen Chemical class 0.000 claims description 7
238000004519 manufacturing process Methods 0.000 claims description 6
239000000725 suspension Substances 0.000 claims description 6
125000003118 aryl group Chemical group 0.000 claims description 5
239000003054 catalyst Substances 0.000 claims description 5
125000002252 acyl group Chemical group 0.000 claims description 4
125000003282 alkyl amino group Chemical group 0.000 claims description 4
239000003381 stabilizer Substances 0.000 claims description 4
125000001118 alkylidene group Chemical group 0.000 claims description 3
229910052736 halogen Inorganic materials 0.000 claims description 3
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 3
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 2
150000002367 halogens Chemical class 0.000 claims description 2
125000004962 sulfoxyl group Chemical group 0.000 claims description 2
125000001183 hydrocarbyl group Chemical group 0.000 claims 3
-1 aliphatic acyl radical Chemical class 0.000 description 47
239000000243 solution Substances 0.000 description 39
239000000126 substance Substances 0.000 description 34
XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 17
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 15
229920001577 copolymer Polymers 0.000 description 14
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
239000000463 material Substances 0.000 description 11
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
238000001035 drying Methods 0.000 description 10
239000004848 polyfunctional curative Substances 0.000 description 10
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 9
150000008064 anhydrides Chemical class 0.000 description 9
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 8
229910001868 water Inorganic materials 0.000 description 8
239000002253 acid Substances 0.000 description 7
239000002904 solvent Substances 0.000 description 7
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 6
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
125000001931 aliphatic group Chemical group 0.000 description 6
239000002585 base Substances 0.000 description 6
230000000694 effects Effects 0.000 description 6
150000002118 epoxides Chemical class 0.000 description 6
RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 5
239000004593 Epoxy Substances 0.000 description 5
150000007513 acids Chemical class 0.000 description 5
239000000654 additive Substances 0.000 description 5
239000003513 alkali Substances 0.000 description 5
150000001412 amines Chemical class 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 5
239000001913 cellulose Substances 0.000 description 5
229920002678 cellulose Polymers 0.000 description 5
239000008367 deionised water Substances 0.000 description 5
238000011049 filling Methods 0.000 description 5
238000005755 formation reaction Methods 0.000 description 5
150000002430 hydrocarbons Chemical group 0.000 description 5
229910052751 metal Inorganic materials 0.000 description 5
238000012545 processing Methods 0.000 description 5
239000000047 product Substances 0.000 description 5
230000001681 protective effect Effects 0.000 description 5
150000003839 salts Chemical class 0.000 description 5
238000003756 stirring Methods 0.000 description 5
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 4
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical class [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 4
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 4
150000001298 alcohols Chemical class 0.000 description 4
239000000460 chlorine Substances 0.000 description 4
239000000084 colloidal system Substances 0.000 description 4
238000007334 copolymerization reaction Methods 0.000 description 4
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
229910021641 deionized water Inorganic materials 0.000 description 4
235000014113 dietary fatty acids Nutrition 0.000 description 4
238000006073 displacement reaction Methods 0.000 description 4
150000002148 esters Chemical class 0.000 description 4
239000000194 fatty acid Substances 0.000 description 4
229930195729 fatty acid Natural products 0.000 description 4
238000010438 heat treatment Methods 0.000 description 4
239000003999 initiator Substances 0.000 description 4
FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 4
239000002184 metal Substances 0.000 description 4
229920002689 polyvinyl acetate Polymers 0.000 description 4
239000011118 polyvinyl acetate Substances 0.000 description 4
230000009257 reactivity Effects 0.000 description 4
238000005507 spraying Methods 0.000 description 4
BEQKKZICTDFVMG-UHFFFAOYSA-N 1,2,3,4,6-pentaoxepane-5,7-dione Chemical compound O=C1OOOOC(=O)O1 BEQKKZICTDFVMG-UHFFFAOYSA-N 0.000 description 3
JYSUYJCLUODSLN-UHFFFAOYSA-N 1,3-benzothiazol-2-ylhydrazine Chemical compound C1=CC=C2SC(NN)=NC2=C1 JYSUYJCLUODSLN-UHFFFAOYSA-N 0.000 description 3
WNXJIVFYUVYPPR-UHFFFAOYSA-N 1,3-dioxolane Chemical compound C1COCO1 WNXJIVFYUVYPPR-UHFFFAOYSA-N 0.000 description 3
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
LCFVJGUPQDGYKZ-UHFFFAOYSA-N Bisphenol A diglycidyl ether Chemical compound C=1C=C(OCC2OC2)C=CC=1C(C)(C)C(C=C1)=CC=C1OCC1CO1 LCFVJGUPQDGYKZ-UHFFFAOYSA-N 0.000 description 3
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
229910000831 Steel Inorganic materials 0.000 description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 3
230000008901 benefit Effects 0.000 description 3
238000006243 chemical reaction Methods 0.000 description 3
229910052801 chlorine Inorganic materials 0.000 description 3
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
238000004090 dissolution Methods 0.000 description 3
238000002474 experimental method Methods 0.000 description 3
150000004665 fatty acids Chemical class 0.000 description 3
238000011010 flushing procedure Methods 0.000 description 3
239000007789 gas Substances 0.000 description 3
OAKJQQAXSVQMHS-UHFFFAOYSA-N hydrazine group Chemical group NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 3
239000012948 isocyanate Substances 0.000 description 3
150000002513 isocyanates Chemical class 0.000 description 3
239000007788 liquid Substances 0.000 description 3
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
150000002978 peroxides Chemical class 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
239000011347 resin Substances 0.000 description 3
229920005989 resin Polymers 0.000 description 3
239000010959 steel Substances 0.000 description 3
238000012360 testing method Methods 0.000 description 3
229910052718 tin Inorganic materials 0.000 description 3
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 3
229920002554 vinyl polymer Polymers 0.000 description 3
VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 2
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
OECTYKWYRCHAKR-UHFFFAOYSA-N 4-vinylcyclohexene dioxide Chemical compound C1OC1C1CC2OC2CC1 OECTYKWYRCHAKR-UHFFFAOYSA-N 0.000 description 2
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical class NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 2
XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 2
ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical class CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
239000004372 Polyvinyl alcohol Substances 0.000 description 2
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 2
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 2
XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
239000012190 activator Substances 0.000 description 2
150000001299 aldehydes Chemical class 0.000 description 2
150000001336 alkenes Chemical class 0.000 description 2
125000003545 alkoxy group Chemical group 0.000 description 2
150000003863 ammonium salts Chemical class 0.000 description 2
125000000129 anionic group Chemical group 0.000 description 2
239000000010 aprotic solvent Substances 0.000 description 2
125000003710 aryl alkyl group Chemical group 0.000 description 2
150000001555 benzenes Chemical class 0.000 description 2
230000000903 blocking effect Effects 0.000 description 2
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
229910052794 bromium Inorganic materials 0.000 description 2
DIKBFYAXUHHXCS-UHFFFAOYSA-N bromoform Chemical compound BrC(Br)Br DIKBFYAXUHHXCS-UHFFFAOYSA-N 0.000 description 2
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
150000001735 carboxylic acids Chemical class 0.000 description 2
230000008859 change Effects 0.000 description 2
239000007795 chemical reaction product Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
229910052802 copper Inorganic materials 0.000 description 2
239000010949 copper Substances 0.000 description 2
125000000753 cycloalkyl group Chemical group 0.000 description 2
ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 description 2
DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
239000000975 dye Substances 0.000 description 2
125000003700 epoxy group Chemical group 0.000 description 2
125000005670 ethenylalkyl group Chemical group 0.000 description 2
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
230000002349 favourable effect Effects 0.000 description 2
229920000578 graft copolymer Polymers 0.000 description 2
229920001519 homopolymer Polymers 0.000 description 2
150000002429 hydrazines Chemical class 0.000 description 2
125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
239000003112 inhibitor Substances 0.000 description 2
239000001023 inorganic pigment Substances 0.000 description 2
229910052742 iron Inorganic materials 0.000 description 2
239000010410 layer Substances 0.000 description 2
239000011976 maleic acid Substances 0.000 description 2
POULHZVOKOAJMA-UHFFFAOYSA-N methyl undecanoic acid Natural products CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
IPCSVZSSVZVIGE-UHFFFAOYSA-N n-hexadecanoic acid Natural products CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
125000001280 n-hexyl group Chemical group C(CCCCC)* 0.000 description 2
238000010915 one-step procedure Methods 0.000 description 2
HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 description 2
229920002451 polyvinyl alcohol Polymers 0.000 description 2
125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
239000012429 reaction media Substances 0.000 description 2
230000009467 reduction Effects 0.000 description 2
229910052709 silver Inorganic materials 0.000 description 2
239000004332 silver Substances 0.000 description 2
150000005846 sugar alcohols Polymers 0.000 description 2
VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
238000012546 transfer Methods 0.000 description 2
UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 2
229920001567 vinyl ester resin Polymers 0.000 description 2
GKXVJHDEWHKBFH-UHFFFAOYSA-N xylylenediamine group Chemical group C=1(C(=CC=CC1)CN)CN GKXVJHDEWHKBFH-UHFFFAOYSA-N 0.000 description 2
IMYZYCNQZDBZBQ-UHFFFAOYSA-N (+-)-8-(cis-3-octyl-oxiranyl)-octanoic acid Natural products CCCCCCCCC1OC1CCCCCCCC(O)=O IMYZYCNQZDBZBQ-UHFFFAOYSA-N 0.000 description 1
VRVUYKONLXCSKZ-UHFFFAOYSA-N (2-hydrazinyl-1,3-benzothiazol-5-yl) hydrogen sulfate Chemical compound OS(=O)(=O)OC1=CC=C2SC(=NN)NC2=C1 VRVUYKONLXCSKZ-UHFFFAOYSA-N 0.000 description 1
XAFMIOCHKFJAPL-UHFFFAOYSA-N (2-hydrazinyl-1,3-benzothiazol-7-yl) hydrogen sulfate Chemical compound C1=CC(OS(O)(=O)=O)=C2SC(=NN)NC2=C1 XAFMIOCHKFJAPL-UHFFFAOYSA-N 0.000 description 1
NWSVJJIONOBBLD-UHFFFAOYSA-N (2-hydrazinyl-4-methyl-1,3-benzothiazol-7-yl) hydrogen sulfate Chemical compound CC1=CC=C(OS(O)(=O)=O)C2=C1NC(=NN)S2 NWSVJJIONOBBLD-UHFFFAOYSA-N 0.000 description 1
DYWNRVWOUASMDT-UHFFFAOYSA-N (4-methyl-1,3-benzothiazol-2-yl)hydrazine Chemical compound CC1=CC=CC2=C1N=C(NN)S2 DYWNRVWOUASMDT-UHFFFAOYSA-N 0.000 description 1
MJAOIHNAUFRSRU-UHFFFAOYSA-N (5-chloro-1,3-benzothiazol-2-yl)hydrazine Chemical compound ClC1=CC=C2SC(NN)=NC2=C1 MJAOIHNAUFRSRU-UHFFFAOYSA-N 0.000 description 1
WYGADNCVURKPND-UHFFFAOYSA-N (5-hexyl-1,3-benzothiazol-2-yl)hydrazine Chemical compound CCCCCCC1=CC=C2SC(=NN)NC2=C1 WYGADNCVURKPND-UHFFFAOYSA-N 0.000 description 1
QIVKJRKJMPQOCD-UHFFFAOYSA-N (5-methoxy-1,3-benzothiazol-2-yl)hydrazine Chemical compound COC1=CC=C2SC(NN)=NC2=C1 QIVKJRKJMPQOCD-UHFFFAOYSA-N 0.000 description 1
WPVGYMPMOXIOTQ-UHFFFAOYSA-N (5-methyl-1,3-benzothiazol-2-yl)hydrazine Chemical compound CC1=CC=C2SC(NN)=NC2=C1 WPVGYMPMOXIOTQ-UHFFFAOYSA-N 0.000 description 1
XLSYUNFZUXHOHF-UHFFFAOYSA-N (6,7-dimethyl-1,3-benzothiazol-2-yl)hydrazine Chemical compound CC1=CC=C2NC(=NN)SC2=C1C XLSYUNFZUXHOHF-UHFFFAOYSA-N 0.000 description 1
IRTHAFQSCWGAOP-UHFFFAOYSA-N (7-chloro-1,3-benzothiazol-2-yl)hydrazine Chemical compound C1=CC(Cl)=C2SC(=NN)NC2=C1 IRTHAFQSCWGAOP-UHFFFAOYSA-N 0.000 description 1
DGKGVSMWSIEPEK-UHFFFAOYSA-N (7-methyl-1,3-benzothiazol-2-yl)hydrazine Chemical compound CC1=CC=CC2=C1SC(NN)=N2 DGKGVSMWSIEPEK-UHFFFAOYSA-N 0.000 description 1
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
WLQXEFXDBYHMRG-UPHRSURJSA-N (z)-4-(oxiran-2-ylmethoxy)-4-oxobut-2-enoic acid Chemical class OC(=O)\C=C/C(=O)OCC1CO1 WLQXEFXDBYHMRG-UPHRSURJSA-N 0.000 description 1
UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical class ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical class NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 description 1
ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 2,3-dimethylbutane Chemical group CC(C)C(C)C ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 0.000 description 1
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150000002927 oxygen compounds Chemical class 0.000 description 1
239000012188 paraffin wax Substances 0.000 description 1
239000002245 particle Substances 0.000 description 1
150000002976 peresters Chemical class 0.000 description 1
150000004965 peroxy acids Chemical class 0.000 description 1
JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
229920001568 phenolic resin Polymers 0.000 description 1
229960005323 phenoxyethanol Drugs 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
238000005498 polishing Methods 0.000 description 1
229920000767 polyaniline Polymers 0.000 description 1
229920000647 polyepoxide Polymers 0.000 description 1
229920000573 polyethylene Polymers 0.000 description 1
229920001228 polyisocyanate Polymers 0.000 description 1
239000005056 polyisocyanate Substances 0.000 description 1
239000002685 polymerization catalyst Substances 0.000 description 1
230000000379 polymerizing effect Effects 0.000 description 1
229920000056 polyoxyethylene ether Polymers 0.000 description 1
229920001155 polypropylene Polymers 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
239000004814 polyurethane Substances 0.000 description 1
229920002635 polyurethane Polymers 0.000 description 1
229920000915 polyvinyl chloride Polymers 0.000 description 1
239000004800 polyvinyl chloride Substances 0.000 description 1
239000011148 porous material Substances 0.000 description 1
239000011591 potassium Substances 0.000 description 1
229910052939 potassium sulfate Inorganic materials 0.000 description 1
238000003825 pressing Methods 0.000 description 1
238000002203 pretreatment Methods 0.000 description 1
230000002265 prevention Effects 0.000 description 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical class CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 1
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
AOJFQRQNPXYVLM-UHFFFAOYSA-N pyridin-1-ium;chloride Chemical compound [Cl-].C1=CC=[NH+]C=C1 AOJFQRQNPXYVLM-UHFFFAOYSA-N 0.000 description 1
230000035484 reaction time Effects 0.000 description 1
WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 description 1
229960003656 ricinoleic acid Drugs 0.000 description 1
FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 description 1
239000004208 shellac Substances 0.000 description 1
ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 1
229940113147 shellac Drugs 0.000 description 1
235000013874 shellac Nutrition 0.000 description 1
CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 description 1
239000004328 sodium tetraborate Substances 0.000 description 1
235000010339 sodium tetraborate Nutrition 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000000600 sorbitol Substances 0.000 description 1
230000006641 stabilisation Effects 0.000 description 1
238000011105 stabilization Methods 0.000 description 1
239000008117 stearic acid Substances 0.000 description 1
150000003440 styrenes Chemical class 0.000 description 1
238000006467 substitution reaction Methods 0.000 description 1
LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000001117 sulphuric acid Substances 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
230000008961 swelling Effects 0.000 description 1
239000000454 talc Substances 0.000 description 1
229910052623 talc Inorganic materials 0.000 description 1
235000012976 tarts Nutrition 0.000 description 1
OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 description 1
SWAXTRYEYUTSAP-UHFFFAOYSA-N tert-butyl ethaneperoxoate Chemical compound CC(=O)OOC(C)(C)C SWAXTRYEYUTSAP-UHFFFAOYSA-N 0.000 description 1
CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 description 1
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 1
239000011135 tin Substances 0.000 description 1
235000021122 unsaturated fatty acids Nutrition 0.000 description 1
150000004670 unsaturated fatty acids Chemical class 0.000 description 1
230000004584 weight gain Effects 0.000 description 1
235000019786 weight gain Nutrition 0.000 description 1
239000000080 wetting agent Substances 0.000 description 1
239000012224 working solution Substances 0.000 description 1
239000008096 xylene Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1
239000011701 zinc Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/002—Scale prevention in a polymerisation reactor or its auxiliary parts
- C08F2/004—Scale prevention in a polymerisation reactor or its auxiliary parts by a prior coating on the reactor walls
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F291/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds according to more than one of the groups C08F251/00 - C08F289/00

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Organic Chemistry (AREA)
Polymerisation Methods In General (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Thiazole And Isothizaole Compounds (AREA)

NO780291A 1977-01-27 1978-01-26 Fremgangsmaate til fremstilling av vinylkloridpolymerisater NO780291L (no)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19772703280 DE2703280A1 (de)	1977-01-27	1977-01-27	Verfahren zur herstellung von vinylchlorid-polymerisation

Publications (1)

Publication Number	Publication Date
NO780291L true NO780291L (no)	1978-07-28

Family

ID=5999662

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO780291A NO780291L (no)	1977-01-27	1978-01-26	Fremgangsmaate til fremstilling av vinylkloridpolymerisater

Country Status (14)

Country	Link
US (1)	US4143097A (fr)
JP (1)	JPS5396087A (fr)
AR (1)	AR224999A1 (fr)
AT (1)	AT362585B (fr)
BE (1)	BE863401A (fr)
CA (1)	CA1102490A (fr)
DD (1)	DD134108A5 (fr)
DE (1)	DE2703280A1 (fr)
FR (1)	FR2401178A1 (fr)
GB (1)	GB1595757A (fr)
IT (1)	IT1093271B (fr)
NL (1)	NL7800967A (fr)
NO (1)	NO780291L (fr)
SE (1)	SE7800989L (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2757924A1 (de) *	1977-12-24	1979-07-05	Hoechst Ag	Verfahren zur herstellung von vinylchlorid-polymerisaten
US4321363A (en) *	1980-02-21	1982-03-23	Nippon Soda Company Limited	Adsorbent for urokinase containing agarose
DE3413876A1 (de) *	1984-04-12	1985-10-17	Ludwig Heumann & Co GmbH, 8500 Nürnberg	Arzneimittel
DE3815397C2 (de) *	1988-05-05	1998-02-26	Wacker Chemie Gmbh	Verfahren zur Herstellung einer Autoklavenbeschichtung
JP2764660B2 (ja) *	1991-05-17	1998-06-11	信越化学工業株式会社	重合体スケール付着防止剤および重合体スケールの付着防止方法
US6001937A (en) *	1998-11-17	1999-12-14	Occidental Chemical Corporation	Reducing scale in vinyl polymerizations
KR20090088384A (ko) *	2006-12-11	2009-08-19	바스프 에스이	이소시아네이트의 제조 방법

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
IE36799B1 (en) *	1971-12-14	1977-03-02	Loctite Ltd	Cyanoacrylate adhesive composition
JPS5345836B2 (fr) *	1974-04-26	1978-12-09
JPS5113881A (en) *	1974-07-24	1976-02-03	Kanegafuchi Chemical Ind	Enkabiniruno jugohoho

1977
- 1977-01-27 DE DE19772703280 patent/DE2703280A1/de not_active Withdrawn
1978
- 1978-01-25 US US05/872,155 patent/US4143097A/en not_active Expired - Lifetime
- 1978-01-25 AR AR270844A patent/AR224999A1/es active
- 1978-01-25 IT IT19605/78A patent/IT1093271B/it active
- 1978-01-25 DD DD78203416A patent/DD134108A5/xx unknown
- 1978-01-26 AT AT57678A patent/AT362585B/de not_active IP Right Cessation
- 1978-01-26 SE SE7800989A patent/SE7800989L/xx unknown
- 1978-01-26 GB GB3169/78A patent/GB1595757A/en not_active Expired
- 1978-01-26 NL NL7800967A patent/NL7800967A/xx not_active Application Discontinuation
- 1978-01-26 CA CA295,769A patent/CA1102490A/fr not_active Expired
- 1978-01-26 NO NO780291A patent/NO780291L/no unknown
- 1978-01-26 JP JP678678A patent/JPS5396087A/ja active Pending
- 1978-01-27 BE BE184695A patent/BE863401A/fr not_active IP Right Cessation
- 1978-01-27 FR FR7802304A patent/FR2401178A1/fr not_active Withdrawn

Also Published As

Publication number	Publication date
NL7800967A (nl)	1978-07-31
BE863401A (fr)	1978-07-27
JPS5396087A (en)	1978-08-22
US4143097A (en)	1979-03-06
SE7800989L (sv)	1978-07-28
GB1595757A (en)	1981-08-19
IT1093271B (it)	1985-07-19
DD134108A5 (de)	1979-02-07
AR224999A1 (es)	1982-02-15
AT362585B (de)	1981-05-25
CA1102490A (fr)	1981-06-02
FR2401178A1 (fr)	1979-03-23
IT7819605A0 (it)	1978-01-25
ATA57678A (de)	1980-10-15
DE2703280A1 (de)	1978-08-10

Publication	Publication Date	Title
CA1116347A (fr)	1982-01-12	Cuve de reaction a revetement pour la polymerisation d'olefines
CA1085094A (fr)	1980-09-02	Polymerisation d'halogenure de vinyle dans une cuve de reaction aux parois traitees
NO780291L (no)	1978-07-28	Fremgangsmaate til fremstilling av vinylkloridpolymerisater
NO772843L (no)	1978-02-17	Fremgangsm}te til hindring av oppbygning av polymere p} innerflaten i et polymerisasjonskar samt polymerisasjonskar for fremgangsm}ten
EP0003875B1 (fr)	1981-06-24	Produit de revêtement à utiliser dans un réacteur pour la polymérisation d'halogénure de vinyle, le réacteur et le procédé
NO754343L (fr)	1976-06-29
CA2138182C (fr)	1996-11-12	Procede pour la polymerisation du chlorure de vinyle
EP0035547B1 (fr)	1984-05-30	Procede de revetement de reacteurs par application de la vapeur d'un compose organique
US5352726A (en)	1994-10-04	Autodepositing composition containing vinylidene chloride based resin
US4049894A (en)	1977-09-20	Latex modified portland cement and use thereof in polymerization reactors
CA1113942A (fr)	1981-12-08	Procede industriel d'obtention de polymeres de chlorure de vinyle
CA1094747A (fr)	1981-01-27	Reacteurs et procede de polymerisation d'halogenure de vinyle
US4661569A (en)	1987-04-28	Method of inhibiting polymer deposition on reactor walls during free-radical polymerization
FI62319C (fi)	1982-12-10	Foerfarande foer polymerisering av vinylklorid i vattendispersion
EP0459369B1 (fr)	1995-03-15	Polymère contenant du fluor pour peinture et composition de peinture contenant ce polymère
US4374966A (en)	1983-02-22	Process for the manufacture of vinyl chloride polymers by coating polymerization vessels
EP0035537A1 (fr)	1981-09-16	Procede de revetement de reacteurs par application d'un compose organique sous forme de vapeur.
EP0019198A1 (fr)	1980-11-26	Procédé pour la préparation de polymères de chlorure de vinyle, produit pour revêtir les cuves de polymérisation et cuve de polymérisation revêtue de ce produit
US4585842A (en)	1986-04-29	Method of treating a polymerizing reactor
EP0006418B1 (fr)	1983-03-09	Prévention de l'encroûtage par les polymères de chlorure de vinyle dans les réacteurs de polymérisation au moyen d'oxalyl-bis(benzylidène hydrazide) et d'alumine
JP2001040006A (ja)	2001-02-13	エチレン性二重結合を有する単量体の重合体を製造する方法
KR810001790B1 (ko)	1981-11-14	비닐 할라이드 단량체의 중합방법
JPS58180509A (ja)	1983-10-22	ビニル系またはジエン系単量体の重合方法
JP2001040005A (ja)	2001-02-13	エチレン性二重結合を有する単量体の重合体を製造する方法
NO153372B (no)	1985-11-25	Fremgangsmaate for polymerisering av vinylklorid.