NO971421L - Fremgangsmåte for fremstilling av 1,3-alkandioler og 3-hydroksyaldehyder - Google Patents

Fremgangsmåte for fremstilling av 1,3-alkandioler og 3-hydroksyaldehyder

Info

Publication number
NO971421L
NO971421L NO971421A NO971421A NO971421L NO 971421 L NO971421 L NO 971421L NO 971421 A NO971421 A NO 971421A NO 971421 A NO971421 A NO 971421A NO 971421 L NO971421 L NO 971421L
Authority
NO
Norway
Prior art keywords
preparation
hydroxyaldehydes
alkanediols
oxirane
weight
Prior art date
Application number
NO971421A
Other languages
English (en)
Other versions
NO971421D0 (no
NO307562B1 (no
Inventor
Kevin Dale Allen
Juan Pedro Arhancet
David Cleve Eubanks
Howard Lam-Ho Fong
Thomas Clayton Forschner
David William Johnson
Jiang Jen Lin
Stephen Blake Mullin
Joseph Broun Powell
Thomas Carl Semple
Lynn Henry Slaugh
Terry Blane Thomason
Paul Richard Weider
Original Assignee
Shell Int Research
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US08/316,669 external-priority patent/US5576471A/en
Priority claimed from US08/316,660 external-priority patent/US5585528A/en
Priority claimed from US08/316,679 external-priority patent/US5545767A/en
Priority claimed from US08/316,677 external-priority patent/US5463146A/en
Priority claimed from US08/316,680 external-priority patent/US5563302A/en
Application filed by Shell Int Research filed Critical Shell Int Research
Publication of NO971421D0 publication Critical patent/NO971421D0/no
Publication of NO971421L publication Critical patent/NO971421L/no
Publication of NO307562B1 publication Critical patent/NO307562B1/no

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C07C45/58—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom in three-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/16—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxo-reaction combined with reduction
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
    • C07C47/19—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen containing hydroxy groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Steroid Compounds (AREA)

Abstract

Fremgangsmåte for fremstilling av 1,3-alkandioler og 3-hydroksyaldehyder ved hydroformylering av et oksiran med karbonmonoksyd og hydrogen i nærvær av én eller flere hydroformyleringskatalysatorer basert på metall fra gruppe VIII og som kan inneholde opp til 50mol%, basert på metallet, fosfinmodifiserte katalysa-torer, idet konsentrasjonen av oksiranet ved reaksjonens begynnelse er lavere enn 15 vekt%, basert på vekten av den totale flytende reaksjonsblanding. Fremgangsmåten muliggjør fremstilling av 1,3-propandiol med høye utbytter og høy selektivitet.
NO971421A 1994-09-30 1997-03-25 Fremgangsmåte for fremstilling av 1,3-alkandioler og 3- hydroksyaldehyder NO307562B1 (no)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US08/316,669 US5576471A (en) 1994-09-30 1994-09-30 Cobalt-catalyzed process for preparing 1,3-propanediol using a lipophilic dihydroxyarene promoter
US08/316,660 US5585528A (en) 1994-09-30 1994-09-30 Cobalt-catalyzed process for preparing 1,3-propanediol using a lipophilic tertiary amine promoter
US08/316,679 US5545767A (en) 1994-09-30 1994-09-30 Process for preparing 1,3-propanediol
US08/316,677 US5463146A (en) 1994-09-30 1994-09-30 Process for preparing 1,3-propanediol
US08/316,680 US5563302A (en) 1994-09-30 1994-09-30 Cobalt-catalyzed process for preparing 1,3-propanediol using a lipophilic phosphine oxide promoter
PCT/EP1995/003870 WO1996010552A1 (en) 1994-09-30 1995-09-28 Process for preparing 1,3-alkanediols and 3-hydroxyaldehydes

Publications (3)

Publication Number Publication Date
NO971421D0 NO971421D0 (no) 1997-03-25
NO971421L true NO971421L (no) 1997-03-25
NO307562B1 NO307562B1 (no) 2000-04-25

Family

ID=27541008

Family Applications (1)

Application Number Title Priority Date Filing Date
NO971421A NO307562B1 (no) 1994-09-30 1997-03-25 Fremgangsmåte for fremstilling av 1,3-alkandioler og 3- hydroksyaldehyder

Country Status (23)

Country Link
EP (1) EP0783476B1 (no)
JP (1) JP3850439B2 (no)
KR (1) KR100361109B1 (no)
CN (1) CN1074405C (no)
AT (1) ATE174320T1 (no)
AU (1) AU694573B2 (no)
BR (1) BR9509110A (no)
CZ (1) CZ290721B6 (no)
DE (1) DE69506574T2 (no)
DK (1) DK0783476T3 (no)
ES (1) ES2126937T3 (no)
FI (1) FI971268A7 (no)
HU (1) HUT77464A (no)
MX (1) MX9702285A (no)
MY (1) MY113319A (no)
NO (1) NO307562B1 (no)
NZ (1) NZ294599A (no)
PL (1) PL181023B1 (no)
RU (1) RU2142934C1 (no)
SK (1) SK281565B6 (no)
TR (1) TR199501189A2 (no)
TW (1) TW415935B (no)
WO (1) WO1996010552A1 (no)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HUT77463A (hu) * 1994-09-30 1998-05-28 Shell Internationale Research Maatschappij B.V. Eljárás 1,3-alkán-diolok és 3-hidroxi-aldehidek előállítására
DE69506580T2 (de) * 1994-09-30 1999-06-17 Shell Internationale Research Maatschappij B.V., Den Haag/S'gravenhage Verfahren zur herstellung von 1,3-alkandiolen und 3-hydroxyaldehyden
CA2256688C (en) * 1996-05-30 2005-10-18 Shell Internationale Research Maatschappij B.V. Process for preparing 1,3-alkanediols
US5786524A (en) * 1996-05-30 1998-07-28 Shell Oil Company Process for preparation of 1,3-propanediol via hydrogenation of 3-hydroxypropanal
DE19852104A1 (de) * 1998-11-12 2000-05-18 Degussa Verfahren zur Herstellung von ß-Hydroxyaldehyden
CN1252012C (zh) * 2000-03-22 2006-04-19 国际壳牌研究有限公司 制备1,3－二醇的方法
US6545190B2 (en) * 2001-03-15 2003-04-08 Shell Oil Company One step process for preparing a 1,3-diol
TW592819B (en) * 2001-05-18 2004-06-21 Kevin Dale Allen One-step production of 1,3-propanediol from ethylene oxide and syngas with a cobalt-iron catalyst
TW593238B (en) * 2001-05-18 2004-06-21 Kevin Dale Allen One-step production of 1,3-propanediol from ethylene oxide and syngas with a catalyst with a N-heterocyclic ligand
US6576802B2 (en) * 2001-06-04 2003-06-10 Shell Oil Company One-step production of 1, 3-propanediol from ethylene oxide and syngas with a catalyst with a phospholanoalkane ligand
US7276634B2 (en) * 2002-10-03 2007-10-02 Shell Oil Company Reduction of the viscosity of reactive heavy byproducts during the production of 1,3-propanediol
MY136121A (en) * 2002-11-01 2008-08-29 Shell Int Research Method for removal of mw176 cyclic acetal and solid acid catalyzed reactive stripping of impurities formed during the production of 1, 3-propanediol
RU2317970C2 (ru) * 2003-02-24 2008-02-27 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Очистка 1,3-пропандиола путем перегонки
CN1310864C (zh) * 2004-04-29 2007-04-18 中国石油化工股份有限公司 制备3－羟基丙醛和1，3－丙二醇的方法
CN102826970B (zh) * 2011-06-17 2015-08-19 中国石油化工股份有限公司 一种低碳烯烃氢甲酰化二段反应方法和装置
CN105585435B (zh) * 2014-10-24 2018-02-13 中国石油化工股份有限公司 生产1,3‑丙二醇的方法
CN105585436B (zh) * 2014-10-24 2017-11-17 中国石油化工股份有限公司 醋酸乙烯合成1,3‑丙二醇的方法
CN105585442B (zh) * 2014-10-24 2017-11-21 中国石油化工股份有限公司 用于1,3‑丙二醇合成的方法
CN105585441B (zh) * 2014-10-24 2018-02-13 中国石油化工股份有限公司 用于生产1,3‑丙二醇的方法
CN105585444B (zh) * 2014-10-24 2017-12-15 中国石油化工股份有限公司 1,3‑丙二醇的生产方法
CN108017510B (zh) * 2016-11-03 2021-02-02 万华化学集团股份有限公司 一种羟基特戊醛的制备方法，及其在新戊二醇制备方面的应用
JP2019001746A (ja) * 2017-06-15 2019-01-10 株式会社クラレ ジオールの製造方法
WO2019098242A1 (ja) * 2017-11-15 2019-05-23 三菱ケミカル株式会社 アルデヒドの製造方法及びアルコールの製造方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3456017A (en) * 1965-10-21 1969-07-15 Shell Oil Co Glycol production
US3463819A (en) * 1965-10-21 1969-08-26 Shell Oil Co Glycol production
US3687981A (en) * 1968-01-17 1972-08-29 Du Pont Process for making a dioxane
CA1279657C (en) * 1986-08-20 1991-01-29 Mark A. Murphy Process for making 1,3-glycols from epoxides
US4973741A (en) * 1989-06-29 1990-11-27 Eastman Kodak Company Difunctional products from ethylene oxide and synthesis gas
RU2038844C1 (ru) * 1990-05-04 1995-07-09 Юнион Карбайд Кемикалз Энд Пластикс Текнолоджи Корпорейшн Каталитическая композиция для гидроформилирования этиленоксида, способ ее получения и способ получения 1,3-пропандиола и 3-гидроксипропионового альдегида
WO1994018149A1 (en) * 1993-02-05 1994-08-18 Shell Internationale Research Maatschappij B.V. Process for making 1,3-diols and 3-hydroxyaldehydes
DE69506580T2 (de) * 1994-09-30 1999-06-17 Shell Internationale Research Maatschappij B.V., Den Haag/S'gravenhage Verfahren zur herstellung von 1,3-alkandiolen und 3-hydroxyaldehyden
HUT77463A (hu) * 1994-09-30 1998-05-28 Shell Internationale Research Maatschappij B.V. Eljárás 1,3-alkán-diolok és 3-hidroxi-aldehidek előállítására

Also Published As

Publication number Publication date
DK0783476T3 (da) 1999-08-16
MY113319A (en) 2002-01-31
ATE174320T1 (de) 1998-12-15
CZ94497A3 (cs) 1998-02-18
AU3744595A (en) 1996-04-26
AU694573B2 (en) 1998-07-23
BR9509110A (pt) 1998-07-14
MX9702285A (es) 1997-06-28
WO1996010552A1 (en) 1996-04-11
NO971421D0 (no) 1997-03-25
PL181023B1 (pl) 2001-05-31
KR100361109B1 (ko) 2003-03-06
FI971268A0 (fi) 1997-03-26
FI971268A7 (fi) 1997-03-26
SK38897A3 (en) 1997-11-05
DE69506574T2 (de) 1999-06-17
PL319439A1 (en) 1997-08-04
SK281565B6 (sk) 2001-05-10
CZ290721B6 (cs) 2002-10-16
EP0783476B1 (en) 1998-12-09
JPH10507747A (ja) 1998-07-28
NO307562B1 (no) 2000-04-25
KR970706226A (ko) 1997-11-03
TR199501189A2 (tr) 1996-06-21
DE69506574D1 (de) 1999-01-21
NZ294599A (en) 1998-12-23
CN1158603A (zh) 1997-09-03
EP0783476A1 (en) 1997-07-16
ES2126937T3 (es) 1999-04-01
JP3850439B2 (ja) 2006-11-29
HUT77464A (hu) 1998-05-28
CN1074405C (zh) 2001-11-07
TW415935B (en) 2000-12-21
RU2142934C1 (ru) 1999-12-20

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