PL400207A1 - A method for producing cellulose and zinc (II) oxide composites using cyclohexylammonium ionic liquids - Google Patents
A method for producing cellulose and zinc (II) oxide composites using cyclohexylammonium ionic liquidsInfo
- Publication number
- PL400207A1 PL400207A1 PL400207A PL40020712A PL400207A1 PL 400207 A1 PL400207 A1 PL 400207A1 PL 400207 A PL400207 A PL 400207A PL 40020712 A PL40020712 A PL 40020712A PL 400207 A1 PL400207 A1 PL 400207A1
- Authority
- PL
- Poland
- Prior art keywords
- zinc
- cellulose
- cyclohexylammonium
- ionic liquids
- added
- Prior art date
Links
- 239000001913 cellulose Substances 0.000 title abstract 6
- 229920002678 cellulose Polymers 0.000 title abstract 6
- 239000002608 ionic liquid Substances 0.000 title abstract 4
- PAFZNILMFXTMIY-UHFFFAOYSA-O cyclohexylammonium Chemical compound [NH3+]C1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-O 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- RNWHGQJWIACOKP-UHFFFAOYSA-N zinc;oxygen(2-) Chemical class [O-2].[Zn+2] RNWHGQJWIACOKP-UHFFFAOYSA-N 0.000 title abstract 3
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical class [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 abstract 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 abstract 1
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000002131 composite material Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 239000000945 filler Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- 235000005985 organic acids Nutrition 0.000 abstract 1
- 239000004033 plastic Substances 0.000 abstract 1
- 229920003023 plastic Polymers 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Przedmiotem wynalazku jest nowy sposób wytwarzania kompozytów celulozy i tlenku cynku(II) z wykorzystaniem cykloheksyloamoniowych cieczy jonowych majacych zastosowanie jako wypelniacze w produkcji tworzyw sztucznych. W odmianie sposób otrzymywania nowych kompozytów celulozy i tlenku cynku(II) z wykorzystaniem cykloheksyloamoniowych cieczy jonowych polega na tym, ze do cieczy jonowej okreslonej wzorem ogólnym 1, w którym R oznacza prostolancuchowy podstawnik alkilowy zlozony z 1 do 20 atomów wegla, lub podstawnik benzylowy lub allilowy, zas A reszte kwasowa kwasów organicznych dodaje sie celuloze w temperaturze od 20 do 120°C, w ilosci od 0,05 do 30% wagowych, nastepnie po jej rozpuszczeniu dodaje sie tlenek cynku(II) w ilosci od 0,01 do 50% wagowych w przeliczeniu na ilosc dodanej uprzednio celulozy, po czym tak przygotowany roztwór ochladza sie i dodaje do niego rozpuszczalnik. Wytracony kompozyt celulozy i tlenku cynku(II) odsacza sie i suszy w temperaturze od 20 do 60°C, przez okres 1 do48 godzin.The subject of the invention is a new method for producing cellulose and zinc (II) composites using cyclohexylammonium ionic liquids for use as fillers in the production of plastics. In a variation, the method of obtaining new cellulose and zinc (II) oxide composites using cyclohexylammonium ionic liquids is based on the ionic liquid defined by the general formula 1, in which R is a straight chain alkyl substituent of 1 to 20 carbon atoms, or a benzyl substituent or allyl, while the rest of the organic acids are added cellulose at a temperature of 20 to 120 ° C in an amount of 0.05 to 30% by weight, then after its dissolution zinc (II) oxide is added in an amount of 0.01 to 50 % by weight based on the amount of cellulose added previously, after which the solution thus prepared is cooled and the solvent added to it. The precipitated cellulose and zinc (II) composite is filtered off and dried at a temperature of 20 to 60 ° C for a period of 1 to 48 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL400207A PL226097B1 (en) | 2012-08-01 | 2012-08-01 | Process for producing cellulose and a composite oxide of zinc (II) using the cyclo-hexyl-ammonium ionic liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL400207A PL226097B1 (en) | 2012-08-01 | 2012-08-01 | Process for producing cellulose and a composite oxide of zinc (II) using the cyclo-hexyl-ammonium ionic liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL400207A1 true PL400207A1 (en) | 2014-02-03 |
| PL226097B1 PL226097B1 (en) | 2017-06-30 |
Family
ID=50023156
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL400207A PL226097B1 (en) | 2012-08-01 | 2012-08-01 | Process for producing cellulose and a composite oxide of zinc (II) using the cyclo-hexyl-ammonium ionic liquid |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL226097B1 (en) |
-
2012
- 2012-08-01 PL PL400207A patent/PL226097B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL226097B1 (en) | 2017-06-30 |
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