PL401583A1 - Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography - Google Patents

Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography

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Publication number
PL401583A1
PL401583A1 PL401583A PL40158312A PL401583A1 PL 401583 A1 PL401583 A1 PL 401583A1 PL 401583 A PL401583 A PL 401583A PL 40158312 A PL40158312 A PL 40158312A PL 401583 A1 PL401583 A1 PL 401583A1
Authority
PL
Poland
Prior art keywords
inlet
carrier gas
adsorbate
ionization detector
stream
Prior art date
Application number
PL401583A
Other languages
Polish (pl)
Other versions
PL220801B1 (en
Inventor
Piotr M. Slomkiewicz
Original Assignee
Uniwersytet Jana Kochanowskiego W Kielcach
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uniwersytet Jana Kochanowskiego W Kielcach filed Critical Uniwersytet Jana Kochanowskiego W Kielcach
Priority to PL401583A priority Critical patent/PL220801B1/en
Publication of PL401583A1 publication Critical patent/PL401583A1/en
Publication of PL220801B1 publication Critical patent/PL220801B1/en

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Abstract

Zespól detektorów cieplno-przewodnosciowego i plomieniowo-jonizacyjnego do pomiarów adsorpcji metoda inwersyjnej chromatografii gazowej z dzielnikiem strumienia gazu nosnego z adsorbatem i z dwoma zaworami czterodroznymi ma wlot (11) gazu nosnego z adsorbatem, polaczony ze stozkowa komora dzielnika (19), w której znajduje sie przesuwana sruba mikrometryczna (34) kalibrowana kapilara (20), której czesc jest w walcowej komorze dozownika (21), a komory stozkowa (19) i walcowa (21) rozdziela uszczelka (22). Ponadto zespól ma w pierwszej pozycji roboczej zaworu czterodroznego (24) strumien gazu nosnego z adsorbatem z kanalika (23), polaczonego ze stozkowa komora dzielnika (19), polaczony z wlotem (26) do detektora plomieniowo-jonizacyjnego (27). Wlot (42) pomocniczego gazu nosnego jest polaczony z wylotem (39), a w drugiej pozycji roboczej zaworu czterodroznego (24) strumien gazu nosnego z adsorbatem z kanalika (23), polaczonego ze stozkowa komora dzielnika (19) jest polaczony z wylotem (39), a wlot (42) pomocniczego gazu nosnego jest polaczony wlotem (26) do detektora plomieniowo-jonizacyjnego (27). Zespól ma takze w pierwszej pozycji roboczej zaworu czterodroznego (30) strumien gazu nosnego z adsorbatem z kanalika (29), polaczonego z walcowa komora dzielnika (21) i jest polaczony z wlotem (32) do detektora plomieniowo-jonizacyjnego (31), a wlot (37) pomocniczego gazu nosnego jest polaczony z wylotem (38). W drugiej pozycji roboczej zaworu czterodroznego (30) strumien gazu nosnego z adsorbatem z kanalika (29), polaczonego z walcowa komora dzielnika (21) jest polaczony z wylotem (38), a wlot (37) pomocniczego gazu nosnego jest polaczony wlotem (32) do detektora plomieniowo-jonizacyjnego (31).A set of thermal conductivity and flame ionization detectors for adsorption measurements using inverse gas chromatography with an adsorbate gas stream divider and two four-way valves has an inlet (11) of adsorbate nasal gas, connected to the conical divider chamber (19), in which the sliding micrometer screw (34) calibrated capillary (20), part of which is in the cylindrical dispenser chamber (21), and the conical (19) and cylindrical (21) chambers are separated by a gasket (22). In addition, the assembly has in its first operating position a four-way valve (24) a stream of carrier gas with an adsorbate from a channel (23), connected to the conical divider chamber (19), connected to the inlet (26) to the flame ionization detector (27). The inert carrier gas inlet (42) is connected to the outlet (39), and in the second operating position of the four-way valve (24) the stream of carrier gas with the adsorbate from the channel (23) connected to the conical divider chamber (19) is connected to the outlet (39) and the inlet (42) of the auxiliary carrier gas is connected by an inlet (26) to the flame ionization detector (27). The assembly also has in the first operating position of the four-way valve (30) a stream of carrier gas with a channel adsorbate (29), connected to the cylindrical divider chamber (21) and is connected to the inlet (32) to the flame ionization detector (31), and the inlet (37) the auxiliary carrier gas is connected to the outlet (38). In the second operating position of the four-way valve (30), the carrier gas stream with the adsorbate from the channel (29) connected to the cylindrical divider chamber (21) is connected to the outlet (38), and the inlet (37) of the secondary carrier gas is connected to the inlet (32) for flame ionization detector (31).

PL401583A 2012-11-12 2012-11-12 Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography PL220801B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL401583A PL220801B1 (en) 2012-11-12 2012-11-12 Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL401583A PL220801B1 (en) 2012-11-12 2012-11-12 Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography

Publications (2)

Publication Number Publication Date
PL401583A1 true PL401583A1 (en) 2013-06-24
PL220801B1 PL220801B1 (en) 2016-01-29

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ID=48671932

Family Applications (1)

Application Number Title Priority Date Filing Date
PL401583A PL220801B1 (en) 2012-11-12 2012-11-12 Thermo-conductive and flame-ionization detector system, especially for inverse gas chromatography

Country Status (1)

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PL (1) PL220801B1 (en)

Also Published As

Publication number Publication date
PL220801B1 (en) 2016-01-29

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