PL410319A1 - New quaternary alkoxymethyl tebuconazole chlorides, method for producing them and their application as growth inhibitors of mycelium - Google Patents
New quaternary alkoxymethyl tebuconazole chlorides, method for producing them and their application as growth inhibitors of myceliumInfo
- Publication number
- PL410319A1 PL410319A1 PL410319A PL41031914A PL410319A1 PL 410319 A1 PL410319 A1 PL 410319A1 PL 410319 A PL410319 A PL 410319A PL 41031914 A PL41031914 A PL 41031914A PL 410319 A1 PL410319 A1 PL 410319A1
- Authority
- PL
- Poland
- Prior art keywords
- tebuconazole
- alkoxymethyl
- chlorides
- mycelium
- quaternary
- Prior art date
Links
- 239000005839 Tebuconazole Substances 0.000 title abstract 5
- -1 alkoxymethyl tebuconazole chlorides Chemical class 0.000 title abstract 3
- 239000003966 growth inhibitor Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- PXMNMQRDXWABCY-UHFFFAOYSA-N 1-(4-chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol Chemical compound C1=NC=NN1CC(O)(C(C)(C)C)CCC1=CC=C(Cl)C=C1 PXMNMQRDXWABCY-UHFFFAOYSA-N 0.000 abstract 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 4
- 238000000034 method Methods 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 244000053095 fungal pathogen Species 0.000 abstract 1
- 239000003112 inhibitor Substances 0.000 abstract 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Plural Heterocyclic Compounds (AREA)
Abstract
Przedmiotem wynalazku są nowe czwartorzędowe alkoksymetylowe chlorki tebukonazolu o wzorze ogólnym 1, w którym R oznacza podstawnik alkilowy zawierający od 3 do 18 atomów węgla, sposób ich wytwarzania oraz zastosowanie jako inhibitorów wzrostu grzybni. Sposób ich otrzymywania polega na tym, że tebukonazol poddaje się reakcji z eterem chlorometylowoalkilowym w stosunku molowym tebukonazolu do eteru równym 1:1-1,5, w środowisku bezwodnego rozpuszczalnika organicznego, w temperaturze od 25°C do 120°C, w czasie od 1 do 24 godzin, po czym powstały produkt reakcji odsącza się pod obniżonym ciśnieniem, dalej przemywa bezwodnym rozpuszczalnikiem organicznym, a następnie suszy się pod obniżonym ciśnieniem w temperaturze od 40°C do 80°C, w czasie od 8 do 24 godzin. Nowe czwartorzędowe alkoksymetylowe chlorki tebukonazolu mają zastosowanie jako inhibitory wzrostu patogenów grzybowych.The present invention relates to new tebuconazole quaternary alkoxymethyl chlorides of general formula 1 in which R is an alkyl substituent containing from 3 to 18 carbon atoms, the method of their preparation and the use as mycelium growth inhibitors. The method of their preparation consists in the fact that tebuconazole is reacted with chloromethylalkyl ether in a molar ratio of tebuconazole to ether of 1: 1-1.5, in an anhydrous organic solvent medium, at a temperature from 25 ° C to 120 ° C, during After 1 to 24 hours, the resulting reaction product is filtered off with suction, further washed with anhydrous organic solvent, and then dried under reduced pressure at 40 ° C to 80 ° C for 8 to 24 hours. New tebuconazole quaternary alkoxymethyl chlorides are used as inhibitors of fungal pathogen growth.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL410319A PL229315B1 (en) | 2014-12-01 | 2014-12-01 | New quaternary alkoxymethyl tebuconazole chlorides, method for producing them and their application as growth inhibitors of mycelium |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL410319A PL229315B1 (en) | 2014-12-01 | 2014-12-01 | New quaternary alkoxymethyl tebuconazole chlorides, method for producing them and their application as growth inhibitors of mycelium |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL410319A1 true PL410319A1 (en) | 2016-06-06 |
| PL229315B1 PL229315B1 (en) | 2018-07-31 |
Family
ID=56086931
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL410319A PL229315B1 (en) | 2014-12-01 | 2014-12-01 | New quaternary alkoxymethyl tebuconazole chlorides, method for producing them and their application as growth inhibitors of mycelium |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL229315B1 (en) |
-
2014
- 2014-12-01 PL PL410319A patent/PL229315B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL229315B1 (en) | 2018-07-31 |
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