PL413444A1 - Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles - Google Patents

Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

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Publication number
PL413444A1
PL413444A1 PL413444A PL41344415A PL413444A1 PL 413444 A1 PL413444 A1 PL 413444A1 PL 413444 A PL413444 A PL 413444A PL 41344415 A PL41344415 A PL 41344415A PL 413444 A1 PL413444 A1 PL 413444A1
Authority
PL
Poland
Prior art keywords
solution
solvent
suspension
silver nanoparticles
silver
Prior art date
Application number
PL413444A
Other languages
Polish (pl)
Other versions
PL234471B1 (en
Inventor
Bożena Tyliszczak
Agnieszka Sobczak-Kupiec
Katarzyna Bialik-Wąs
Dagmara Malina
Original Assignee
Politechnika Krakowska im. Tadeusza Kościuszki
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Politechnika Krakowska im. Tadeusza Kościuszki filed Critical Politechnika Krakowska im. Tadeusza Kościuszki
Priority to PL413444A priority Critical patent/PL234471B1/en
Publication of PL413444A1 publication Critical patent/PL413444A1/en
Publication of PL234471B1 publication Critical patent/PL234471B1/en

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  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

Zgłoszenie dotyczy sposobu wytwarzania zawiesiny nanocząstek srebra. Sposób wytwarzania zawiesiny nanocząstek srebra polega na redukcji soli srebra środkiem redukującym pochodzenia roślinnego i charakteryzuje się tym, że jako środek redukujący stosuje się hormon roślinny, przy czym redukcję prowadzi się w obecności stabilizatora. Według korzystnego wariantu wykonania sposób wytwarzania obejmuje następujące etapy: a) sporządza się roztwór stabilizatora w wodzie lub w mieszaninie rozpuszczalnika organicznego i wody, po czym w roztworze tym rozpuszcza się sól srebra (roztwór A); b) sporządza się roztwór hormonu roślinnego, korzystnie w tym samym rozpuszczalniku, w którym sporządza się roztwór A, przy czym stosunek wagowy bursztynu do rozpuszczalnika zawarty jest w granicach od 1 : 100 do 10 : 1 (roztwór B); c) roztwór B dodaje się do roztworu A, przy ciągłym mieszaniu, w temperaturze utrzymującej stan ciekły rozpuszczalnika lub podwyższonej do temperatury wrzenia rozpuszczalnika, przy czym stosunek objętościowy roztworu A do roztworu B zawarty jest w granicach od 1 : 100 do 100 : 1. Ujawniono także zawiesinę nanocząstek srebra, zawierającą hormon roślinny i stabilizator, w której stężenie nanocząstek srebra korzystnie zawarte jest w przedziale od 100 mg/dm3 do 5000 mg/dm3.The application relates to a method of producing a silver nanoparticle suspension. The method of producing a suspension of silver nanoparticles consists in reducing the silver salt with a reducing agent of plant origin and is characterized in that as a reducing agent plant hormone is used, the reduction being carried out in the presence of a stabilizer. According to a preferred embodiment, the production method comprises the following steps: a) a stabilizer solution is prepared in water or in a mixture of an organic solvent and water, after which the silver salt (solution A) is dissolved in the solution; b) a solution of the plant hormone is prepared, preferably in the same solvent in which solution A is prepared, the weight ratio of amber to solvent being in the range from 1: 100 to 10: 1 (solution B); c) solution B is added to solution A, with continuous stirring, at a temperature that maintains the liquid state of the solvent or is elevated to the boiling point of the solvent, the volume ratio of solution A to solution B being in the range from 1: 100 to 100: 1. Disclosed also a silver nanoparticle suspension containing plant hormone and stabilizer in which the concentration of silver nanoparticles is preferably in the range from 100 mg / dm3 to 5000 mg / dm3.

PL413444A 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles PL234471B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL413444A PL234471B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL413444A PL234471B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Publications (2)

Publication Number Publication Date
PL413444A1 true PL413444A1 (en) 2017-02-13
PL234471B1 PL234471B1 (en) 2020-02-28

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ID=57965439

Family Applications (1)

Application Number Title Priority Date Filing Date
PL413444A PL234471B1 (en) 2015-08-06 2015-08-06 Method for producing a suspension of silver nanoparticles and the suspension of silver nanoparticles

Country Status (1)

Country Link
PL (1) PL234471B1 (en)

Also Published As

Publication number Publication date
PL234471B1 (en) 2020-02-28

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