PL413951A1 - Method for producing optically pure (+)-(R)-7-hydroxyflavanone - Google Patents
Method for producing optically pure (+)-(R)-7-hydroxyflavanoneInfo
- Publication number
- PL413951A1 PL413951A1 PL413951A PL41395115A PL413951A1 PL 413951 A1 PL413951 A1 PL 413951A1 PL 413951 A PL413951 A PL 413951A PL 41395115 A PL41395115 A PL 41395115A PL 413951 A1 PL413951 A1 PL 413951A1
- Authority
- PL
- Poland
- Prior art keywords
- hydroxyflavanone
- optically pure
- hours
- organic solvent
- water
- Prior art date
Links
- SWAJPHCXKPCPQZ-CQSZACIVSA-N (2R)-7-hydroxyflavanone Chemical compound C1([C@H]2CC(=O)C3=CC=C(C=C3O2)O)=CC=CC=C1 SWAJPHCXKPCPQZ-CQSZACIVSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000003960 organic solvent Substances 0.000 abstract 2
- -1 7-hydroxyflavanone (±) -acetate Chemical compound 0.000 abstract 1
- 241000228245 Aspergillus niger Species 0.000 abstract 1
- 241000233866 Fungi Species 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 238000004587 chromatography analysis Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000002537 cosmetic Substances 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 230000009466 transformation Effects 0.000 abstract 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Sposób wytwarzania (+)-(R)-7-hydroksyflawanonu o wzorze 2, polega na tym, że do podłoża odpowiedniego dla grzybów strzępkowych wprowadza się szczep Aspergillus niger SBJ, następnie po upływie co najmniej 48 godzin do hodowli wprowadza się substrat, którym jest (±)-octan 7-hydroksyflawanonu o wzorze 1, rozpuszczony w rozpuszczalniku organicznym mieszającym się z wodą, transformację prowadzi się przy ciągłym wstrząsaniu, co najwyżej 30 godzin, po czym produkt ekstrahuje się rozpuszczalnikiem organicznym niemieszającym się z wodą i oczyszcza chromatograficznie. Związek ten może znaleźć zastosowanie jako antyoksydant w przemyśle spożywczym oraz jako składnik preparatów farmaceutycznych i kosmetycznych.The method of producing (+) - (R) -7-hydroxyflavanone of the formula II consists in the introduction of Aspergillus niger SBJ strain into a medium suitable for filamentous fungi, then after at least 48 hours the substrate which is 7-hydroxyflavanone (±) -acetate 1, dissolved in a water-miscible organic solvent, transformation is carried out with continuous shaking, at most 30 hours, after which the product is extracted with a water-immiscible organic solvent and purified by chromatography. This compound can be used as an antioxidant in the food industry and as an ingredient in pharmaceutical and cosmetic preparations.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL41395115A PL233420B1 (en) | 2015-09-14 | 2015-09-14 | Method for producing optically pure (+)-(R)-7-hydroxyflavanone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL41395115A PL233420B1 (en) | 2015-09-14 | 2015-09-14 | Method for producing optically pure (+)-(R)-7-hydroxyflavanone |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL413951A1 true PL413951A1 (en) | 2017-03-27 |
| PL233420B1 PL233420B1 (en) | 2019-10-31 |
Family
ID=58360215
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL41395115A PL233420B1 (en) | 2015-09-14 | 2015-09-14 | Method for producing optically pure (+)-(R)-7-hydroxyflavanone |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL233420B1 (en) |
-
2015
- 2015-09-14 PL PL41395115A patent/PL233420B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL233420B1 (en) | 2019-10-31 |
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