PL418768A1 - Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV) - Google Patents

Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV)

Info

Publication number
PL418768A1
PL418768A1 PL418768A PL41876816A PL418768A1 PL 418768 A1 PL418768 A1 PL 418768A1 PL 418768 A PL418768 A PL 418768A PL 41876816 A PL41876816 A PL 41876816A PL 418768 A1 PL418768 A1 PL 418768A1
Authority
PL
Poland
Prior art keywords
zirconium
sol
oxide
ultrasound
volume
Prior art date
Application number
PL418768A
Other languages
English (en)
Other versions
PL238466B1 (pl
Inventor
Przemysław Jodłowski
Roman Jędrzejczyk
Damian Chlebda
Anna Dziedzicka
Original Assignee
Politechnika Krakowska im. Tadeusza Kościuszki
Uniwersytet Jagielloński
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Krakowska im. Tadeusza Kościuszki, Uniwersytet Jagielloński filed Critical Politechnika Krakowska im. Tadeusza Kościuszki
Priority to PL418768A priority Critical patent/PL238466B1/pl
Priority to PCT/PL2017/000066 priority patent/WO2018056849A1/en
Publication of PL418768A1 publication Critical patent/PL418768A1/pl
Publication of PL238466B1 publication Critical patent/PL238466B1/pl

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0219—Coating the coating containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0225—Coating of metal substrates
    • B01J37/0226—Oxidation of the substrate, e.g. anodisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0228—Coating in several steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/036—Precipitation; Co-precipitation to form a gel or a cogel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • B01J37/343—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of ultrasonic wave energy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0213—Preparation of the impregnating solution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Health & Medical Sciences (AREA)
  • Plasma & Fusion (AREA)
  • Toxicology (AREA)
  • Dispersion Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV), w którym to sposobie na aktywowane metaliczne podłoże z utworzoną na nim warstwą tlenków nanosi się zol, zawierający tlenek cyrkonu(IV), suszy naniesioną warstwę i następnie kalcynuje, przy czym w procesie preparowania zolu używa się n-propanolanu cyrkonu(IV) jako prekursora ZrO2, a ponadto lodowatego kwasu octowego, wody i substancji stabilizujących zol, takich jak glikole, charakteryzuje się tym, że tlenek cyrkonu(IV) zawarty w zolu nanoszonym na metaliczne podłoże stanowi produkt procesu, w którym roztwór o stężeniu 1 - 2,5 mol/dm3 n-propanolanu cyrkonu(IV) rozpuszczonego w n-propanolu, z dodatkiem lodowatego kwasu octowego w ilości 50 - 65% obj. w odniesieniu do objętości roztworu n-propanolanu cyrkonu(IV), poddaje się działaniu pola ultradźwiękowego (ultradźwięków) o mocy 60 - 100 W i częstotliwości 20 kHz i utrzymując temperaturę układu w zakresie 10 do 60°C, wprowadza się do niego małymi porcjami wodę dejonizowaną w ilości 10 - 15% obj. w przeliczeniu na całkowitą objętość układu, przy czym wodę zaczyna wprowadzać się korzystnie po 20 min. od zapoczątkowania oddziaływania ultradźwiękami na układ. Operację oddziaływania ultradźwiękami na roztwór układ prowadzi się przez okres 25 do 60 min. przy nieciągłych w czasie seriach, gdzie poszczególne przedziały czasu oddziaływania ultradźwiękami trwają przez 1 do 5 min., a przerwy między nimi 1 do 3 min.
PL418768A 2016-09-20 2016-09-20 Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV) PL238466B1 (pl)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PL418768A PL238466B1 (pl) 2016-09-20 2016-09-20 Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV)
PCT/PL2017/000066 WO2018056849A1 (en) 2016-09-20 2017-06-19 Method of preparing a layer of zirconium(iv) oxide as a catalytic carrier on a metallic substrate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL418768A PL238466B1 (pl) 2016-09-20 2016-09-20 Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV)

Publications (2)

Publication Number Publication Date
PL418768A1 true PL418768A1 (pl) 2018-03-26
PL238466B1 PL238466B1 (pl) 2021-08-23

Family

ID=59631837

Family Applications (1)

Application Number Title Priority Date Filing Date
PL418768A PL238466B1 (pl) 2016-09-20 2016-09-20 Sposób wytwarzania na metalicznym podłożu warstwy katalitycznego nośnika z tlenku cyrkonu(IV)

Country Status (2)

Country Link
PL (1) PL238466B1 (pl)
WO (1) WO2018056849A1 (pl)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114324568A (zh) * 2021-12-31 2022-04-12 浙江大学 鸟嘌呤肽核酸自组装纳米球基光子晶体的声场辅助制备方法
CN114427086B (zh) * 2022-01-08 2022-10-11 华中科技大学 一种Al2O3纳米片增强ZrO2阻氚涂层及其制备方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4331631A (en) 1979-11-28 1982-05-25 General Motors Corporation Enhanced oxide whisker growth on peeled Al-containing stainless steel foil
US4318828A (en) 1980-08-15 1982-03-09 General Motors Corporation Enhanced oxide whisker growth on cold-rolled aluminum-containing stainless steel foil
CN1056198C (zh) 1994-05-19 2000-09-06 北京科技大学 溶胶凝胶法制备抗高温氧化陶瓷涂层的工艺方法
US5585136A (en) 1995-03-22 1996-12-17 Queen's University At Kingston Method for producing thick ceramic films by a sol gel coating process
PL183563B1 (pl) 1997-07-11 2002-06-28 Andreas Steiner Sposób wytwarzania warstwy Al2O3 na powierzchni elementów ze stali chromowo-aluminiowej

Also Published As

Publication number Publication date
PL238466B1 (pl) 2021-08-23
WO2018056849A1 (en) 2018-03-29

Similar Documents

Publication Publication Date Title
PE20130181A1 (es) Procedimiento para la preparacion de 4-{4-[({[4-cloro-3-(trifluorometil)fenil]amino}carbonil)amino]-3-fluorofenoxi}-n-metilpiridina-2-carboxamida, sus sales y su monohidrato
AR090017A1 (es) Agonistas de fgfr1 y sus metodos de uso
AR091098A1 (es) ANTICUERPOS E INMUNOCONJUGADOS CONTRA Ly6E Y METODOS DE USO
MY195318A (en) Multispecific Antibody Constructs
WO2013154999A3 (en) Method of preparation of nanopore and uses thereof
CY1110812T1 (el) Παραγωγα διφαινυλοξυοξικου οξεος για τη θεραπεια αναπνευστικων διαταραχων
WO2013048222A3 (ko) 실리카 합성 펩타이드 및 이의 용도
CL2012003722A1 (es) Compuestos derivados del acido naf-2-ilacetico; composicion farmaceutica; y uso para el tratamiento del sida.
ATE530204T1 (de) Antimikrobielles medizintechnisches produkt, verfahren zu seiner herstellung und verwendung
MX2016007839A (es) Recubrimiento para superficie.
CL2017002233A1 (es) Un factor de coagulación (fvii o fviia) modificado con tres péptidos carboxi terminal de gonadotropina coriónica unidos al carboxi terminal de fvii o fviia; polinucleótido que lo codifica; composición farmacéutica que lo comprende; uso de fvii o fviia modificado para el tratamiento de coagulación de la sangre o un trastorno de coagulación; método para extender la vía media biológica de un factor de coagulación; método para producir dicho fvii o fviia.
EA201400401A1 (ru) Биокомпозит для регенерации поврежденных тканей и органов, набор для изготовления биокомпозита и способ лечения
MX349068B (es) Material semiconductor de titania nanoestructurada y proceso de obtencion.
MX383551B (es) Derivados de glutarimida, uso de los mismos, composicion farmaceutica basada en los mismos y metodos para producir derivados de glutarimida
EA201691563A1 (ru) Сухой кислотный концентрат в гранулированной форме
AR090881A1 (es) Un proceso para la produccion de acido metacrilico y sus derivados y polimeros producidos a partir de estos
ATE510818T1 (de) Kohlensäure- und schwefelsäuresalze von 3-(2,2,2- trimethylhydrazinium)propionatestern und deren verwendung zur herstellung von 3-(2,2,2- trimethylhydrazinium)propionat-dihydrat
EP2647609A3 (de) Glutaminreiche Peptide als Luftporenbildner in Baustoffmassen
BR112012020306A8 (pt) Método para produzir ácido pirrolidona carboxílico ou um sal do mesmo
JP2016525410A5 (pl)
BR112013026747A2 (pt) processo e aparelho
BR112014004829A2 (pt) métodos de ativação da provocação das substâncias de geração de sinal encapsulado e mecanismo utilizando as substâncias de geração de sinal ativado
EP2646366A4 (en) PROCESS FOR THE PREPARATION OF SALPETIC ACID
RU2013151577A (ru) Способ получения гуанина
EP3787985A4 (en) Method and system for preparing hypochlorous acid solutions with prolonged shelf-life