PL421574A1 - Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania - Google Patents

Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania

Info

Publication number
PL421574A1
PL421574A1 PL421574A PL42157417A PL421574A1 PL 421574 A1 PL421574 A1 PL 421574A1 PL 421574 A PL421574 A PL 421574A PL 42157417 A PL42157417 A PL 42157417A PL 421574 A1 PL421574 A1 PL 421574A1
Authority
PL
Poland
Prior art keywords
barbital
nitropyridine
crystals
amino
producing
Prior art date
Application number
PL421574A
Other languages
English (en)
Other versions
PL237569B1 (pl
Inventor
Marlena GRYL
Tomasz SEIDLER
Joanna WOJNARSKA
Original Assignee
Uniwersytet Jagielloński
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uniwersytet Jagielloński filed Critical Uniwersytet Jagielloński
Priority to PL421574A priority Critical patent/PL237569B1/pl
Priority to PCT/PL2018/050020 priority patent/WO2018208181A1/en
Publication of PL421574A1 publication Critical patent/PL421574A1/pl
Publication of PL237569B1 publication Critical patent/PL237569B1/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72—Nitrogen atoms
    • C07D213/73—Unsubstituted amino or imino radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/60—Three or more oxygen or sulfur atoms
    • C07D239/62—Barbituric acids
    • C07D239/64—Salts of organic bases; Organic double compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/54—Organic compounds
    • C30B29/58—Macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/02—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent
    • C30B7/04—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent using aqueous solvents
    • G—PHYSICS
    • G02—OPTICS
    • G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
    • G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
    • G02F1/35—Non-linear optics
    • G02F1/355—Non-linear optics characterised by the materials used
    • G02F1/361—Organic materials
    • G02F1/3611—Organic materials containing Nitrogen
    • G02F1/3612—Heterocycles having N as heteroatom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Nonlinear Science (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Pyridine Compounds (AREA)

Abstract

Przedmiotem zgłoszenia są ko-kryształy 2-amino-5-nitropirydyny i barbitalu o dyfraktogramie rentgenowskim wykazującym obecność charakterystycznych odległości międzypłaszczyznowych wynoszących dla formy (I) dhkl 2.966X, 3.5823, 2.9972, 2.9302, 3.0772, 5.2652, 5.7601, 4.0461 oraz dla formy (II) dhkl 3.165X, 3.0506, 3.1173, 5.1172, 3.2742, 4.8192, 2.7672, 3.4612. Przedmiotem zgłoszenia jest również sposób wytwarzania ko-kryształów 2-amino-5-nitropirydyny i barbitalu.
PL421574A 2017-05-12 2017-05-12 Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania PL237569B1 (pl)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PL421574A PL237569B1 (pl) 2017-05-12 2017-05-12 Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania
PCT/PL2018/050020 WO2018208181A1 (en) 2017-05-12 2018-05-12 2-amino-5-nitropyridine and barbital co-crystals and method for production thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL421574A PL237569B1 (pl) 2017-05-12 2017-05-12 Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania

Publications (2)

Publication Number Publication Date
PL421574A1 true PL421574A1 (pl) 2018-11-19
PL237569B1 PL237569B1 (pl) 2021-05-04

Family

ID=64104798

Family Applications (1)

Application Number Title Priority Date Filing Date
PL421574A PL237569B1 (pl) 2017-05-12 2017-05-12 Ko-kryształy 2-amino-5-nitropirydyny i barbitalu oraz sposób ich wytwarzania

Country Status (2)

Country Link
PL (1) PL237569B1 (pl)
WO (1) WO2018208181A1 (pl)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116536747A (zh) * 2022-11-18 2023-08-04 中国科学院福建物质结构研究所 C5h14n2i4化合物、双折射光学晶体及其制法和用途

Also Published As

Publication number Publication date
WO2018208181A1 (en) 2018-11-15
PL237569B1 (pl) 2021-05-04

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