PL422655A1 - Method for synthesis of metal nanoparticles - Google Patents
Method for synthesis of metal nanoparticlesInfo
- Publication number
- PL422655A1 PL422655A1 PL422655A PL42265517A PL422655A1 PL 422655 A1 PL422655 A1 PL 422655A1 PL 422655 A PL422655 A PL 422655A PL 42265517 A PL42265517 A PL 42265517A PL 422655 A1 PL422655 A1 PL 422655A1
- Authority
- PL
- Poland
- Prior art keywords
- extract
- peat
- metal nanoparticles
- synthesis
- nanoparticles
- Prior art date
Links
- 239000002082 metal nanoparticle Substances 0.000 title abstract 3
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- 239000003415 peat Substances 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 3
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 abstract 3
- 229910004042 HAuCl4 Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 abstract 1
- 229910000366 copper(II) sulfate Inorganic materials 0.000 abstract 1
- 239000008367 deionised water Substances 0.000 abstract 1
- 229910021641 deionized water Inorganic materials 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000004021 humic acid Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000002105 nanoparticle Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób syntezy nanocząstek metali, który polega na tym, że w pierwszym etapie otrzymuje się ekstrakt torfowy zawierający kwasy humusowe poprzez utworzenie roztworu torfu zawierającego wymienione kwasy w ilości co najmniej 5 g na 1 kg użytego torfu, w wodzie dejonizowanej w stosunku od 0,1 :1 do korzystnie 1:1 jednostek masy, wspomagając tą operację wstrząsaniem, z którego korzystnie po ogrzaniu do temperatury 90°C przez minimum 15 minut separuje się ekstrakt od nierozpuszczalnych resztek, a następnie zatęża się go najlepiej do połowy. Następnie w kolejnym etapie wprowadza się do niego rozpuszczalne w wodzie sole metali korzystnie w formie ciekłej, z których będą syntetyzowane nanocząstki, w ilości od 0,25 g do 5 g na litr ekstraktu i po wymieszaniu pozostawia się w suchym i ciemnym pomieszczeniu w celu powstania nanocząstek metalu. Korzystnym jest by jako sole do otrzymanego ekstraktu wprowadzać sól AgNO3 lub CuSO4 lub Zr(NO3)2 lub HAuCl4.The subject of the application is a method for the synthesis of metal nanoparticles, which consists in obtaining, in the first stage, a peat extract containing humic acids by creating a peat solution containing the mentioned acids in an amount of at least 5 g per 1 kg of peat used, in deionized water in a ratio of 0 1:1 to preferably 1:1 mass units, supporting this operation with shaking, which, preferably after heating to 90°C for at least 15 minutes, separates the extract from insoluble residues and then concentrates it, preferably to half. Then, in the next stage, water-soluble metal salts are introduced into it, preferably in liquid form, from which nanoparticles will be synthesized, in an amount from 0.25 g to 5 g per liter of extract and, after mixing, it is left in a dry and dark room to form metal nanoparticles. It is preferable to introduce AgNO3 or CuSO4 or Zr(NO3)2 or HAuCl4 salt as salts into the obtained extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL422655A PL238644B1 (en) | 2017-08-28 | 2017-08-28 | Method for synthesis of metal nanoparticles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL422655A PL238644B1 (en) | 2017-08-28 | 2017-08-28 | Method for synthesis of metal nanoparticles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL422655A1 true PL422655A1 (en) | 2019-03-11 |
| PL238644B1 PL238644B1 (en) | 2021-09-20 |
Family
ID=65629571
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL422655A PL238644B1 (en) | 2017-08-28 | 2017-08-28 | Method for synthesis of metal nanoparticles |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL238644B1 (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005080489A1 (en) * | 2004-02-23 | 2005-09-01 | Caiteng Zhang | A solution of metal-polymer chelate(s) and applications thereof |
| US20110117179A1 (en) * | 2005-06-03 | 2011-05-19 | Prezacor, Inc. | Compositions comprising elemental metals and uses therefor |
-
2017
- 2017-08-28 PL PL422655A patent/PL238644B1/en unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005080489A1 (en) * | 2004-02-23 | 2005-09-01 | Caiteng Zhang | A solution of metal-polymer chelate(s) and applications thereof |
| US20110117179A1 (en) * | 2005-06-03 | 2011-05-19 | Prezacor, Inc. | Compositions comprising elemental metals and uses therefor |
Non-Patent Citations (1)
| Title |
|---|
| B. MARCZEWSKA, R. KUZIOŁA, M. SZOJA, WYKORZYSTANIE TORFU DO USUWANIA METALI CIĘŻKICH Z WÓD, 2016 * |
Also Published As
| Publication number | Publication date |
|---|---|
| PL238644B1 (en) | 2021-09-20 |
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