PL443497A1 - Sposób utleniania α-pinenu - Google Patents

Sposób utleniania α-pinenu

Info

Publication number
PL443497A1
PL443497A1 PL443497A PL44349723A PL443497A1 PL 443497 A1 PL443497 A1 PL 443497A1 PL 443497 A PL443497 A PL 443497A PL 44349723 A PL44349723 A PL 44349723A PL 443497 A1 PL443497 A1 PL 443497A1
Authority
PL
Poland
Prior art keywords
pinene
weight
catalyst
oxygen
oxidation
Prior art date
Application number
PL443497A
Other languages
English (en)
Other versions
PL247497B1 (pl
Inventor
Agnieszka Wróblewska
Jadwiga Grzeszczak
Original Assignee
Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zachodniopomorski Uniwersytet Technologiczny W Szczecinie filed Critical Zachodniopomorski Uniwersytet Technologiczny W Szczecinie
Priority to PL443497A priority Critical patent/PL247497B1/pl
Publication of PL443497A1 publication Critical patent/PL443497A1/pl
Publication of PL247497B1 publication Critical patent/PL247497B1/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C13/00—Cyclic hydrocarbons containing rings other than, or in addition to, six-membered aromatic rings
    • C07C13/02—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof
    • C07C13/16—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with a six-membered ring
    • C07C13/20—Monocyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with a six-membered ring with a cyclohexene ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/16—Clays or other mineral silicates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C13/00—Cyclic hydrocarbons containing rings other than, or in addition to, six-membered aromatic rings
    • C07C13/28—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof
    • C07C13/32—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with condensed rings
    • C07C13/39—Polycyclic hydrocarbons or acyclic hydrocarbon derivatives thereof with condensed rings with a bicyclo ring system containing seven carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
    • C07C27/10—Processes involving the simultaneous production of more than one class of oxygen-containing compounds by oxidation of hydrocarbons
    • C07C27/12—Processes involving the simultaneous production of more than one class of oxygen-containing compounds by oxidation of hydrocarbons with oxygen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób utleniania α-pinenu, według wynalazku w obecności katalizatora zawierającego tytan, pod ciśnieniem atmosferycznym z intensywnością mieszania 500 obr./minutę w atmosferze tlenu, przy czym do reaktora szklanego wprowadza się w pierwszej kolejności α-pinen, później katalizator, na samym końcu doprowadza się tlen przez bełkotkę, stosując przepływ tlenu 40 ml/min, zaś proces utleniania prowadzi się w temperaturze 80°C - 120°C, w czasie od 1 h do 24 h, charakteryzuje się tym, że stosuje się katalizator zeolitowy - klinoptylolity o różnej wielkości cząstek 20 µm, 50 µm, 200 µm lub 500 - 1000 µm i o zawartości w strukturze tytanu 0,2% wagowych oraz glinu 3,7% - 4,8% wagowych, w ilości 0,05% - 1,50% wagowych w mieszaninie reakcyjnej.
PL443497A 2023-01-16 2023-01-16 Sposób utleniania α-pinenu PL247497B1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL443497A PL247497B1 (pl) 2023-01-16 2023-01-16 Sposób utleniania α-pinenu

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL443497A PL247497B1 (pl) 2023-01-16 2023-01-16 Sposób utleniania α-pinenu

Publications (2)

Publication Number Publication Date
PL443497A1 true PL443497A1 (pl) 2024-07-22
PL247497B1 PL247497B1 (pl) 2025-07-14

Family

ID=91958082

Family Applications (1)

Application Number Title Priority Date Filing Date
PL443497A PL247497B1 (pl) 2023-01-16 2023-01-16 Sposób utleniania α-pinenu

Country Status (1)

Country Link
PL (1) PL247497B1 (pl)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL449818A1 (pl) * 2024-09-13 2026-03-16 Zachodniopomorski Uniwersytet Technologiczny W Szczecinie Sposób utleniania α-pinenu w obecności katalizatora

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2156514A1 (es) * 1998-12-04 2001-06-16 Univ Valencia Politecnica Materiales microporosos de alta superficie activos en reacciones de oxidacion.
CN112742453A (zh) * 2019-10-30 2021-05-04 中国石油化工股份有限公司 一种含钛分子筛的制备方法、含钛分子筛和催化剂及选择性氧化方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2156514A1 (es) * 1998-12-04 2001-06-16 Univ Valencia Politecnica Materiales microporosos de alta superficie activos en reacciones de oxidacion.
CN112742453A (zh) * 2019-10-30 2021-05-04 中国石油化工股份有限公司 一种含钛分子筛的制备方法、含钛分子筛和催化剂及选择性氧化方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
A. WRÓBLEWSKA ET AL: "Microporous and Mesoporous Materials, Volume 305, 1 October 2020, 110384", THE APPLICATION OF TS-1 MATERIALS WITH DIFFERENT TITANIUM CONTENTS AS CATALYSTS FOR THE AUTOXIDATION OF Α-PINENE *
A. WRÓBLEWSKA ET: "Materials 2021, 14(24), 7799", THE STUDIES ON Α-PINENE OXIDATION OVER THE TS-1. THE INFLUENCE OF THE TEMPERATURE, REACTION TIME, TITANIUM AND CATALYST CONTENT *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL449818A1 (pl) * 2024-09-13 2026-03-16 Zachodniopomorski Uniwersytet Technologiczny W Szczecinie Sposób utleniania α-pinenu w obecności katalizatora

Also Published As

Publication number Publication date
PL247497B1 (pl) 2025-07-14

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