PL445394A1 - N-(5′-fenylo-[1,1′:3′,1″-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)benzamid i sposób jego otrzymywania - Google Patents

N-(5′-fenylo-[1,1′:3′,1″-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)benzamid i sposób jego otrzymywania

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Publication number
PL445394A1
PL445394A1 PL445394A PL44539423A PL445394A1 PL 445394 A1 PL445394 A1 PL 445394A1 PL 445394 A PL445394 A PL 445394A PL 44539423 A PL44539423 A PL 44539423A PL 445394 A1 PL445394 A1 PL 445394A1
Authority
PL
Poland
Prior art keywords
triphenylvinyl
terphenyl
phenyl
benzamide
mixture
Prior art date
Application number
PL445394A
Other languages
English (en)
Other versions
PL247543B1 (pl
Inventor
Artur Kasprzak
Jakub Cyniak
Original Assignee
Politechnika Warszawska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Warszawska filed Critical Politechnika Warszawska
Priority to PL445394A priority Critical patent/PL247543B1/pl
Publication of PL445394A1 publication Critical patent/PL445394A1/pl
Publication of PL247543B1 publication Critical patent/PL247543B1/pl

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/64—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings
    • C07C233/67—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms
    • C07C233/75—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by singly-bound oxygen atoms with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by a carbon atom of a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Przedmiotem zgłoszenia jest N-(5'-fenylo-[1,1':3',1"-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)benzamid o wzorze 1 oraz sposób jego otrzymania z zastosowaniem reakcji sprzęgania, charakteryzujący się tym, że przygotowuje się mieszaninę kwasu 4-(1,2,2-trifenylowinylo)benzoesowego, 5'-fenylo-[1,1':3',1"-terfenylo]-4-aminy i reagenta sprzęgającego w stosunku molowym 1:1:1, po czym do mieszaniny dodaje się roztwór kwasu solnego o stężeniu 1 mol•dm3, a uzyskany osad wydziela się z mieszaniny reakcyjnej na drodze ekstrakcji, zaś czysty produkt wyodrębnia się na drodze chromatografii kolumnowej.
PL445394A 2023-06-29 2023-06-29 N-(5’-fenylo-[1,1’:3’,1”-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)- benzamid i sposób jego otrzymywania PL247543B1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL445394A PL247543B1 (pl) 2023-06-29 2023-06-29 N-(5’-fenylo-[1,1’:3’,1”-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)- benzamid i sposób jego otrzymywania

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL445394A PL247543B1 (pl) 2023-06-29 2023-06-29 N-(5’-fenylo-[1,1’:3’,1”-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)- benzamid i sposób jego otrzymywania

Publications (2)

Publication Number Publication Date
PL445394A1 true PL445394A1 (pl) 2024-12-30
PL247543B1 PL247543B1 (pl) 2025-07-21

Family

ID=96430936

Family Applications (1)

Application Number Title Priority Date Filing Date
PL445394A PL247543B1 (pl) 2023-06-29 2023-06-29 N-(5’-fenylo-[1,1’:3’,1”-terfenylo]-4-ylo)-4-(1,2,3-trifenylowinylo)- benzamid i sposób jego otrzymywania

Country Status (1)

Country Link
PL (1) PL247543B1 (pl)

Also Published As

Publication number Publication date
PL247543B1 (pl) 2025-07-21

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