PL446667A1 - Glikoporfiryny typu A4 i sposób ich otrzymywania - Google Patents
Glikoporfiryny typu A4 i sposób ich otrzymywaniaInfo
- Publication number
- PL446667A1 PL446667A1 PL446667A PL44666723A PL446667A1 PL 446667 A1 PL446667 A1 PL 446667A1 PL 446667 A PL446667 A PL 446667A PL 44666723 A PL44666723 A PL 44666723A PL 446667 A1 PL446667 A1 PL 446667A1
- Authority
- PL
- Poland
- Prior art keywords
- general formula
- temperature
- compound
- type
- glycoporphyrin
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 150000001875 compounds Chemical class 0.000 abstract 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000003446 ligand Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 229910000073 phosphorus hydride Inorganic materials 0.000 abstract 1
- 229910000027 potassium carbonate Inorganic materials 0.000 abstract 1
- VFWRGKJLLYDFBY-UHFFFAOYSA-N silver;hydrate Chemical compound O.[Ag].[Ag] VFWRGKJLLYDFBY-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Przedmiotem zgłoszenia jest glikoporfiryna typu A<sub>4</sub> o ogólnym wzorze 1 oraz sposób jej wytwarzania obejmujący: a) reakcję 5,10,15,20-tetrakis(4-(4,4,5,5-tetrametylo-1,3,2-dioksoborolan-2-ylo)fenylo)porfirynato)cynku(II) z związkiem o wzorze ogólnym 2 w mieszaninie N,N-dimetyloformamidu i toluenu w stosunku objętościowym 1:5, w obecności katalizatora palladowego, ligandu fosfinowego, tlenku srebra (I) i zasady w temperaturze 60 - 80°C, korzystnie w temperaturze 70°C przez 3 - 24 h, korzystnie przez 18 h z otrzymaniem związku o wzorze ogólnym 3; b) reakcję związku o wzorze ogólnym 3 otrzymanego w etapie a) z węglanem metalu, korzystnie węglanem potasu prowadzoną w mieszaninie metanolu i chlorku metylenu w stosunku objętościowym 1:1, w temperaturze 20 - 50°C, korzystnie w temperaturze pokojowej z otrzymaniem glikoporfiryny o wzorze ogólnym 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL446667A PL446667A1 (pl) | 2023-11-07 | 2023-11-07 | Glikoporfiryny typu A4 i sposób ich otrzymywania |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL446667A PL446667A1 (pl) | 2023-11-07 | 2023-11-07 | Glikoporfiryny typu A4 i sposób ich otrzymywania |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL446667A1 true PL446667A1 (pl) | 2024-06-03 |
Family
ID=91333047
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL446667A PL446667A1 (pl) | 2023-11-07 | 2023-11-07 | Glikoporfiryny typu A4 i sposób ich otrzymywania |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL446667A1 (pl) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL453256A1 (pl) * | 2025-09-17 | 2026-04-27 | Politechnika Warszawska | Związki porfirynowo-cukrowe typu A4 oraz sposób ich wytwarzania |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080279781A1 (en) * | 2007-05-10 | 2008-11-13 | Brookhaven Science Associates, Llc | Glycosylated Carboranylporphyrins and Uses Thereof |
| WO2013015774A1 (en) * | 2011-07-22 | 2013-01-31 | Biolitec Pharma Marketing Ltd | Glyco-substituted dihydroxy-chlorins and b-functionalized chlorins for anti-microbial photodynamic therapy |
-
2023
- 2023-11-07 PL PL446667A patent/PL446667A1/pl unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080279781A1 (en) * | 2007-05-10 | 2008-11-13 | Brookhaven Science Associates, Llc | Glycosylated Carboranylporphyrins and Uses Thereof |
| WO2013015774A1 (en) * | 2011-07-22 | 2013-01-31 | Biolitec Pharma Marketing Ltd | Glyco-substituted dihydroxy-chlorins and b-functionalized chlorins for anti-microbial photodynamic therapy |
Non-Patent Citations (1)
| Title |
|---|
| GODLEWSKI B. ET AL., SONOGASHIRA CROSS-COUPLING AS A KEY STEP IN THE SYNTHESIS OF NEW GLYCOPORPHYRINS. ORG. CHEM. FRONT., 2022,9, 2396-2404; HTTPS://DOI.ORG/10.1039/D1QO01909K * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL453256A1 (pl) * | 2025-09-17 | 2026-04-27 | Politechnika Warszawska | Związki porfirynowo-cukrowe typu A4 oraz sposób ich wytwarzania |
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