PL445313A1 - Glikoporfiryny i sposób ich otrzymywania - Google Patents

Glikoporfiryny i sposób ich otrzymywania

Info

Publication number
PL445313A1
PL445313A1 PL445313A PL44531323A PL445313A1 PL 445313 A1 PL445313 A1 PL 445313A1 PL 445313 A PL445313 A PL 445313A PL 44531323 A PL44531323 A PL 44531323A PL 445313 A1 PL445313 A1 PL 445313A1
Authority
PL
Poland
Prior art keywords
general formula
compound
glycoporphyrins
temperature
reacting
Prior art date
Application number
PL445313A
Other languages
English (en)
Inventor
Maciej Malinowski
Bartosz Godlewski
Mikołaj Ziółkowski
Dariusz Baran
Original Assignee
Politechnika Warszawska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Warszawska filed Critical Politechnika Warszawska
Priority to PL445313A priority Critical patent/PL445313A1/pl
Publication of PL445313A1 publication Critical patent/PL445313A1/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

Przedmiotem wynalazku jest glikoporfiryna o ogólnym wzorze 1 oraz sposób jej wytwarzania obejmujący: a) reakcję (5-(4-(4,4,5,5-tetrametylo-1,3,2-dioksoboralan-2-ylo)fenylo-10,15,20-trifenyloporfirynato)cynku(II) ze związkiem o wzorze ogólnym 2 lub ze związkiem o wzorze ogólnym 3 w mieszaninie N,N-dimetyloformamidu i toluenu w stosunku objętościowym 1:5, w obecności katalizatora palladowego, ligandu fosfinowego, tlenku srebra (I) i zasady w temperaturze 70°C-110°C przez 3-24 h, korzystnie przez 18 h z otrzymaniem związku o wzorze ogólnym 4 lub 5; b) reakcję związku o wzorze ogólnym 4 lub 5 otrzymanego w etapie a) z węglanem metalu prowadzoną w mieszaninie metanolu i chlorku metylenu w stosunku objętościowym 1:1, w temperaturze 20°C-50°C, korzystnie w temperaturze pokojowej z otrzymaniem glikoporfiryn o wzorze ogólnym 1.
PL445313A 2023-06-22 2023-06-22 Glikoporfiryny i sposób ich otrzymywania PL445313A1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL445313A PL445313A1 (pl) 2023-06-22 2023-06-22 Glikoporfiryny i sposób ich otrzymywania

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL445313A PL445313A1 (pl) 2023-06-22 2023-06-22 Glikoporfiryny i sposób ich otrzymywania

Publications (1)

Publication Number Publication Date
PL445313A1 true PL445313A1 (pl) 2024-12-23

Family

ID=94644290

Family Applications (1)

Application Number Title Priority Date Filing Date
PL445313A PL445313A1 (pl) 2023-06-22 2023-06-22 Glikoporfiryny i sposób ich otrzymywania

Country Status (1)

Country Link
PL (1) PL445313A1 (pl)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL451782A1 (pl) * 2025-04-11 2025-12-08 Politechnika Warszawska Glikoporfiryny typu trans-A2B2 oraz sposób ich otrzymywania

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080279781A1 (en) * 2007-05-10 2008-11-13 Brookhaven Science Associates, Llc Glycosylated Carboranylporphyrins and Uses Thereof
WO2013015774A1 (en) * 2011-07-22 2013-01-31 Biolitec Pharma Marketing Ltd Glyco-substituted dihydroxy-chlorins and b-functionalized chlorins for anti-microbial photodynamic therapy

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080279781A1 (en) * 2007-05-10 2008-11-13 Brookhaven Science Associates, Llc Glycosylated Carboranylporphyrins and Uses Thereof
WO2013015774A1 (en) * 2011-07-22 2013-01-31 Biolitec Pharma Marketing Ltd Glyco-substituted dihydroxy-chlorins and b-functionalized chlorins for anti-microbial photodynamic therapy

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
GODLEWSKI B. ET AL., SONOGASHIRA CROSS-COUPLING AS A KEY STEP IN THE SYNTHESIS OF NEW GLYCOPORPHYRINS. ORG. CHEM. FRONT., 2022,9, 2396-2404; HTTPS://DOI.ORG/10.1039/D1QO01909K *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL451782A1 (pl) * 2025-04-11 2025-12-08 Politechnika Warszawska Glikoporfiryny typu trans-A2B2 oraz sposób ich otrzymywania

Similar Documents

Publication Publication Date Title
PL445313A1 (pl) Glikoporfiryny i sposób ich otrzymywania
DE602004022389D1 (de) Ir-PHENYLPYRAZOLKOMPLEXE
US20120025177A1 (en) Phosphorescent light-emitting iridium complex containing pyridyltriazole ligand
MY136959A (en) Quinoline intermediates of receptor tyrosine kinase inhibitors and the synthesis thereof
CY1106989T1 (el) Ενεργοποιητες γλυκοκινασης τυπου 5-υποκατεστημενης πυραζινης ή πυριδινης
CY1109680T1 (el) Υποκατεστημενες πυριδινονες ως ρυθμιστες της ρ38 μαρ κινασης
NO20073701L (no) Nye fremgangsmater for fremstilling av et 2H-kromen
Hu et al. Blue-to-green electrophosphorescence from iridium (III) complexes with cyclometalated pyrimidine ligands
ATE526381T1 (de) Organische elektrolumineszenzvorrichtung sowie platinverbindung
EP4234524A3 (en) Compound for organic electronic element, organic electronic element using the same, and an electronic device thereof
BG102525A (en) Method and intermediate compounds for the preparation of 1-benzyl-4-((5,6-dimethoxy-1-indanon)-2-yl)-methylpiperidine
PL446667A1 (pl) Glikoporfiryny typu A4 i sposób ich otrzymywania
DK2035437T3 (da) Boran-æter-komplekser
Nosova et al. Synthesis and fluorescent properties of 2-styryl-6, 7-difluoro-8-hydroxyquinoline and its Zn (II) complex
SG158864A1 (en) Processes for preparing 4-(phenoxy-5-methyl-pyrimidin-4-yloxy)piperidine-1- carboxylic acid derivatives and related compounds
Sangari et al. Influence of ancillary ligands on the photophysical properties of cyclometalated organoplatinum (II) complexes
Huixia et al. Synthesis and characterization of blue-to-green electrophosphorescence emitter based on pyrazole iridium complexes
West-Nielsen et al. Strong intramolecular hydrogen bonding involving nitro-and acetyl groups. Deuterium isotope effects on chemical shifts
ATE455118T1 (de) Chemisches zwischenprodukt
AU2001269388A1 (en) New processes for the production of fexofenadine
US4367336A (en) 2-Substituted-5-trifluoromethylpyridines and process for producing the same
Casas et al. Novel gold (I) 7-azacoumarin complex: Synthesis, structure, optical properties, and cytotoxic effects
Edkins et al. Divergent Approach for Tris-Heteroleptic Cyclometalated Iridium Complexes Using Triisopropylsilylethynyl-Substituted Synthons
US5416236A (en) Aniline derivatives and process for producing the same
Pinter et al. Blue emissive palladium (II) complex with benzoquinoline and N-heterocyclic carbene ligands