PL448691A1 - Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego - Google Patents

Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego

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Publication number
PL448691A1
PL448691A1 PL448691A PL44869124A PL448691A1 PL 448691 A1 PL448691 A1 PL 448691A1 PL 448691 A PL448691 A PL 448691A PL 44869124 A PL44869124 A PL 44869124A PL 448691 A1 PL448691 A1 PL 448691A1
Authority
PL
Poland
Prior art keywords
mbar
rpm
aminoacetic acid
sodium
hydrin
Prior art date
Application number
PL448691A
Other languages
English (en)
Inventor
Iga Bartłomiejczyk
Małgorzata Milewska
Andrzej Milewski
Original Assignee
Politechnika Śląska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Śląska filed Critical Politechnika Śląska
Priority to PL448691A priority Critical patent/PL448691A1/pl
Publication of PL448691A1 publication Critical patent/PL448691A1/pl

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego, który polega na tym, że kwas aminooctowy i wodorotlenek sodu w równomolowej ilości rozpuszcza się w wodzie otrzymując roztwór od 40% do 67% wag. aminooctanu sodu (glicynianu sodu), następnie na każdy mol glicynianu sodu wprowadza się od 1 mol do 2 mol epichlorohydryny w porcjach stanowiących nie więcej niż 26% wag. roztworu glicynianu sodu, jednocześnie reagenty miesza się w zakresie od 100 rpm do 250 rpm, w czasie od 24h do 72h, po czym mieszaninę poreakcyjną zakwasza się kwasem mineralnym do pH od 2 do 1, odparowuje odbierając wodę w temperaturze do 55°C pod obniżonym ciśnieniem od 250 mbar do 6 mbar, otrzymany produkt zadaje się metanolem w ilości równej zawartości mieszaniny poreakcyjnej i miesza przez 4h do 8h w zakresie od 100 rpm do 250 rpm, nierozpuszczalną frakcję usuwa się przez filtrację, a metanol odparowuje w temperaturze do 30°C pod obniżonym ciśnieniem od 130 mbar do 6 mbar.
PL448691A 2024-05-28 2024-05-28 Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego PL448691A1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL448691A PL448691A1 (pl) 2024-05-28 2024-05-28 Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL448691A PL448691A1 (pl) 2024-05-28 2024-05-28 Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego

Publications (1)

Publication Number Publication Date
PL448691A1 true PL448691A1 (pl) 2025-12-01

Family

ID=97831625

Family Applications (1)

Application Number Title Priority Date Filing Date
PL448691A PL448691A1 (pl) 2024-05-28 2024-05-28 Sposób otrzymywania pochodnych hydrynowych kwasu aminooctowego

Country Status (1)

Country Link
PL (1) PL448691A1 (pl)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0770596A1 (en) * 1994-07-08 1997-05-02 Kao Corporation Novel amine compound and detergent composition containing the same
EP3257840A1 (en) * 2015-02-13 2017-12-20 Toray Fine Chemicals Co., Ltd. Method for producing compound having n,n-bis(2-hydroxy-3-chloropropyl)amino group
CN109627181A (zh) * 2019-01-31 2019-04-16 上海锦迪助剂材料有限公司 一种氨基酸改性的两性表面活性剂及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0770596A1 (en) * 1994-07-08 1997-05-02 Kao Corporation Novel amine compound and detergent composition containing the same
EP3257840A1 (en) * 2015-02-13 2017-12-20 Toray Fine Chemicals Co., Ltd. Method for producing compound having n,n-bis(2-hydroxy-3-chloropropyl)amino group
CN109627181A (zh) * 2019-01-31 2019-04-16 上海锦迪助剂材料有限公司 一种氨基酸改性的两性表面活性剂及其制备方法

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