SE452975B - Forfarande for framstellning av granulert stabiliserat natriumperkarbonat - Google Patents

Forfarande for framstellning av granulert stabiliserat natriumperkarbonat

Info

Publication number: SE452975B
Authority: SE; Sweden
Prior art keywords: sodium percarbonate; sodium; hydrogen peroxide; suspension; granulated
Prior art date: 1985-11-15

Application number

SE8505415A

Other languages

English (en)

Swedish (sv)

Other versions

SE8505415L (sv

SE8505415D0 (sv

Inventor

E A Chernyshev

V P Pavlov

J L Martynjuk

V E Trubkin

V V Burdin

E M Emelyanov

L I Ovchinnikova

Z P Volkova

V B Kolevatova

V A Budkov

I A Abramov

P E Zotin

V M Romanov

V A Gradov

L S Shevnitsyn

V V Smirnov

T M Izmailova

V G Braitsev

I S Lukonin

Original Assignee

Gnii Khim

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1985-11-15

Filing date

1985-11-15

Publication date

1988-01-04

1985-11-12 Priority to FI854441A priority Critical patent/FI76054C/fi

1985-11-13 Priority to AT3304/85A priority patent/AT391121B/de

1985-11-15 Application filed by Gnii Khim filed Critical Gnii Khim

1985-11-15 Priority to SE8505415A priority patent/SE452975B/sv

1985-11-15 Publication of SE8505415D0 publication Critical patent/SE8505415D0/xx

1987-05-16 Publication of SE8505415L publication Critical patent/SE8505415L/

1988-01-04 Publication of SE452975B publication Critical patent/SE452975B/sv

Links

VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 title claims description 60
229940045872 sodium percarbonate Drugs 0.000 title claims description 60
238000000034 method Methods 0.000 title claims description 35
238000002360 preparation method Methods 0.000 title claims description 6
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 54
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 34
239000000243 solution Substances 0.000 claims description 32
239000007864 aqueous solution Substances 0.000 claims description 20
239000000725 suspension Substances 0.000 claims description 17
239000000203 mixture Substances 0.000 claims description 14
238000001035 drying Methods 0.000 claims description 10
239000003381 stabilizer Substances 0.000 claims description 8
239000000271 synthetic detergent Substances 0.000 claims description 8
239000007900 aqueous suspension Substances 0.000 claims description 7
238000006243 chemical reaction Methods 0.000 claims description 5
239000008187 granular material Substances 0.000 description 16
239000002245 particle Substances 0.000 description 16
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 13
239000004115 Sodium Silicate Substances 0.000 description 12
229910052911 sodium silicate Inorganic materials 0.000 description 11
GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 10
235000019982 sodium hexametaphosphate Nutrition 0.000 description 10
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 10
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 9
230000015572 biosynthetic process Effects 0.000 description 9
239000012467 final product Substances 0.000 description 9
239000000047 product Substances 0.000 description 9
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 8
229910052760 oxygen Inorganic materials 0.000 description 8
239000001301 oxygen Substances 0.000 description 8
230000003179 granulation Effects 0.000 description 7
238000005469 granulation Methods 0.000 description 7
238000003786 synthesis reaction Methods 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
238000004519 manufacturing process Methods 0.000 description 6
238000003756 stirring Methods 0.000 description 6
238000012360 testing method Methods 0.000 description 6
CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 5
229910001385 heavy metal Inorganic materials 0.000 description 5
238000002156 mixing Methods 0.000 description 5
235000019830 sodium polyphosphate Nutrition 0.000 description 5
239000000470 constituent Substances 0.000 description 4
238000001914 filtration Methods 0.000 description 4
239000012535 impurity Substances 0.000 description 4
235000011007 phosphoric acid Nutrition 0.000 description 4
-1 701 g of dry Chemical compound 0.000 description 3
239000000654 additive Substances 0.000 description 3
229910052783 alkali metal Inorganic materials 0.000 description 2
150000001340 alkali metals Chemical class 0.000 description 2
238000005119 centrifugation Methods 0.000 description 2
239000007795 chemical reaction product Substances 0.000 description 2
239000013078 crystal Substances 0.000 description 2
238000009826 distribution Methods 0.000 description 2
229910052943 magnesium sulfate Inorganic materials 0.000 description 2
235000019341 magnesium sulphate Nutrition 0.000 description 2
239000012452 mother liquor Substances 0.000 description 2
235000019353 potassium silicate Nutrition 0.000 description 2
239000002244 precipitate Substances 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
238000003860 storage Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
229920000388 Polyphosphate Polymers 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
230000000996 additive effect Effects 0.000 description 1
229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
239000007844 bleaching agent Substances 0.000 description 1
235000012180 bread and bread product Nutrition 0.000 description 1
239000012267 brine Substances 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
235000011180 diphosphates Nutrition 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
239000000428 dust Substances 0.000 description 1
230000008030 elimination Effects 0.000 description 1
238000003379 elimination reaction Methods 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
238000002347 injection Methods 0.000 description 1
239000007924 injection Substances 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
239000011777 magnesium Substances 0.000 description 1
229910052749 magnesium Inorganic materials 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
150000002736 metal compounds Chemical class 0.000 description 1
239000010413 mother solution Substances 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
150000003018 phosphorus compounds Chemical class 0.000 description 1
239000001205 polyphosphate Substances 0.000 description 1
235000011176 polyphosphates Nutrition 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000000376 reactant Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
235000017550 sodium carbonate Nutrition 0.000 description 1
229910000029 sodium carbonate Inorganic materials 0.000 description 1
235000019794 sodium silicate Nutrition 0.000 description 1
235000019351 sodium silicates Nutrition 0.000 description 1
HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
230000000087 stabilizing effect Effects 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000013517 stratification Methods 0.000 description 1
238000005303 weighing Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/10—Peroxyhydrates; Peroxyacids or salts thereof containing carbon
- C01B15/103—Peroxyhydrates; Peroxyacids or salts thereof containing carbon containing only alkali metals as metals

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Inorganic Chemistry (AREA)
Detergent Compositions (AREA)

SE8505415A 1985-11-15 1985-11-15 Forfarande for framstellning av granulert stabiliserat natriumperkarbonat SE452975B (sv)

Priority Applications (3)

Application Number	Priority Date	Filing Date	Title
FI854441A FI76054C (fi)	1985-11-15	1985-11-12	Foerfarande foer framstaellning av natriumperkarbonat i granulatform.
AT3304/85A AT391121B (de)	1985-11-15	1985-11-13	Verfahren zur herstellung von granuliertem stabilisiertem natriumperkarbonat
SE8505415A SE452975B (sv)	1985-11-15	1985-11-15	Forfarande for framstellning av granulert stabiliserat natriumperkarbonat

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
SE8505415A SE452975B (sv)	1985-11-15	1985-11-15	Forfarande for framstellning av granulert stabiliserat natriumperkarbonat

Publications (3)

Publication Number	Publication Date
SE8505415D0 SE8505415D0 (sv)	1985-11-15
SE8505415L SE8505415L (sv)	1987-05-16
SE452975B true SE452975B (sv)	1988-01-04

Family

ID=20362150

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SE8505415A SE452975B (sv)	1985-11-15	1985-11-15	Forfarande for framstellning av granulert stabiliserat natriumperkarbonat

Country Status (3)

Country	Link
AT (1)	AT391121B (de)
FI (1)	FI76054C (de)
SE (1)	SE452975B (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FI920318A0 (fi) *	1991-01-25	1992-01-24	Central Glass Co Ltd	Kontinuerligt foerfarande foer framstaellning av natriumperkarbonat.
US5560896A (en) *	1993-08-31	1996-10-01	Degussa Aktiengesellschaft	Method for producing granulated sodium percarbonate
DE4338401A1 (de) *	1993-11-10	1995-05-11	Degussa	Verfahren zur Herstellung von abriebfestem Natriumpercarbonat mit hoher Lösegeschwindigkeit
DE4408359A1 (de) *	1994-03-14	1995-09-21	Henkel Kgaa	Lagerstabil fixiertes Wasserstoffperoxid enthaltende Mehrstoffgemische in Feststofform, Verfahren zu ihrer Herstellung und ihre Verwendung
DE19532558A1 (de) *	1995-09-04	1997-03-06	Henkel Kgaa	Lagerstabil fixiertes Wasserstoffperoxid enthaltende Mehrstoffgemische in Feststofform, Verfahren zu ihrer Herstellung und ihre Verwendung (II)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
LU75466A1 (de) *	1976-07-27	1978-02-08
DE2644147C3 (de) *	1976-09-30	1983-05-19	Degussa Ag, 6000 Frankfurt	Verfahren zur Herstellung eines kompakten, grobkörnigen Natriumpercarbonats
DE2644148C3 (de) *	1976-09-30	1983-05-11	Degussa Ag, 6000 Frankfurt	Kontinuierliches Verfahren zur Herstellung eines kompakten, grobkörnigen Natriumpercarbonats

1985
- 1985-11-12 FI FI854441A patent/FI76054C/fi not_active IP Right Cessation
- 1985-11-13 AT AT3304/85A patent/AT391121B/de not_active IP Right Cessation
- 1985-11-15 SE SE8505415A patent/SE452975B/sv not_active IP Right Cessation

Also Published As

Publication number	Publication date
FI854441L (fi)	1987-05-13
FI854441A0 (fi)	1985-11-12
ATA330485A (de)	1990-02-15
FI76054B (fi)	1988-05-31
AT391121B (de)	1990-08-27
SE8505415L (sv)	1987-05-16
SE8505415D0 (sv)	1985-11-15
FI76054C (fi)	1988-09-09

Legal Events

Date

Code

Title

Description

1995-01-31

NUG

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Effective date: 19900706

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