SE505324C2 - Framställning av 11C-metyljodid - Google Patents

Framställning av 11C-metyljodid

Info

Publication number: SE505324C2
Authority: SE; Sweden
Prior art keywords: iodine; methyl iodide; trap; capture; produced
Prior art date: 1994-11-14

Application number

SE9403913A

Other languages

English (en)

Swedish (sv)

Other versions

SE9403913D0 (sv

SE9403913L (sv

Inventor

Peter Larsen

Martin Orbe

Kent Dahlstroem

Johan Ulin

Original Assignee

Gems Pet Systems Ab

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1994-11-14

Filing date

1994-11-14

Publication date

1997-08-04

1994-11-14 Application filed by Gems Pet Systems Ab filed Critical Gems Pet Systems Ab

1994-11-14 Priority to SE9403913A priority Critical patent/SE505324C2/sv

1994-11-14 Publication of SE9403913D0 publication Critical patent/SE9403913D0/xx

1995-10-20 Priority to US08/836,606 priority patent/US6008421A/en

1995-10-20 Priority to JP51596496A priority patent/JP3839050B2/ja

1995-10-20 Priority to EP95937259A priority patent/EP0792253B1/en

1995-10-20 Priority to DK95937259T priority patent/DK0792253T3/da

1995-10-20 Priority to CA002205299A priority patent/CA2205299C/en

1995-10-20 Priority to DE69524976T priority patent/DE69524976T2/de

1995-10-20 Priority to AU39419/95A priority patent/AU3941995A/en

1995-10-20 Priority to PCT/SE1995/001247 priority patent/WO1996015086A1/en

1996-05-15 Publication of SE9403913L publication Critical patent/SE9403913L/xx

1997-08-04 Publication of SE505324C2 publication Critical patent/SE505324C2/sv

Links

238000000034 method Methods 0.000 claims abstract description 28
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims abstract description 27
229910052740 iodine Inorganic materials 0.000 claims abstract description 27
239000011630 iodine Substances 0.000 claims abstract description 27
238000006243 chemical reaction Methods 0.000 claims abstract description 18
238000010438 heat treatment Methods 0.000 claims abstract description 14
238000004519 manufacturing process Methods 0.000 claims abstract description 7
238000001816 cooling Methods 0.000 claims description 15
239000000463 material Substances 0.000 claims description 15
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 15
229910052756 noble gas Inorganic materials 0.000 claims description 15
INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 claims description 13
238000009833 condensation Methods 0.000 claims description 11
230000005494 condensation Effects 0.000 claims description 11
239000007788 liquid Substances 0.000 claims description 9
239000002808 molecular sieve Substances 0.000 claims description 9
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 9
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
239000000969 carrier Substances 0.000 claims description 6
239000003054 catalyst Substances 0.000 claims description 5
238000009835 boiling Methods 0.000 claims description 4
239000012535 impurity Substances 0.000 claims description 3
PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical class II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 3
238000012856 packing Methods 0.000 claims description 3
229920000642 polymer Polymers 0.000 claims description 3
239000000843 powder Substances 0.000 claims description 3
230000003134 recirculating effect Effects 0.000 claims description 2
238000010926 purge Methods 0.000 claims 2
239000002516 radical scavenger Substances 0.000 claims 2
239000007789 gas Substances 0.000 abstract description 9
239000011261 inert gas Substances 0.000 abstract 1
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 14
239000000203 mixture Substances 0.000 description 11
229910052734 helium Inorganic materials 0.000 description 7
235000011121 sodium hydroxide Nutrition 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
239000001307 helium Substances 0.000 description 6
SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 6
239000010453 quartz Substances 0.000 description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
229910002092 carbon dioxide Inorganic materials 0.000 description 4
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
239000001569 carbon dioxide Substances 0.000 description 3
238000004817 gas chromatography Methods 0.000 description 3
238000005658 halogenation reaction Methods 0.000 description 3
239000012280 lithium aluminium hydride Substances 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
239000007787 solid Substances 0.000 description 3
108010063955 thrombin receptor peptide (42-47) Proteins 0.000 description 3
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
229910052786 argon Inorganic materials 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
238000010531 catalytic reduction reaction Methods 0.000 description 2
230000026030 halogenation Effects 0.000 description 2
238000006192 iodination reaction Methods 0.000 description 2
229910052754 neon Inorganic materials 0.000 description 2
238000000746 purification Methods 0.000 description 2
230000002285 radioactive effect Effects 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
239000000126 substance Substances 0.000 description 2
MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
229910045601 alloy Inorganic materials 0.000 description 1
239000000956 alloy Substances 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
239000000919 ceramic Substances 0.000 description 1
239000013078 crystal Substances 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
230000000694 effects Effects 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
229910000043 hydrogen iodide Inorganic materials 0.000 description 1
230000026045 iodination Effects 0.000 description 1
HVTICUPFWKNHNG-UHFFFAOYSA-N iodoethane Chemical compound CCI HVTICUPFWKNHNG-UHFFFAOYSA-N 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
229910052743 krypton Inorganic materials 0.000 description 1
-1 lithium aluminum hydride Chemical compound 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
229910052763 palladium Inorganic materials 0.000 description 1
230000002572 peristaltic effect Effects 0.000 description 1
229910052697 platinum Inorganic materials 0.000 description 1
238000007348 radical reaction Methods 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000006722 reduction reaction Methods 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
229910052703 rhodium Inorganic materials 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
229910052724 xenon Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Physical Or Chemical Processes And Apparatus (AREA)

SE9403913A 1994-11-14 1994-11-14 Framställning av 11C-metyljodid SE505324C2 (sv)

Priority Applications (9)

Application Number	Priority Date	Filing Date	Title
SE9403913A SE505324C2 (sv)	1994-11-14	1994-11-14	Framställning av 11C-metyljodid
PCT/SE1995/001247 WO1996015086A1 (en)	1994-11-14	1995-10-20	Production of 11c-methyl iodide
DK95937259T DK0792253T3 (da)	1994-11-14	1995-10-20	Fremstilling af 11C-methyliodid
JP51596496A JP3839050B2 (ja)	1994-11-14	1995-10-20	▲上１１▼ｃ−沃化メチルの製造
EP95937259A EP0792253B1 (en)	1994-11-14	1995-10-20	Production of [11C] methyl iodide
US08/836,606 US6008421A (en)	1994-11-14	1995-10-20	Production of 11 C-methyl iodide
CA002205299A CA2205299C (en)	1994-11-14	1995-10-20	Production of 11c-methyl iodide
DE69524976T DE69524976T2 (de)	1994-11-14	1995-10-20	Herstellung von [11C] Methyljodid
AU39419/95A AU3941995A (en)	1994-11-14	1995-10-20	Production of 11c-methyl iodide

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
SE9403913A SE505324C2 (sv)	1994-11-14	1994-11-14	Framställning av 11C-metyljodid

Publications (3)

Publication Number	Publication Date
SE9403913D0 SE9403913D0 (sv)	1994-11-14
SE9403913L SE9403913L (sv)	1996-05-15
SE505324C2 true SE505324C2 (sv)	1997-08-04

Family

ID=20395962

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SE9403913A SE505324C2 (sv)	1994-11-14	1994-11-14	Framställning av 11C-metyljodid

Country Status (9)

Country	Link
US (1)	US6008421A (da)
EP (1)	EP0792253B1 (da)
JP (1)	JP3839050B2 (da)
AU (1)	AU3941995A (da)
CA (1)	CA2205299C (da)
DE (1)	DE69524976T2 (da)
DK (1)	DK0792253T3 (da)
SE (1)	SE505324C2 (da)
WO (1)	WO1996015086A1 (da)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP5278865B2 (ja) *	2004-05-27	2013-09-04	住友重機械工業株式会社	ヨウ化メチル製造装置、ヨウ化メチル製造方法及びメチルトリフレート製造装置
GB0505952D0 (en)	2005-03-23	2005-04-27	Hammersmith Imanet Ltd	Preparation of 11c methyl iodide
GB2432371B (en)	2005-11-17	2011-06-15	Epichem Ltd	Improved bubbler for the transportation of substances by a carrier gas
WO2007069043A2 (en) *	2005-12-14	2007-06-21	Ge Healthcare Limited	Non thermal plasma method to prepare [11c] methyl iodide from [11c] methane and iodine
US7812201B2 (en)	2008-10-01	2010-10-12	Targa Resources, Inc.	Process and catalyst for converting alkanes
CN102597310B (zh)	2009-11-02	2015-02-04	西格玛-奥吉奇有限责任公司	固态前体输送组件以及相关方法
US8261876B2 (en) *	2010-03-09	2012-09-11	Autoneum Management Ag	Automotive trim part for sound insulation and absorption
JP2010280730A (ja) *	2010-09-22	2010-12-16	Sumitomo Heavy Ind Ltd	ヨウ化メチル製造装置、ヨウ化メチル製造方法及びメチルトリフレート製造装置
US9101895B2 (en)	2011-04-15	2015-08-11	General Electric Company	System for mixing and dispersing microbubble pharmaceuticals
CN104326864B (zh) *	2014-10-15	2016-07-06	太仓沪试试剂有限公司	一种光伏材料用高纯级二碘甲烷的纯化方法
CN104370689B (zh) *	2014-10-20	2016-03-30	太仓沪试试剂有限公司	一种led材料用高纯级碘甲烷的纯化方法
WO2023017343A1 (en) *	2021-08-11	2023-02-16	Novo Integrated Sciences Inc.	Controlled gaseous iodine sublimation from solid iodine for atmospheric iodine nutrition, disinfection and therapeutic uses

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5177275A (en) *	1989-05-01	1993-01-05	Pcr Group, Inc.	Reaction of substrate compounds with fluorine in an eductor

1994
- 1994-11-14 SE SE9403913A patent/SE505324C2/sv not_active IP Right Cessation
1995
- 1995-10-20 DE DE69524976T patent/DE69524976T2/de not_active Expired - Lifetime
- 1995-10-20 US US08/836,606 patent/US6008421A/en not_active Expired - Lifetime
- 1995-10-20 WO PCT/SE1995/001247 patent/WO1996015086A1/en not_active Ceased
- 1995-10-20 AU AU39419/95A patent/AU3941995A/en not_active Abandoned
- 1995-10-20 EP EP95937259A patent/EP0792253B1/en not_active Expired - Lifetime
- 1995-10-20 JP JP51596496A patent/JP3839050B2/ja not_active Expired - Fee Related
- 1995-10-20 DK DK95937259T patent/DK0792253T3/da active
- 1995-10-20 CA CA002205299A patent/CA2205299C/en not_active Expired - Fee Related

Also Published As

Publication number	Publication date
CA2205299A1 (en)	1996-05-23
DK0792253T3 (da)	2002-04-22
DE69524976D1 (de)	2002-02-14
EP0792253B1 (en)	2002-01-09
DE69524976T2 (de)	2002-08-22
AU3941995A (en)	1996-06-06
JPH10509449A (ja)	1998-09-14
EP0792253A1 (en)	1997-09-03
SE9403913D0 (sv)	1994-11-14
JP3839050B2 (ja)	2006-11-01
SE9403913L (sv)	1996-05-15
WO1996015086A1 (en)	1996-05-23
CA2205299C (en)	2007-06-05
US6008421A (en)	1999-12-28

Legal Events

Date	Code	Title	Description
2014-07-01	NUG	Patent has lapsed

Publication	Publication Date	Title
SE505324C2 (sv)	1997-08-04	Framställning av 11C-metyljodid
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JP6078674B2 (ja)	2017-02-08	水素分離膜モジュール及びこれを用いた水素分離方法
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CN115385302B (zh)	2024-01-02	一种废中子靶的氚回收纯化系统及方法
GB2389903A (en)	2003-12-24	Providing a gaseous product for analysis
JP2019059650A (ja)	2019-04-18	酸素同位体置換方法及び酸素同位体置換装置
Mock et al.	1995	Solid-phase reversible trap for [11C] carbon dioxide using carbon molecular sieves
JP5620705B2 (ja)	2014-11-05	酸素同位体の濃縮方法および酸素同位体の濃縮装置
US20100178237A1 (en)	2010-07-15	Process for recovery of water isotopologues
DE102009032241A1 (de)	2011-08-18	Bei Umgebungstemperatur arbeitender Luftzerleger
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FR2553771A1 (fr)	1985-04-26	Procede et dispositif pour concentrer des solutions aqueuses d'oxyde d'ethylene
JPH0531331A (ja)	1993-02-09	水素同位体の分離方法
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WO2010105803A1 (de)	2010-09-23	Vorrichtung zur trennung von gasgemischen in ihre komponenten
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