SG82013A1 - Process for crystallizing and collecting n3-trifluoroacetyl-basic amino acid - Google Patents
Process for crystallizing and collecting n3-trifluoroacetyl-basic amino acidInfo
- Publication number
- SG82013A1 SG82013A1 SG9903657A SG1999003657A SG82013A1 SG 82013 A1 SG82013 A1 SG 82013A1 SG 9903657 A SG9903657 A SG 9903657A SG 1999003657 A SG1999003657 A SG 1999003657A SG 82013 A1 SG82013 A1 SG 82013A1
- Authority
- SG
- Singapore
- Prior art keywords
- amino acid
- basic amino
- trifluoroacetyl
- crystallizing
- collecting
- Prior art date
Links
- 150000001413 amino acids Chemical class 0.000 title abstract 6
- 239000007788 liquid Substances 0.000 abstract 3
- 150000002148 esters Chemical class 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000003002 pH adjusting agent Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/22—Separation; Purification; Stabilisation; Use of additives
- C07C231/24—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5184696 | 1996-03-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SG82013A1 true SG82013A1 (en) | 2001-07-24 |
Family
ID=12898225
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SG9903657A SG82013A1 (en) | 1996-03-08 | 1997-03-06 | Process for crystallizing and collecting n3-trifluoroacetyl-basic amino acid |
Country Status (9)
| Country | Link |
|---|---|
| EP (2) | EP1061067B1 (de) |
| JP (1) | JP3788996B2 (de) |
| AT (2) | ATE202334T1 (de) |
| DE (2) | DE69705275T2 (de) |
| DK (2) | DK0826664T3 (de) |
| ES (2) | ES2209744T3 (de) |
| PT (1) | PT1061067E (de) |
| SG (1) | SG82013A1 (de) |
| WO (1) | WO1997032841A1 (de) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU3075300A (en) * | 1999-01-21 | 2000-08-07 | Kaneka Corporation | Method for isolation of n-protected s-phenylcysteine |
| CN105348134B (zh) * | 2015-12-09 | 2017-06-06 | 九江天赐高新材料有限公司 | 一种n‑酰基氨基酸的精制纯化方法 |
| CN111470993A (zh) * | 2020-05-22 | 2020-07-31 | 安徽安力肽生物科技有限公司 | 一种不结块Beta-丙氨酸制备方法 |
| CN118108617B (zh) * | 2024-03-05 | 2024-10-15 | 山东极地医药科技有限公司 | 一种三氟乙酰赖氨酸的生产工艺 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB938782A (en) * | 1959-02-17 | 1963-10-09 | Hoechst Ag | Process for n-trifluoracetylating amino acids and peptides |
| EP0239063A2 (de) * | 1986-03-27 | 1987-09-30 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | Verfahren zur Herstellung von N-omega-Trifluoracetylaminosäure |
| US4943679A (en) * | 1987-01-26 | 1990-07-24 | Rhone-Poulenc Chimie | Process for the N-ω-trifluoroacetylation of saturated aliphatic monocarboxylic α,ω-diamino acids |
-
1997
- 1997-03-06 DK DK97905454T patent/DK0826664T3/da active
- 1997-03-06 WO PCT/JP1997/000690 patent/WO1997032841A1/ja not_active Ceased
- 1997-03-06 DE DE69705275T patent/DE69705275T2/de not_active Expired - Fee Related
- 1997-03-06 EP EP00120296A patent/EP1061067B1/de not_active Expired - Lifetime
- 1997-03-06 EP EP97905454A patent/EP0826664B1/de not_active Revoked
- 1997-03-06 PT PT00120296T patent/PT1061067E/pt unknown
- 1997-03-06 AT AT97905454T patent/ATE202334T1/de not_active IP Right Cessation
- 1997-03-06 DE DE1997627324 patent/DE69727324T2/de not_active Expired - Fee Related
- 1997-03-06 JP JP53167097A patent/JP3788996B2/ja not_active Expired - Fee Related
- 1997-03-06 AT AT00120296T patent/ATE258162T1/de not_active IP Right Cessation
- 1997-03-06 DK DK00120296T patent/DK1061067T3/da active
- 1997-03-06 ES ES00120296T patent/ES2209744T3/es not_active Expired - Lifetime
- 1997-03-06 ES ES97905454T patent/ES2157555T3/es not_active Expired - Lifetime
- 1997-03-06 SG SG9903657A patent/SG82013A1/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB938782A (en) * | 1959-02-17 | 1963-10-09 | Hoechst Ag | Process for n-trifluoracetylating amino acids and peptides |
| EP0239063A2 (de) * | 1986-03-27 | 1987-09-30 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | Verfahren zur Herstellung von N-omega-Trifluoracetylaminosäure |
| US4943679A (en) * | 1987-01-26 | 1990-07-24 | Rhone-Poulenc Chimie | Process for the N-ω-trifluoroacetylation of saturated aliphatic monocarboxylic α,ω-diamino acids |
Also Published As
| Publication number | Publication date |
|---|---|
| DK0826664T3 (da) | 2001-09-03 |
| DK1061067T3 (da) | 2004-04-05 |
| JP3788996B2 (ja) | 2006-06-21 |
| ATE202334T1 (de) | 2001-07-15 |
| DE69705275T2 (de) | 2002-05-16 |
| DE69705275D1 (de) | 2001-07-26 |
| ATE258162T1 (de) | 2004-02-15 |
| EP0826664B1 (de) | 2001-06-20 |
| EP1061067A2 (de) | 2000-12-20 |
| ES2157555T3 (es) | 2001-08-16 |
| WO1997032841A1 (en) | 1997-09-12 |
| PT1061067E (pt) | 2004-06-30 |
| EP0826664A1 (de) | 1998-03-04 |
| DE69727324T2 (de) | 2004-11-18 |
| DE69727324D1 (de) | 2004-02-26 |
| EP1061067A3 (de) | 2001-01-17 |
| ES2209744T3 (es) | 2004-07-01 |
| EP0826664A4 (de) | 1998-04-29 |
| EP1061067B1 (de) | 2004-01-21 |
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