SU1142162A1 - Способ приготовлени катализатора на носителе дл процесса селективного гидрировани - Google Patents

Способ приготовлени катализатора на носителе дл процесса селективного гидрировани Download PDF

Info

Publication number: SU1142162A1
Authority: SU; USSR - Soviet Union
Prior art keywords: nickel; catalyst; drying; salt; washing
Prior art date: 1980-01-02

Application number

SU807771477A

Other languages

English (en)

Russian (ru)

Inventor

Владимир Заплетал

Ярослав Прхлик

Франтишек Углирж

Йиржи Чмолик

Йиржи Ружичка

Вацлав Спевачек

Владимир Прохазка

Йиржи Стухлик

Original Assignee

Устреди Про Выналезы А Объевы Чсав (Инопредприятие)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-01-02

Filing date

1980-11-25

Publication date

1985-02-28

1980-11-25 Application filed by Устреди Про Выналезы А Объевы Чсав (Инопредприятие) filed Critical Устреди Про Выналезы А Объевы Чсав (Инопредприятие)

1985-02-28 Application granted granted Critical

1985-02-28 Publication of SU1142162A1 publication Critical patent/SU1142162A1/ru

Links

239000003054 catalyst Substances 0.000 title claims abstract description 34
238000000034 method Methods 0.000 title claims abstract description 17
238000005984 hydrogenation reaction Methods 0.000 title description 11
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 42
229910052759 nickel Inorganic materials 0.000 claims abstract description 19
238000001035 drying Methods 0.000 claims abstract description 16
229910000033 sodium borohydride Inorganic materials 0.000 claims abstract description 16
239000012279 sodium borohydride Substances 0.000 claims abstract description 16
238000005406 washing Methods 0.000 claims abstract description 14
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 11
238000001354 calcination Methods 0.000 claims abstract description 11
230000000694 effects Effects 0.000 claims abstract description 11
229930195733 hydrocarbon Natural products 0.000 claims abstract description 10
150000002430 hydrocarbons Chemical class 0.000 claims abstract description 10
239000002244 precipitate Substances 0.000 claims abstract description 9
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 8
229910052739 hydrogen Inorganic materials 0.000 claims abstract description 8
239000001257 hydrogen Substances 0.000 claims abstract description 8
150000002815 nickel Chemical class 0.000 claims abstract description 8
239000000203 mixture Substances 0.000 claims abstract description 6
229910052751 metal Inorganic materials 0.000 claims abstract description 5
239000002184 metal Substances 0.000 claims abstract description 5
150000003839 salts Chemical class 0.000 claims abstract description 5
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 4
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 4
229910052804 chromium Inorganic materials 0.000 claims abstract description 4
239000011651 chromium Substances 0.000 claims abstract description 4
229910052802 copper Inorganic materials 0.000 claims abstract description 4
239000010949 copper Substances 0.000 claims abstract description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 4
229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 4
229910052709 silver Inorganic materials 0.000 claims abstract description 3
239000004332 silver Substances 0.000 claims abstract description 3
KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims abstract 4
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims abstract 2
229910052763 palladium Inorganic materials 0.000 claims abstract 2
238000000465 moulding Methods 0.000 claims description 4
239000007864 aqueous solution Substances 0.000 claims description 3
230000008021 deposition Effects 0.000 claims 1
230000001376 precipitating effect Effects 0.000 abstract description 3
238000007493 shaping process Methods 0.000 abstract description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
230000003197 catalytic effect Effects 0.000 abstract 1
238000001723 curing Methods 0.000 abstract 1
239000000243 solution Substances 0.000 description 12
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
239000000725 suspension Substances 0.000 description 7
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
238000001914 filtration Methods 0.000 description 5
238000001556 precipitation Methods 0.000 description 5
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
229910021586 Nickel(II) chloride Inorganic materials 0.000 description 3
QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 3
229910000008 nickel(II) carbonate Inorganic materials 0.000 description 3
ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 description 3
238000006722 reduction reaction Methods 0.000 description 3
RRKODOZNUZCUBN-CCAGOZQPSA-N (1z,3z)-cycloocta-1,3-diene Chemical compound C1CC\C=C/C=C\C1 RRKODOZNUZCUBN-CCAGOZQPSA-N 0.000 description 2
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
WJTCGQSWYFHTAC-UHFFFAOYSA-N cyclooctane Chemical compound C1CCCCCCC1 WJTCGQSWYFHTAC-UHFFFAOYSA-N 0.000 description 2
239000004914 cyclooctane Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
239000007791 liquid phase Substances 0.000 description 2
239000012452 mother liquor Substances 0.000 description 2
KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 description 2
150000002894 organic compounds Chemical class 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
239000011541 reaction mixture Substances 0.000 description 2
239000000741 silica gel Substances 0.000 description 2
229910002027 silica gel Inorganic materials 0.000 description 2
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
239000011734 sodium Substances 0.000 description 2
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
238000010521 absorption reaction Methods 0.000 description 1
239000003513 alkali Substances 0.000 description 1
239000012670 alkaline solution Substances 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
UCIYGNATMHQYCT-OWOJBTEDSA-N cyclodecene Chemical compound C1CCCC\C=C\CCC1 UCIYGNATMHQYCT-OWOJBTEDSA-N 0.000 description 1
ZOLLIQAKMYWTBR-RYMQXAEESA-N cyclododecatriene Chemical compound C/1C\C=C\CC\C=C/CC\C=C\1 ZOLLIQAKMYWTBR-RYMQXAEESA-N 0.000 description 1
URYYVOIYTNXXBN-UPHRSURJSA-N cyclooctene Chemical compound C1CCC\C=C/CC1 URYYVOIYTNXXBN-UPHRSURJSA-N 0.000 description 1
239000004913 cyclooctene Substances 0.000 description 1
238000011010 flushing procedure Methods 0.000 description 1
239000002638 heterogeneous catalyst Substances 0.000 description 1
150000004678 hydrides Chemical class 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 1
229910000363 nickel(II) sulfate Inorganic materials 0.000 description 1
BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 1
230000008092 positive effect Effects 0.000 description 1
238000011084 recovery Methods 0.000 description 1
239000011833 salt mixture Substances 0.000 description 1
229910001961 silver nitrate Inorganic materials 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1

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Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Steroid Compounds (AREA)

SU807771477A 1980-01-02 1980-11-25 Способ приготовлени катализатора на носителе дл процесса селективного гидрировани SU1142162A1 (ru)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
CS580A CS211004B1 (en)	1980-01-02	1980-01-02	Preparation method of nickel catalyst on the carrier for selective hydrogenizations

Publications (1)

Publication Number	Publication Date
SU1142162A1 true SU1142162A1 (ru)	1985-02-28

Family

ID=5331436

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SU807771477A SU1142162A1 (ru)	1980-01-02	1980-11-25	Способ приготовлени катализатора на носителе дл процесса селективного гидрировани

Country Status (4)

Country	Link
BG (1)	BG37550A1 (cs)
CS (1)	CS211004B1 (cs)
DD (1)	DD157495A3 (cs)
SU (1)	SU1142162A1 (cs)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EA012411B1 (ru) *	2004-03-19	2009-10-30	Каталитик Дистиллейшн Текнолоджиз	Никелевый катализатор, способ получения катализатора и способ селективного гидрирования

1980
- 1980-01-02 CS CS580A patent/CS211004B1/cs unknown
- 1980-11-17 BG BG4969280A patent/BG37550A1/xx unknown
- 1980-11-17 DD DD22529980A patent/DD157495A3/de not_active IP Right Cessation
- 1980-11-25 SU SU807771477A patent/SU1142162A1/ru active

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EA012411B1 (ru) *	2004-03-19	2009-10-30	Каталитик Дистиллейшн Текнолоджиз	Никелевый катализатор, способ получения катализатора и способ селективного гидрирования

Also Published As

Publication number	Publication date
DD157495A3 (de)	1982-11-17
BG37550A1 (en)	1985-07-16
CS211004B1 (en)	1982-01-29

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SU1142162A1 - Способ приготовлени катализатора на носителе дл процесса селективного гидрировани - Google Patents

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Links

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Applications Claiming Priority (1)

Publications (1)

Family

ID=5331436

Family Applications (1)

Country Status (4)

Cited By (1)

Cited By (1)

Also Published As

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