SU474971A4 - Способ получени этиленового ненасыщенного сложного бета-окси-эфира - Google Patents

Способ получени этиленового ненасыщенного сложного бета-окси-эфира

Info

Publication number: SU474971A4
Authority: SU; USSR - Soviet Union
Prior art keywords: reaction; acid; gel; tin; catalyst
Prior art date: 1972-04-10

Application number

SU1907616A

Other languages

English (en)

Russian (ru)

Inventor

Б.Рэдлав Сол

Original Assignee

Континентал Кэн Компани Инк (Фирма)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1972-04-10

Filing date

1973-04-09

Publication date

1975-06-25

1973-04-09 Application filed by Континентал Кэн Компани Инк (Фирма) filed Critical Континентал Кэн Компани Инк (Фирма)

1975-06-25 Application granted granted Critical

1975-06-25 Publication of SU474971A4 publication Critical patent/SU474971A4/ru

Links

VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 title claims description 3
239000005977 Ethylene Substances 0.000 title claims description 3
238000004519 manufacturing process Methods 0.000 title description 5
238000006243 chemical reaction Methods 0.000 claims description 17
239000002253 acid Substances 0.000 claims description 13
239000003054 catalyst Substances 0.000 claims description 10
230000015572 biosynthetic process Effects 0.000 claims description 8
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 7
239000007795 chemical reaction product Substances 0.000 claims description 7
150000002148 esters Chemical class 0.000 claims description 7
238000000034 method Methods 0.000 claims description 7
239000000047 product Substances 0.000 claims description 7
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
239000011541 reaction mixture Substances 0.000 claims description 6
NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 5
IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 5
239000000203 mixture Substances 0.000 claims description 5
239000003381 stabilizer Substances 0.000 claims description 5
-1 tin halide salt Chemical class 0.000 claims description 4
AXZWODMDQAVCJE-UHFFFAOYSA-L tin(II) chloride (anhydrous) Chemical compound [Cl-].[Cl-].[Sn+2] AXZWODMDQAVCJE-UHFFFAOYSA-L 0.000 claims description 4
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 3
125000004432 carbon atom Chemical group C* 0.000 claims description 3
150000003839 salts Chemical class 0.000 claims description 3
229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 2
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
150000001735 carboxylic acids Chemical class 0.000 claims description 2
229910052736 halogen Inorganic materials 0.000 claims description 2
235000011150 stannous chloride Nutrition 0.000 claims description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 6
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 6
239000011521 glass Substances 0.000 claims 2
235000011007 phosphoric acid Nutrition 0.000 claims 2
238000003786 synthesis reaction Methods 0.000 claims 2
229930185605 Bisphenol Natural products 0.000 claims 1
LCFVJGUPQDGYKZ-UHFFFAOYSA-N Bisphenol A diglycidyl ether Chemical compound C=1C=C(OCC2OC2)C=CC=1C(C)(C)C(C=C1)=CC=C1OCC1CO1 LCFVJGUPQDGYKZ-UHFFFAOYSA-N 0.000 claims 1
241000795633 Olea <sea slug> Species 0.000 claims 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 1
125000005396 acrylic acid ester group Chemical group 0.000 claims 1
239000003513 alkali Substances 0.000 claims 1
150000003841 chloride salts Chemical class 0.000 claims 1
230000000052 comparative effect Effects 0.000 claims 1
238000005202 decontamination Methods 0.000 claims 1
230000003588 decontaminative effect Effects 0.000 claims 1
XXBDWLFCJWSEKW-UHFFFAOYSA-N dimethylbenzylamine Chemical compound CN(C)CC1=CC=CC=C1 XXBDWLFCJWSEKW-UHFFFAOYSA-N 0.000 claims 1
238000002474 experimental method Methods 0.000 claims 1
238000009472 formulation Methods 0.000 claims 1
230000005865 ionizing radiation Effects 0.000 claims 1
208000028867 ischemia Diseases 0.000 claims 1
229910001510 metal chloride Inorganic materials 0.000 claims 1
239000012299 nitrogen atmosphere Substances 0.000 claims 1
238000006116 polymerization reaction Methods 0.000 claims 1
CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 claims 1
229910001950 potassium oxide Inorganic materials 0.000 claims 1
CZEZFPXHDTYEBI-UNNPPQAFSA-N rosane Chemical compound C1CCC(C)(C)[C@H]2[C@@H]1[C@]1(C)CC[C@](CC)(C)C[C@H]1CC2 CZEZFPXHDTYEBI-UNNPPQAFSA-N 0.000 claims 1
150000003512 tertiary amines Chemical class 0.000 claims 1
238000004448 titration Methods 0.000 claims 1
229920006395 saturated elastomer Polymers 0.000 description 6
239000000126 substance Substances 0.000 description 4
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
150000007513 acids Chemical class 0.000 description 3
125000003118 aryl group Chemical group 0.000 description 3
239000000463 material Substances 0.000 description 3
230000005855 radiation Effects 0.000 description 3
239000007787 solid Substances 0.000 description 3
239000002904 solvent Substances 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
125000001931 aliphatic group Chemical group 0.000 description 2
239000003153 chemical reaction reagent Substances 0.000 description 2
239000003795 chemical substances by application Substances 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
238000000576 coating method Methods 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
239000000976 ink Substances 0.000 description 2
150000008442 polyphenolic compounds Chemical class 0.000 description 2
235000013824 polyphenols Nutrition 0.000 description 2
235000011118 potassium hydroxide Nutrition 0.000 description 2
238000000926 separation method Methods 0.000 description 2
DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical compound NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
239000004593 Epoxy Substances 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
239000004721 Polyphenylene oxide Substances 0.000 description 1
239000012298 atmosphere Substances 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
LDHQCZJRKDOVOX-NSCUHMNNSA-N crotonic acid Chemical compound C\C=C\C(O)=O LDHQCZJRKDOVOX-NSCUHMNNSA-N 0.000 description 1
230000000694 effects Effects 0.000 description 1
125000003700 epoxy group Chemical group 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
125000000623 heterocyclic group Chemical group 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
230000003993 interaction Effects 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
229910052744 lithium Inorganic materials 0.000 description 1
229910052751 metal Inorganic materials 0.000 description 1
239000002184 metal Substances 0.000 description 1
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
239000000178 monomer Substances 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
235000015097 nutrients Nutrition 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
IPCSVZSSVZVIGE-UHFFFAOYSA-N palmitic acid group Chemical group C(CCCCCCCCCCCCCCC)(=O)O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 1
239000000123 paper Substances 0.000 description 1
FDPIMTJIUBPUKL-UHFFFAOYSA-N pentan-3-one Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 description 1
239000003504 photosensitizing agent Substances 0.000 description 1
230000000704 physical effect Effects 0.000 description 1
229920000058 polyacrylate Polymers 0.000 description 1
229920000647 polyepoxide Polymers 0.000 description 1
229920000570 polyether Polymers 0.000 description 1
MWWATHDPGQKSAR-UHFFFAOYSA-N propyne Chemical compound CC#C MWWATHDPGQKSAR-UHFFFAOYSA-N 0.000 description 1
239000012429 reaction media Substances 0.000 description 1
229920005989 resin Polymers 0.000 description 1
239000011347 resin Substances 0.000 description 1
230000002441 reversible effect Effects 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
239000000758 substrate Substances 0.000 description 1
LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
239000002023 wood Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/62—Use of additives, e.g. for stabilisation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/24—Preparation of carboxylic acid esters by reacting carboxylic acids or derivatives thereof with a carbon-to-oxygen ether bond, e.g. acetal, tetrahydrofuran
- C07C67/26—Preparation of carboxylic acid esters by reacting carboxylic acids or derivatives thereof with a carbon-to-oxygen ether bond, e.g. acetal, tetrahydrofuran with an oxirane ring
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/14—Polycondensates modified by chemical after-treatment
- C08G59/1433—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds
- C08G59/1438—Polycondensates modified by chemical after-treatment with organic low-molecular-weight compounds containing oxygen
- C08G59/1455—Monocarboxylic acids, anhydrides, halides, or low-molecular-weight esters thereof
- C08G59/1461—Unsaturated monoacids
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
- C08L63/10—Epoxy resins modified by unsaturated compounds
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Materials Engineering (AREA)
Engineering & Computer Science (AREA)
Life Sciences & Earth Sciences (AREA)
Wood Science & Technology (AREA)
Emergency Medicine (AREA)
General Chemical & Material Sciences (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Macromonomer-Based Addition Polymer (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Epoxy Resins (AREA)
Polymerisation Methods In General (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

SU1907616A 1972-04-10 1973-04-09 Способ получени этиленового ненасыщенного сложного бета-окси-эфира SU474971A4 (ru)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US24277772A	1972-04-10	1972-04-10
US30610672A	1972-11-13	1972-11-13

Related Parent Applications (1)

Application Number	Title	Priority Date	Filing Date
SU306106 Addition

Publications (1)

Publication Number	Publication Date
SU474971A4 true SU474971A4 (ru)	1975-06-25

Family

ID=26935330

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SU1907616A SU474971A4 (ru)	1972-04-10	1973-04-09	Способ получени этиленового ненасыщенного сложного бета-окси-эфира

Country Status (11)

Country	Link
JP (1)	JPS5610299B2 (fr)
CA (1)	CA1010189A (fr)
DD (1)	DD107014A5 (fr)
DE (1)	DE2317523C2 (fr)
FR (1)	FR2179893B1 (fr)
GB (1)	GB1400978A (fr)
IT (1)	IT988619B (fr)
NL (1)	NL7304913A (fr)
RO (1)	RO62889A (fr)
SE (1)	SE403771B (fr)
SU (1)	SU474971A4 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4316952A (en)	1980-05-12	1982-02-23	Minnesota Mining And Manufacturing Company	Energy sensitive element having crosslinkable polyester
US4309529A (en)	1980-05-12	1982-01-05	Minnesota Mining And Manufacturing Company	Water-dispersible energy curable heterocyclic group-containing polyesters
DE3316593A1 (de) *	1983-05-06	1984-11-08	Basf Ag, 6700 Ludwigshafen	Verfahren zur herstellung von (meth)-acrylsaeureestern und deren verwendung
DE3528461A1 (de) *	1985-08-08	1987-02-19	Basf Ag	Verfahren zur herstellung von vinylesterharzen
US6706208B2 (en)	1999-12-22	2004-03-16	Nippon Shokubai Co., Ltd.	Stabilized hydroxyalkyl (meth)acrylate

1973
- 1973-03-22 SE SE7304028A patent/SE403771B/xx unknown
- 1973-03-30 IT IT2239973A patent/IT988619B/it active
- 1973-04-07 DE DE19732317523 patent/DE2317523C2/de not_active Expired
- 1973-04-09 NL NL7304913A patent/NL7304913A/xx not_active Application Discontinuation
- 1973-04-09 JP JP3964873A patent/JPS5610299B2/ja not_active Expired
- 1973-04-09 CA CA168,205A patent/CA1010189A/en not_active Expired
- 1973-04-09 RO RO7442273A patent/RO62889A/fr unknown
- 1973-04-09 SU SU1907616A patent/SU474971A4/ru active
- 1973-04-10 DD DD17007273A patent/DD107014A5/xx unknown
- 1973-04-10 FR FR7312799A patent/FR2179893B1/fr not_active Expired
- 1973-04-10 GB GB1702573A patent/GB1400978A/en not_active Expired

Also Published As

Publication number	Publication date
JPS5610299B2 (fr)	1981-03-06
CA1010189A (en)	1977-05-10
DE2317523A1 (de)	1973-11-08
SE403771B (sv)	1978-09-04
FR2179893B1 (fr)	1977-08-19
FR2179893A1 (fr)	1973-11-23
JPS497213A (fr)	1974-01-22
DE2317523C2 (de)	1982-07-29
RO62889A (fr)	1978-01-15
NL7304913A (fr)	1973-10-12
IT988619B (it)	1975-04-30
DD107014A5 (fr)	1974-07-12
GB1400978A (en)	1975-07-16

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US2733252A (en)	1956-01-31	Salts of fatty acid esters of lactylic
DE915870C (de)	1954-07-29	Verfahren zur Herstellung von Mischpolymerisaten
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