SU854929A1 - Способ получени аллантоина - Google Patents

Способ получени аллантоина Download PDF

Info

Publication number: SU854929A1
Authority: SU; USSR - Soviet Union
Prior art keywords: mol; acid; glyoxal; urea; allantoin
Prior art date: 1976-10-29

Application number

SU772530556A

Other languages

English (en)

Russian (ru)

Inventor

Оме Роланд

Шимке Ингольф

Руше Йохен

Original Assignee

Феб Штикштоффверк Пистеритц (Инопредприятие)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1976-10-29

Filing date

1977-10-10

Publication date

1981-08-15

1977-10-10 Application filed by Феб Штикштоффверк Пистеритц (Инопредприятие) filed Critical Феб Штикштоффверк Пистеритц (Инопредприятие)

1981-08-15 Application granted granted Critical

1981-08-15 Publication of SU854929A1 publication Critical patent/SU854929A1/ru

Links

POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 title claims abstract description 24
238000000034 method Methods 0.000 title claims abstract description 20
POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 title claims abstract description 12
229960000458 allantoin Drugs 0.000 title claims abstract description 12
LEQAOMBKQFMDFZ-UHFFFAOYSA-N glyoxal Chemical compound O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 claims abstract description 44
229940015043 glyoxal Drugs 0.000 claims abstract description 22
XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 13
239000004202 carbamide Substances 0.000 claims abstract description 13
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 9
IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 claims abstract description 9
239000002253 acid Substances 0.000 claims abstract description 9
229910017604 nitric acid Inorganic materials 0.000 claims abstract description 9
239000000203 mixture Substances 0.000 claims abstract description 8
239000000706 filtrate Substances 0.000 claims abstract description 7
229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 6
239000011707 mineral Substances 0.000 claims abstract description 6
150000001868 cobalt Chemical class 0.000 claims abstract description 5
150000003863 ammonium salts Chemical class 0.000 claims abstract description 4
MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 claims description 13
150000003839 salts Chemical class 0.000 claims description 4
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims description 2
238000010438 heat treatment Methods 0.000 claims 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 12
229910001868 water Inorganic materials 0.000 abstract description 12
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 8
229910052757 nitrogen Inorganic materials 0.000 abstract description 4
230000003197 catalytic effect Effects 0.000 abstract description 3
239000002537 cosmetic Substances 0.000 abstract description 3
239000003814 drug Substances 0.000 abstract description 2
241001484259 Lacuna Species 0.000 abstract 1
239000003795 chemical substances by application Substances 0.000 abstract 1
238000001816 cooling Methods 0.000 description 8
LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 8
HHLFWLYXYJOTON-UHFFFAOYSA-N glyoxylic acid Chemical compound OC(=O)C=O HHLFWLYXYJOTON-UHFFFAOYSA-N 0.000 description 6
238000003756 stirring Methods 0.000 description 6
MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 description 5
238000001914 filtration Methods 0.000 description 5
JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 5
BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 4
229910052921 ammonium sulfate Inorganic materials 0.000 description 4
235000011130 ammonium sulphate Nutrition 0.000 description 4
239000011541 reaction mixture Substances 0.000 description 4
235000010288 sodium nitrite Nutrition 0.000 description 4
QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 3
239000000047 product Substances 0.000 description 3
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
239000010941 cobalt Substances 0.000 description 2
229910017052 cobalt Inorganic materials 0.000 description 2
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
230000003993 interaction Effects 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
239000012452 mother liquor Substances 0.000 description 2
PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 1
239000004254 Ammonium phosphate Substances 0.000 description 1
102100035475 Blood vessel epicardial substance Human genes 0.000 description 1
235000009417 Helenium Nutrition 0.000 description 1
241000521915 Helenium Species 0.000 description 1
101001094636 Homo sapiens Blood vessel epicardial substance Proteins 0.000 description 1
101000608194 Homo sapiens Pyrin domain-containing protein 1 Proteins 0.000 description 1
101000595404 Homo sapiens Ribonucleases P/MRP protein subunit POP1 Proteins 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
SVMCDCBHSKARBQ-UHFFFAOYSA-N acetic acid;cobalt Chemical compound [Co].CC(O)=O SVMCDCBHSKARBQ-UHFFFAOYSA-N 0.000 description 1
235000019270 ammonium chloride Nutrition 0.000 description 1
229910000148 ammonium phosphate Inorganic materials 0.000 description 1
235000019289 ammonium phosphates Nutrition 0.000 description 1
GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 description 1
MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
ZQVMTYNYYKCYRF-UHFFFAOYSA-N diazanium hydron trisulfate Chemical compound [H+].[H+].[H+].[H+].[NH4+].[NH4+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZQVMTYNYYKCYRF-UHFFFAOYSA-N 0.000 description 1
150000002391 heterocyclic compounds Chemical class 0.000 description 1
MOOYVEVEDVVKGD-UHFFFAOYSA-N oxaldehydic acid;hydrate Chemical compound O.OC(=O)C=O MOOYVEVEDVVKGD-UHFFFAOYSA-N 0.000 description 1
239000007800 oxidant agent Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D233/88—Nitrogen atoms, e.g. allantoin

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Cosmetics (AREA)
Catalysts (AREA)

SU772530556A 1976-10-29 1977-10-10 Способ получени аллантоина SU854929A1 (ru)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DD19551776A DD131171A2 (de)	1976-10-29	1976-10-29	Verfahren zur herstellung von allantoin

Publications (1)

Publication Number	Publication Date
SU854929A1 true SU854929A1 (ru)	1981-08-15

Family

ID=5506135

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SU772530556A SU854929A1 (ru)	1976-10-29	1977-10-10	Способ получени аллантоина

Country Status (8)

Country	Link
BG (1)	BG37288A1 (cs)
CH (1)	CH630078A5 (cs)
CS (1)	CS199378B1 (cs)
DD (1)	DD131171A2 (cs)
DE (1)	DE2714938A1 (cs)
HU (1)	HU176612B (cs)
NL (1)	NL7711232A (cs)
SU (1)	SU854929A1 (cs)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
AT396589B (de) *	1990-06-05	1993-10-25	Chemie Linz Gmbh	Verfahren zur herstellung von allantoin
RU2176910C1 (ru) *	2000-06-26	2001-12-20	Ростовский государственный университет	Антиоксидант

1976
- 1976-10-29 DD DD19551776A patent/DD131171A2/xx unknown
1977
- 1977-04-02 DE DE19772714938 patent/DE2714938A1/de not_active Withdrawn
- 1977-05-04 HU HUSI001573 patent/HU176612B/hu unknown
- 1977-05-17 CS CS322877A patent/CS199378B1/cs unknown
- 1977-05-23 BG BG3638777A patent/BG37288A1/xx unknown
- 1977-10-10 SU SU772530556A patent/SU854929A1/ru active
- 1977-10-13 NL NL7711232A patent/NL7711232A/xx not_active Application Discontinuation
- 1977-10-27 CH CH1307977A patent/CH630078A5/de not_active IP Right Cessation

Also Published As

Publication number	Publication date
DD131171A2 (de)	1978-06-07
DE2714938A1 (de)	1978-05-11
CH630078A5 (en)	1982-05-28
CS199378B1 (en)	1980-07-31
BG37288A1 (en)	1985-05-15
NL7711232A (nl)	1978-05-03
HU176612B (en)	1981-03-28

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