TR199900516T2 - 6-Aminokapronitril ve heksametilendiamin'in ayni zamanli üretimi için yöntem. - Google Patents
6-Aminokapronitril ve heksametilendiamin'in ayni zamanli üretimi için yöntem.Info
- Publication number
- TR199900516T2 TR199900516T2 TR1999/00516T TR9900516T TR199900516T2 TR 199900516 T2 TR199900516 T2 TR 199900516T2 TR 1999/00516 T TR1999/00516 T TR 1999/00516T TR 9900516 T TR9900516 T TR 9900516T TR 199900516 T2 TR199900516 T2 TR 199900516T2
- Authority
- TR
- Turkey
- Prior art keywords
- aminocapronitrile
- hexamethylenediamine
- phosphorus
- mixture
- compound
- Prior art date
Links
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 title abstract 6
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 title abstract 3
- 239000000203 mixture Substances 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 abstract 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- -1 cyanide hydrogen Chemical class 0.000 abstract 1
- 230000036571 hydration Effects 0.000 abstract 1
- 238000006703 hydration reaction Methods 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229910052698 phosphorus Inorganic materials 0.000 abstract 1
- 239000011574 phosphorus Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Özelligi (1) fosfor yüklü bir bilesikteki fosfor olarak hesaplanan agirlik payinin, karisimda indirgenmesi ve (2) elde edilen karisimin bir katalizörün varliginda bir alfa, omega-aminonitrile kismen hidratize edilmesi ve (3) 6-aminokapronitril ve heksametilendiaminin karisimdan ayrilmasi olan, fosfor yüklü bir bilesik ve esas itibariyle adipodinitril içeren ve dönüstürme vasitasiyla butadienden siyanür hidrojen asidi ile, fosfor yüklü bir bilesik içeren bir katalizörün varliginda elde edilen bir karisimdan yola çikilarak 6-aminokapronitril ve heksametilendiamin'in ayni zamanli üretilmesi için yöntem.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19636765A DE19636765A1 (de) | 1996-09-10 | 1996-09-10 | Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TR199900516T2 true TR199900516T2 (tr) | 1999-07-21 |
Family
ID=7805164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TR1999/00516T TR199900516T2 (tr) | 1996-09-10 | 1997-08-21 | 6-Aminokapronitril ve heksametilendiamin'in ayni zamanli üretimi için yöntem. |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US6147247A (tr) |
| EP (1) | EP0929513B1 (tr) |
| JP (1) | JP2001500135A (tr) |
| KR (1) | KR100550177B1 (tr) |
| CN (1) | CN1113854C (tr) |
| AU (1) | AU4380397A (tr) |
| BR (1) | BR9711718A (tr) |
| CA (1) | CA2265488C (tr) |
| CZ (1) | CZ81099A3 (tr) |
| DE (2) | DE19636765A1 (tr) |
| ES (1) | ES2156401T3 (tr) |
| ID (1) | ID18456A (tr) |
| MY (1) | MY116967A (tr) |
| TR (1) | TR199900516T2 (tr) |
| TW (1) | TW372953B (tr) |
| WO (1) | WO1998011051A1 (tr) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19704615A1 (de) * | 1997-02-07 | 1998-08-13 | Basf Ag | Verfahren zur Hydrierung von Verbindungen aus der Gruppe der Imine oder Enamine |
| DE19742221A1 (de) * | 1997-09-24 | 1999-03-25 | Basf Ag | Verfahren zur Herstellung von aliphatischen alpha,omega-Aminonitrilen |
| US6346641B1 (en) * | 1998-07-20 | 2002-02-12 | Basf Aktiengesellschaft | Method for simultaneous production of 6-aminocapronitrile and hexamethylenediamine |
| DE19839338A1 (de) * | 1998-08-28 | 2000-03-02 | Basf Ag | Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin |
| FR2850966B1 (fr) | 2003-02-10 | 2005-03-18 | Rhodia Polyamide Intermediates | Procede de fabrication de composes dinitriles |
| FR2854891B1 (fr) | 2003-05-12 | 2006-07-07 | Rhodia Polyamide Intermediates | Procede de preparation de dinitriles |
| US7973174B2 (en) | 2005-10-18 | 2011-07-05 | Invista North America S.A.R.L. | Process of making 3-aminopentanenitrile |
| WO2007109005A2 (en) | 2006-03-17 | 2007-09-27 | Invista Technologies S.A R.L. | Method for the purification of triorganophosphites by treatment with a basic additive |
| US7880028B2 (en) | 2006-07-14 | 2011-02-01 | Invista North America S.A R.L. | Process for making 3-pentenenitrile by hydrocyanation of butadiene |
| US7919646B2 (en) | 2006-07-14 | 2011-04-05 | Invista North America S.A R.L. | Hydrocyanation of 2-pentenenitrile |
| CN101687658B (zh) | 2007-05-14 | 2013-07-24 | 因温斯特技术公司 | 高效反应器和方法 |
| WO2008157218A1 (en) | 2007-06-13 | 2008-12-24 | Invista Technologies S.A.R.L. | Process for improving adiponitrile quality |
| WO2009091790A1 (en) | 2008-01-15 | 2009-07-23 | Invista Technologies S.A.R.L. | Hydrocyanation of pentenenitriles |
| US7977502B2 (en) | 2008-01-15 | 2011-07-12 | Invista North America S.A R.L. | Process for making and refining 3-pentenenitrile, and for refining 2-methyl-3-butenenitrile |
| EP2334624B1 (en) | 2008-10-14 | 2014-10-01 | Invista Technologies S.à.r.l. | Process for making 2-secondary-alkyl-4,5-di-(normal-alkyl)phenols |
| CN102471218B (zh) | 2009-08-07 | 2014-11-05 | 因温斯特技术公司 | 用于形成二酯的氢化并酯化 |
| EP3416940B1 (en) * | 2016-02-16 | 2019-10-30 | INVISTA Textiles (U.K.) Limited | Promoter for selective nitrile hydrogenation |
| CN108084035A (zh) * | 2017-12-11 | 2018-05-29 | 大连理工大学 | 一种无碱条件下己二腈直接氢化制己二胺的方法 |
| CN114192170A (zh) * | 2021-12-27 | 2022-03-18 | 于向真 | 一种从环己酮肟或己内酰胺合成6-氨基己腈的催化剂及其制备方法 |
| CN117000290B (zh) * | 2022-04-29 | 2025-12-16 | 中国石油化工股份有限公司 | 六亚甲基亚胺合成己二胺的催化剂及其制备方法和合成己二胺的方法 |
| CN117003648B (zh) * | 2022-04-29 | 2025-08-12 | 中国石油化工股份有限公司 | 一种由己内酰胺制备己二胺的方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE235466C (tr) * | ||||
| US2208598A (en) * | 1938-09-24 | 1940-07-23 | Du Pont | Aliphatic amino-nitriles and process of producing them |
| DE848654C (de) * | 1950-08-19 | 1952-09-08 | Basf Ag | Verfahren zur Herstellung von partiellen Hydrierungsprodukten des Adipinsaeuredinitrils |
| US2762835A (en) * | 1953-03-12 | 1956-09-11 | Celanese Corp | Preparation of amino nitriles |
| DE954161C (de) * | 1953-09-06 | 1956-12-13 | Siemens Ag | Einrichtung an Fernschreibmaschinen mit Tastaturwahl |
| BE792649A (fr) * | 1971-12-13 | 1973-06-12 | Rhone Poulenc Sa | Catalyseur a base de nickel raney au fer |
| US4389348A (en) * | 1981-10-26 | 1983-06-21 | Allied Corporation | Selective hydrogenation of dinitrile to omega-aminonitrile and supported rhodium-containing catalyst therefor |
| US4601859A (en) * | 1984-05-04 | 1986-07-22 | Allied Corporation | Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst |
| GB8726279D0 (en) * | 1987-11-10 | 1987-12-16 | Ici Plc | Separation of phosphorus compounds |
| US5151543A (en) * | 1991-05-31 | 1992-09-29 | E. I. Du Pont De Nemours And Company | Selective low pressure hydrogenation of a dinitrile to an aminonitrile |
| NL9102112A (nl) * | 1991-12-18 | 1993-07-16 | Dsm Nv | Werkwijze voor het bereiden van een aminonitril door het partieel hydrogeneren van een nitrilverbinding met twee of meer nitrilgroepen. |
| DE4235466A1 (de) * | 1992-10-21 | 1994-04-28 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Aminonitrilen |
| DE19500222A1 (de) * | 1995-01-05 | 1996-07-11 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
| US5717090A (en) * | 1995-01-05 | 1998-02-10 | Basf Aktiengesellschaft | Simultaneous preparation of caprolactam and hexamethylenediamine |
| US5599962A (en) * | 1995-01-31 | 1997-02-04 | E. I. Du Pont De Nemours And Company | Process for the preparation of ruthenium hydrogenation catalysts and products thereof |
| DE19548289A1 (de) * | 1995-12-22 | 1997-06-26 | Basf Ag | Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin |
-
1996
- 1996-09-10 DE DE19636765A patent/DE19636765A1/de not_active Withdrawn
-
1997
- 1997-08-21 BR BR9711718A patent/BR9711718A/pt not_active IP Right Cessation
- 1997-08-21 CN CN97199516A patent/CN1113854C/zh not_active Expired - Fee Related
- 1997-08-21 US US09/254,454 patent/US6147247A/en not_active Expired - Lifetime
- 1997-08-21 AU AU43803/97A patent/AU4380397A/en not_active Abandoned
- 1997-08-21 JP JP10513186A patent/JP2001500135A/ja not_active Withdrawn
- 1997-08-21 DE DE59703361T patent/DE59703361D1/de not_active Expired - Fee Related
- 1997-08-21 ES ES97941948T patent/ES2156401T3/es not_active Expired - Lifetime
- 1997-08-21 TR TR1999/00516T patent/TR199900516T2/tr unknown
- 1997-08-21 CA CA002265488A patent/CA2265488C/en not_active Expired - Fee Related
- 1997-08-21 EP EP97941948A patent/EP0929513B1/de not_active Expired - Lifetime
- 1997-08-21 CZ CZ99810A patent/CZ81099A3/cs unknown
- 1997-08-21 KR KR1019997001940A patent/KR100550177B1/ko not_active Expired - Fee Related
- 1997-08-21 WO PCT/EP1997/004542 patent/WO1998011051A1/de not_active Ceased
- 1997-09-09 MY MYPI97004170A patent/MY116967A/en unknown
- 1997-09-10 ID IDP973147A patent/ID18456A/id unknown
- 1997-11-07 TW TW086113117A patent/TW372953B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| CZ81099A3 (cs) | 1999-06-16 |
| ID18456A (id) | 1998-04-09 |
| KR20000035988A (ko) | 2000-06-26 |
| CN1113854C (zh) | 2003-07-09 |
| DE59703361D1 (de) | 2001-05-17 |
| CN1236355A (zh) | 1999-11-24 |
| US6147247A (en) | 2000-11-14 |
| KR100550177B1 (ko) | 2006-02-10 |
| CA2265488A1 (en) | 1998-03-19 |
| EP0929513A1 (de) | 1999-07-21 |
| CA2265488C (en) | 2005-10-25 |
| DE19636765A1 (de) | 1998-03-12 |
| ES2156401T3 (es) | 2001-06-16 |
| AU4380397A (en) | 1998-04-02 |
| BR9711718A (pt) | 1999-08-24 |
| JP2001500135A (ja) | 2001-01-09 |
| MY116967A (en) | 2004-04-30 |
| EP0929513B1 (de) | 2001-04-11 |
| WO1998011051A1 (de) | 1998-03-19 |
| TW372953B (en) | 1999-11-01 |
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